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Halogenated Amines - the others From the reference: "explodes violently on heating". I hit it with a MAPP torch, and even ... |
2-12-2004 at 21:44 by: Axt |
Halogenated Amines - the others Nitrogen trichloride and nitrogen triiodide are well known. but what of the others?
Below is some ... |
2-12-2004 at 18:47 by: Axt |
Exotic Primaries - Complex Salts OK, just got some ethylenediamine, since chemoleo has reported that the persulphate precipitates eas ... |
30-11-2004 at 15:11 by: Axt |
acetic peroxide I dont see any reference to sodium peracetate there Organikum!? Sodium perborates are, at the link a ... |
29-11-2004 at 03:14 by: Axt |
HCl + H2O2 = ? Are you by any chance talking about "diggers" HCl? |
26-11-2004 at 04:32 by: Axt |
h202 concentration? Ive shaken H2O2 with ether, I think you would have a hard time hurting yourself with the mix, unless ... |
25-11-2004 at 21:34 by: Axt |
HCl + H2O2 = ? Its not the HCl, more likely a metal salt dissolved in it. Oxidation of ferrous to ferric chloride i ... |
25-11-2004 at 04:14 by: Axt |
Organic Hypochlorites I cant give any more info, only did it once. I chucked a match at it. It takes fire <i>very< ... |
29-10-2004 at 18:58 by: Axt |
Organic Hypochlorites I made EtOCl a while ago, by the method Blaster has just mentioned. Using HCl/MnO2 to generate the c ... |
28-10-2004 at 14:13 by: Axt |
Nitroisobutylglycerol Trinitrate I'd be trying baking soda (NaHCO3) if K2CO3 isnt available. |
28-10-2004 at 13:59 by: Axt |
Ammonium permanganate preparation What did the crystals look like, If you went as far to freeze it I think it less then pure. While it ... |
28-10-2004 at 13:54 by: Axt |
Ammonium permanganate preparation It says 7.9 @ 15°C in CRC. One of them has it wrong.
0.8's a typo I reckon! If that were th ... |
25-10-2004 at 17:31 by: Axt |
Ammonium permanganate preparation [quote][i]Originally posted by neutrino[/i]
NH<sub>4</sub>MnO<sub>4</sub> = ... |
24-10-2004 at 12:05 by: Axt |
Organic peroxides Conveniently, its fairly soluble in Acetone (I think more-so in DCM), why you ask? |
19-10-2004 at 09:17 by: Axt |
Exotic Primaries - Complex Salts [quote][i]Originally posted by Axt[/i]
12.5N2[/quote]
7.5N2 ![:(](./images/smilies/sad.gif)
Mellor 9 (1939), 795 for K2O6V ... |
18-10-2004 at 09:12 by: Axt |
Ammonium permanganate preparation As per pm request,
The ammonium permanganate vid I have <a href="http://geocities.com/rog ... |
18-10-2004 at 08:44 by: Axt |
Nitrated sugars [quote][i]Originally posted by Rosco Bodine[/i]
Axt , did you ever experiment with different ratios ... |
18-10-2004 at 08:30 by: Axt |
Exotic Primaries - Complex Salts Talking of complex persulphates, what of the other peroxy complexes! its a whole branch that hasnt b ... |
18-10-2004 at 08:12 by: Axt |
Nitrated sugars HN = hydrogen nitrate, nitric acid. Seemed like the most logical acronym at the time, but I can now ... |
18-10-2004 at 03:29 by: Axt |
Exotic Primaries - Complex Salts Nice ![:cool:](./images/smilies/cool.gif)
As I said before, I tried with urea, but no colour change nor precip, though I was us ... |
11-10-2004 at 06:28 by: Axt |
glycine nitrate The extract I uploaded was the reference given in Fedoroff, which supposedly gives its syth from its ... |
8-10-2004 at 22:12 by: Axt |
glycine nitrate [quote][i]Originally posted by Rosco Bodine[/i]
Since there is no method described...[/quote]
Migh ... |
7-10-2004 at 02:25 by: Axt |
Methyl Acetylides Igniting a larger amount of the copper product up today resulted in a self sustaining combustion, sm ... |
2-10-2004 at 19:10 by: Axt |
Methyl Acetylides Seems that the patent reference provided shows that straight AgNO3 should create the double salt, si ... |
2-10-2004 at 01:50 by: Axt |
Methyl Acetylides Rosco, No I havn't, and I wont get a chance to try now, won't make it home again for a cou ... |
1-10-2004 at 19:54 by: Axt |
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