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Quantitative NHN synthesis without Hydrazine hydrate
Here is my end result! 8 grams (wow! I wasn't expecting that much!) of clay like NHN. I did burn the ... |
17-12-2021 at 15:23
by: ManyInterests |
Trying for Keto-RDX
[rquote=668798&tid=28395&author=Microtek]If you are satisfied with some of your tests being ... |
17-12-2021 at 10:45
by: ManyInterests |
Trying for Keto-RDX
I have cleaning grade sawdust that is quite thick and all.
But that being said. My keto-RDX synth ... |
17-12-2021 at 09:55
by: ManyInterests |
Trying for Keto-RDX
It's good that I don't need a lot of acetone. However, I don't plan on seperating the K6 from the RD ... |
16-12-2021 at 17:12
by: ManyInterests |
Why are my hydrazine sulfate yields so high?
I don't know if I mentioned it here. But I figured out what happened wrong.
My synthesis didn't w ... |
16-12-2021 at 16:19
by: ManyInterests |
Trying for Keto-RDX
OK so after talking to fredsci93. I plan on using regular hexamine for my synthesis. I measured by e ... |
16-12-2021 at 14:30
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
Well it snowed quite heavily today, so I got a natural ice bath!  |
15-12-2021 at 20:51
by: ManyInterests |
Trying for Keto-RDX
I'm going to making my one and only Keto-RDX synthesis in a few days and I decided to bump this thre ... |
15-12-2021 at 12:09
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
Yeah I forgot about the acid washes and the whole process. Someone told me about an entire battery o ... |
15-12-2021 at 11:25
by: ManyInterests |
NHN synthesis not working
That is good. Because the only danger I ever subjected myself to was disposing of dangerous chemical ... |
15-12-2021 at 03:42
by: ManyInterests |
NHN synthesis not working
Yes. I threw everything at this including my kitchen sink. Now I need to dry this stuff near the rad ... |
15-12-2021 at 02:36
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
Yep. Like you said in the other thread, 10% or 5%. I'll dilute some HCl tomorrow. I ran some quick s ... |
14-12-2021 at 22:21
by: ManyInterests |
Quantitative NHN synthesis without Hydrazine hydrate
OK, so my HCl is around 31.5%, so to 1 part of that, add 2.5 parts of water. simple enough.
[Edited ... |
14-12-2021 at 22:07
by: ManyInterests |
NHN synthesis not working
The glass pan next to it has all my other filterates. I filtered as much as I could of the stuff bef ... |
14-12-2021 at 22:04
by: ManyInterests |
Quantitative NHN synthesis without Hydrazine hydrate
That's good to know. How dilute does the HCl need to be? |
14-12-2021 at 20:54
by: ManyInterests |
NHN synthesis not working
It was as purple as can be! I got me a very large batch of NHN. More than I could ever use in a life ... |
14-12-2021 at 20:52
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
That sounds good. It's what I am doing now.
It is turning the NHN green, as neutralizing it seems ... |
14-12-2021 at 20:50
by: ManyInterests |
Quantitative NHN synthesis without Hydrazine hydrate
so... hurray! I appear to have succeeded.
Bad news? I seem to have a problem cleaning my buchner ... |
14-12-2021 at 20:22
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
Actually wait. I think a sodium hydroxide solution will clear it. I need to wash it several times. I ... |
14-12-2021 at 20:01
by: ManyInterests |
Cleaning buchner funnel after NHN synthesis
I finally succeeded in making some NHN. I believe I filtered off all that I can filter off (the rest ... |
14-12-2021 at 19:46
by: ManyInterests |
NHN synthesis not working
OMG I DID IT!
I realized that I could have freebased so much more hydrazine! I did it! I did it i ... |
14-12-2021 at 18:25
by: ManyInterests |
NHN synthesis not working
OK... I freebased some hydrazine... but I think I added far too much ethanol to the mix. I added aro ... |
14-12-2021 at 18:00
by: ManyInterests |
NHN synthesis not working
Yes I did. The issue didn't happen during synthesis. It happened during my attempts to neutralize th ... |
14-12-2021 at 12:52
by: ManyInterests |
NHN synthesis not working
I was not experimenting with chlorine. I was using bleach to neutralize left over hydrazine.
Also ... |
14-12-2021 at 08:53
by: ManyInterests |
NHN synthesis not working
I made a mistake. I won't make that mistake again and it never happened like this before... Ever. I ... |
14-12-2021 at 05:13
by: ManyInterests |
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