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Acetic anhydride preparation
Engager, acetic anhydride can be made by adding SOCl2 to boiling glacial acetic acid using a reflux ... |
25-8-2008 at 07:49
by: Formatik |
Aniline
[quote] Just heat condense the vapour and redistill. Im waiting on some new glassware at the moment ... |
24-8-2008 at 16:01
by: Formatik |
Hydrogen Peroxide Production
[quote][i]Originally posted by Klute[/i]
I don't think distillation of H2O2 from persulfuric/sulfur ... |
24-8-2008 at 15:34
by: Formatik |
Hydrogen Peroxide Production
Not as insoluble, but in place of barium peroxide, at least CaO2 could also be used. MgO2, ZnO2, SrO ... |
24-8-2008 at 06:33
by: Formatik |
Perchloric acid preparation
[quote][i]Originally posted by chloric1[/i]
Several years ago I made about 100 to 150ml of Aqua reg ... |
21-8-2008 at 20:11
by: Formatik |
Interesting energetic materials
Here's another drawing of 1,6-Di(tetrazol-5-yl)hexazadiene:
[img]http://i296.photobucket.com/albu ... |
21-8-2008 at 20:03
by: Formatik |
Hypergolic Reactions and Energetics
Another simple oxidant worth investigating is bromine trifluoride (BrF3) made by just combining F2 w ... |
21-8-2008 at 15:22
by: Formatik |
1,3 Acetonedicarboxylic Acid
Have a look at the OrgSyn procedure. For an idea on low yields with just conc. H2SO4, see [url=http: ... |
18-8-2008 at 12:06
by: Formatik |
Propylene (oxide) synthesis
[quote][i]Originally posted by 497[/i] @ Shockwave Thanks for that information, I will probably us ... |
18-8-2008 at 11:22
by: Formatik |
Ammonium chlorate?
[quote][i]Originally posted by IrC[/i] Also, it is much more powerful than the iodide. [/quote]
T ... |
17-8-2008 at 20:44
by: Formatik |
HCl from bisulfates
Molten KHSO4 (Mp. 210ºC) reacts with KCl under formation of HCl (E. Mitscherlich, Pogg. Ann. 18 [18 ... |
17-8-2008 at 20:24
by: Formatik |
Interesting energetic materials
[b]Ozobenzene[/b]:
[img]http://i296.photobucket.com/albums/mm198/userp1/ozobenz.jpg[/img]
made ... |
17-8-2008 at 20:18
by: Formatik |
Ammonium chlorate?
[quote][i]Originally posted by IrC[/i]
NCl3 is much like the iodine cousin, so sensitive (especiall ... |
12-8-2008 at 14:45
by: Formatik |
Possible Route to Copper Nitrate
The mods should remove those posts. I will start another thread on this, since I haven't seen this d ... |
10-8-2008 at 20:00
by: Formatik |
Possible Route to Copper Nitrate
Why not just heat inorganic copper salts with a nitrate? Heating under a low flame (bunsen burner) a ... |
10-8-2008 at 17:35
by: Formatik |
Chloratomercuraldehydes and relateds
The compound [b]2-methyl-1-nitratodimercurio-2-nitratomercuriopropane[/b]
[img]http://i296.photob ... |
8-8-2008 at 22:46
by: Formatik |
Chloratomercuraldehydes and relateds
The first is: [b]Chloratodimercuraldehyde[/b], OHC.C(:Hg).Hg.O.ClO2 = C2Hg2ClO4H, this one is best ... |
8-8-2008 at 19:38
by: Formatik |
what is the reaction with urea?
I don't know why this is in this section. But NaBrO reacts quicker with urea than NaClO at regular t ... |
7-8-2008 at 23:22
by: Formatik |
Sensitized nitroparaffin
An interesting patent for this is [url=http://www.google.com/patents?id=GRVUAAAAEBAJ&printsec=ab ... |
7-8-2008 at 23:13
by: Formatik |
ONT
My relative strength estimate: 114% of TNT, by averaging the results of two methods. And for a relat ... |
7-8-2008 at 22:38
by: Formatik |
NA from Pb(NO3)2
It’s a good idea if you have no other options, but Cu(NO3)2 (decomposition temperature 170°C) is ... |
7-8-2008 at 01:06
by: Formatik |
New Energetic Materials - Current Research
[quote][i]Originally posted by Ritter[/i]
If DNB is such great stuff, why isn't there a lot of lite ... |
2-8-2008 at 22:40
by: Formatik |
What reagent would you like to see an illustrated guide for?
[quote][i]Originally posted by kclo4[/i] I added Conc. Hydrochloric acid to my Potassium nitrite and ... |
2-8-2008 at 15:08
by: Formatik |
New Energetic Materials - Current Research
"nitrobiuret ... prepared by adding biuret in small portions to a mixture of concentrated nitric and ... |
2-8-2008 at 14:56
by: Formatik |
FOX-7
[quote][i]Originally posted by Engager[/i]
Dinitrobiurete seems much more easy to make (urea is sta ... |
2-8-2008 at 14:54
by: Formatik |
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