| Search |
| [Next Page] |
thionyl chloride synthesis
Thanks, S.C. Jor may want to look into that muddle but I am more interested in some of the other stu ... |
31-1-2009 at 16:30
by: Sauron |
thionyl chloride synthesis
Consider adding a scrubber system.
You and your neighbors will be happier.
Your blower's moto ... |
31-1-2009 at 15:18
by: Sauron |
thionyl chloride synthesis
Jor apparently has no fume hood.
I just looked up Cl2O in Brauer and this is not so bad. Cl2 drie ... |
31-1-2009 at 15:10
by: Sauron |
thionyl chloride synthesis
Besides the "new" sulfite method, which is only a variation on SO2 and PCl5, and thus only available ... |
31-1-2009 at 14:21
by: Sauron |
thionyl chloride synthesis
Here is the entry I am talking aout from Britannica 1911:
"There are various haloid derivatives o ... |
31-1-2009 at 13:12
by: Sauron |
thionyl chloride synthesis
Just go to Google, search for 1911 encyclopedia, and the Britannica free edition comes right up
S ... |
31-1-2009 at 12:40
by: Sauron |
thionyl chloride synthesis
I did not vaguely remember that sodium sulfite reacts with PCl5 to produce SOCl2. I said that I foun ... |
31-1-2009 at 12:19
by: Sauron |
Practical Vacuum Distillation
There's simple vacuum distillation such as stripping solvent using a rotavap and aspirator pump, and ... |
31-1-2009 at 01:23
by: Sauron |
Oxidation of p-dioxan to Glycolide
Here is a US patent teaching the preparation of glycolide of high purity by the following steps
... |
31-1-2009 at 00:18
by: Sauron |
Oxidation of p-dioxan to Glycolide
Hissingnoise:
Totally wrong!
a) It's a very comfy judge's chair, not a rocker, and
b) It's ... |
30-1-2009 at 21:50
by: Sauron |
preparation of salicylic acid from anthranilic acid
You mean, to get methyl anthranilate?
Anthranilic acid is not that hard to make, from phthalimide ... |
30-1-2009 at 10:22
by: Sauron |
Oxidation of p-dioxan to Glycolide
Glycolide, or diglycolide is the cyclic dimer of glycolic acid. Properly it is 1,4-dioxan-2,5-dione ... |
30-1-2009 at 09:42
by: Sauron |
preparation of salicylic acid from anthranilic acid
It does sound like homework or an open book exam question, doesn't it?
Intermediates in diazotiza ... |
30-1-2009 at 06:55
by: Sauron |
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
Methyl Magic, did you try contacting Swiss chemical companies like Fluka?
They belong to Sigma-Al ... |
30-1-2009 at 00:07
by: Sauron |
fan selection for homemade fumehood - help
Do yourself a real favo and get a proper lab fume hood blower, which is driven by a separate motor s ... |
29-1-2009 at 20:39
by: Sauron |
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
Are you in the right thread, fella?
This one is about oxalyl chloride. |
29-1-2009 at 20:22
by: Sauron |
preparation of salicylic acid from anthranilic acid
I completely agree that salicylic acid is a whole lot easier to come by than anthranilic acid.
So ... |
29-1-2009 at 19:02
by: Sauron |
strange (?) results from nitrating toluene
Maybe she ate it. |
28-1-2009 at 21:36
by: Sauron |
strange (?) results from nitrating toluene
Does that come as a surprise to anyone here?
I thought the thread was about what was supposed to ... |
28-1-2009 at 01:53
by: Sauron |
Leuckart reaction
Youmight just consider getting fresh lit. yourself.
Google
ACS Pubs search engine
RSC searc ... |
28-1-2009 at 00:52
by: Sauron |
Acid Concentration/purification
Guess what? You do not have the power to close a thread, not even your own. |
27-1-2009 at 20:15
by: Sauron |
Uses of Chlorine
Do the words FUME HOOD mean anything to you? |
27-1-2009 at 19:41
by: Sauron |
strange (?) results from nitrating toluene
If you want to have exclusively mononitrotoluenes you must strictly regulate temperature to below 30 ... |
27-1-2009 at 12:25
by: Sauron |
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
The stoichiometry of the reaction between oxalic acid and PCl5 is
(COOH)2 + 2 PCl5 -> 2 POCl3 ... |
27-1-2009 at 10:55
by: Sauron |
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
[quote][i]Originally posted by harrydrez[/i]
He said that you can make your own TCT using methyl th ... |
27-1-2009 at 10:37
by: Sauron |
| [Next Page] |
