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Platinum anode problem
Hmmm. Chloroplatinic acid can be formed by anodizing Platinum in concentrated HCl.

Platinum does ...
4-9-2018 at 15:41
by: zed
Safe to buy from China?
Well yeah. Some of the companies utilize fake feedback, and some of the products are crap.

But, ...
1-9-2018 at 12:53
by: zed
My vacuum pump
Those 30+ Dollar, U.S. models, have a different type of threaded connector.

You can screw them ri ...
1-9-2018 at 12:39
by: zed
cobalt chloride desiccant dangerous?
Back in the day, every child's chemistry set, was stocked with Cobalt Chloride.

We were not espec ...
28-8-2018 at 14:39
by: zed
cobalt chloride desiccant dangerous?
If Cobalt Chloride is very dangerous, we all died a long time ago.

Might have some nasty secrets ...
26-8-2018 at 15:50
by: zed
Anethol in Aniseed/Fennel - Kitchen Chemistry
Well, it has been suggested that Myristicin may undergo an amination in Vivo. Thus accounting for ...
25-8-2018 at 16:51
by: zed
Color of Phenylacetone
Did you open it? Letting O2 into the bottle seems to lead to discoloration.
25-8-2018 at 16:16
by: zed
anyone have experience forming grignards from chlorobenzene
Guys in my neighborhood never did it that way. Bromobenzene forms a Grignard reagent relatively ea ...
17-8-2018 at 15:24
by: zed
Where can I buy precious metals for cheapest prices?
Below spot? Unlikely.

Jewelers and metal buyers, may pay less than spot for scrap (or used jewe ...
12-8-2018 at 15:16
by: zed
Where to get pyridine in UK ?
I have heard that Pyridine might not be an easy buy, here in the U.S..

Easily reduced to Piperidi ...
6-8-2018 at 16:22
by: zed
Looking for cheap lab glass distributor in the US.
Deschem shipments (from China) often arrive within 7 days. At least, in Portland.

Depends.
6-8-2018 at 16:16
by: zed
knoevenagel condensation NaOH catalyst?
http://www.orgsyn.org/demo.aspx?prep=CV1P0413

From Organic Synthesis.

In the distant past, I a ...
4-8-2018 at 12:34
by: zed
Hydrogenolysis of benzylic esters - looking for references
Umm. Somehow reminiscent of Alkylating Indoles, with Amido-Alcohols.

Newfangled kinda thinking. ...
4-8-2018 at 12:23
by: zed
Hydrogenolysis of benzylic esters - looking for references
Lots of ways to perform that reduction. Ester or not.

Commonplace is P/I2. Too easy, in fact. ...
3-8-2018 at 15:09
by: zed
How do you clean stubbornly dirty glassware when no solvent seems to work?
Abrasive cleaning powder?

For cleaning diner coffee pots:Put Dutch Cleanser (Ajax etc.) in flask, ...
27-7-2018 at 16:34
by: zed
P2NP synthesis/crystalization problem
Either the Soxhlet extractor or the Dean-Stark trap, may be used to drive the reaction, in the afore ...
27-7-2018 at 16:15
by: zed
P2NP synthesis/crystalization problem
Try a better procedure.

https://www.thevespiary.org/rhodium/Rhodium/Vespiary/talk/files/938-Physi ...
27-7-2018 at 15:35
by: zed
Increasing water pump pressure using 2 pumps in series?
In series? Sure. Why not? Provided the pumps and parts, can survive the pressure differential wi ...
26-7-2018 at 13:23
by: zed
How should I choose glass joint size?
Umm. Deschem and Nanshin, have online E-bay stores, that you can peruse as required.

Lots of Sox ...
16-7-2018 at 15:31
by: zed
Choosing best reflux column & condenser to order
24/40 glassware is relatively large and sturdy. I received several 200 MM Grahams from Deschem, the ...
16-7-2018 at 15:07
by: zed
D.I.Y. Silicone Stoppers/Bungs ?
I have applied this type of Silicone sealant, and the solvent in it, as I remember by smell, is Glac ...
12-7-2018 at 15:28
by: zed
Magnet oh hotplate stirrer - does it loose stength when hot?
I have some Neodymium type stir bars. Sheathed in HDPE. I made 'em. Their original plating, was j ...
12-7-2018 at 15:17
by: zed
Copper Borate Synthesis and Reactions
Ummm. Recently soaked some wood with a Copper Sulfate solution, followed by a baking soda solution ...
12-7-2018 at 14:29
by: zed
"Unprecedented" reduction of amides
The restriction of LiAlH4 sales, predates current regulations.

Perhaps liability fears, are at th ...
11-7-2018 at 11:25
by: zed
hydrogenolysis with lithium aluminium hydride
What article?

Include a link. It is, in fact, kind of a rule.

Start a topic; include a refere ...
3-7-2018 at 13:20
by: zed
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