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Synthesis of Sulfur Trioxide and Oleum: The persulfate method
I have a few more pictures which I thought might be appreciated by someone trying to follow the expe ...
27-7-2014 at 09:51
by: Hennig Brand
The best way to physically destroy an hard disk
[rquote=339342&tid=31588&author=chornedsnorkack][rquote=339146&tid=31588&author=Henn ...
24-7-2014 at 10:34
by: Hennig Brand
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
Thanks Garage Chemist, I will definitely use your suggestions on my next batch.

Edit:

Ok, I ra ...
23-7-2014 at 05:06
by: Hennig Brand
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
I didn't have it all thought through when I gave the specifications to the glass blower for the quar ...
21-7-2014 at 11:09
by: Hennig Brand
Selling my lab
Just got my order today. Everything looks pretty good and was well packaged.
21-7-2014 at 09:46
by: Hennig Brand
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
I have been off and on working on building a small electric furnace for the last several weeks so th ...
21-7-2014 at 08:19
by: Hennig Brand
The best way to physically destroy an hard disk
Have a look at these pictures which show 14g being tested on a piece of structural steel. Yeah, I th ...
21-7-2014 at 07:56
by: Hennig Brand
The best way to physically destroy an hard disk
My comment about the plastic explosives may not have been the best form of humor, but it seemed like ...
20-7-2014 at 16:51
by: Hennig Brand
The best way to physically destroy an hard disk
Just put a large drill bit in your cordless drill or drill press and drill a large hole (off center) ...
20-7-2014 at 08:16
by: Hennig Brand
DIY distillation app
Sorry for the multiple posting, but I have a small correction for the above post. The receiving flas ...
20-7-2014 at 08:01
by: Hennig Brand
What do you do to prevent yourself from chemicals?
I think it is a good question for someone concerned about their health, especially if exposure is go ...
18-7-2014 at 18:36
by: Hennig Brand
Trinitrotoluene preparation
[rquote=336454&tid=29&author=nitro-genes] The product I obtained back then was slightly yell ...
18-7-2014 at 08:11
by: Hennig Brand
DIY distillation app
I made a few changes to the simple still I posted pictures and a description of in the nitric acid s ...
15-7-2014 at 12:28
by: Hennig Brand
DIY distillation app
I forgot about this thread and made a post about a simple homemade glass distillation apparatus made ...
2-7-2014 at 06:57
by: Hennig Brand
Trinitrotoluene preparation
Thanks for the pointers. I gave the warm NaHCO3 solution wash a try and there was considerable bubbl ...
1-7-2014 at 14:05
by: Hennig Brand
Nitric Acid Synthesis
Simple is often better. ;)

I always wanted one of those, and actually spent some time looking in ...
1-7-2014 at 09:36
by: Hennig Brand
Trinitrotoluene preparation
The following was basically taken right from COPAE, though the words may have gotten changed around ...
30-6-2014 at 18:02
by: Hennig Brand
Cheap and Effective Nitric Acid Distillation Apparatus
Here is a very simple little glass still I made a year or so ago from common flasks without ground g ...
30-6-2014 at 12:03
by: Hennig Brand
Trinitrotoluene preparation
The product did eventually solidify after it was washed with water, and cooled more, and changed in ...
30-6-2014 at 10:30
by: Hennig Brand
Trinitrotoluene preparation
Just above in this thread: http://www.sciencemadness.org/talk/viewthread.php?tid=29&page=8#pid25 ...
30-6-2014 at 10:15
by: Hennig Brand
picramic acid from picric
Yes, playing around with the exponential growth equation and using bacterial growth as an example ma ...
27-6-2014 at 06:22
by: Hennig Brand
picramic acid from picric
Yes, a titration like was described in the Hodgson and Ward paper to determine yield. I still have s ...
25-6-2014 at 11:58
by: Hennig Brand
picramic acid from picric
[rquote=335616&tid=433&author=nitro-genes] After complete reaction, the resulting NaSH solut ...
25-6-2014 at 06:19
by: Hennig Brand
picramic acid from picric
Nice pictures, looks like you have had success. That's a pretty clever idea using Al2S3. Interested ...
24-6-2014 at 12:52
by: Hennig Brand
picramic acid from picric
Thanks for the high praise. I am more of an explosives and science/technology enthusiast than a chem ...
24-6-2014 at 05:41
by: Hennig Brand
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