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Halogenated Amines - the others
From the reference: "explodes violently on heating". I hit it with a MAPP torch, and even ...
2-12-2004 at 21:44
by: Axt
Halogenated Amines - the others
Nitrogen trichloride and nitrogen triiodide are well known. but what of the others?

Below is some ...
2-12-2004 at 18:47
by: Axt
Exotic Primaries - Complex Salts
OK, just got some ethylenediamine, since chemoleo has reported that the persulphate precipitates eas ...
30-11-2004 at 15:11
by: Axt
acetic peroxide
I dont see any reference to sodium peracetate there Organikum!? Sodium perborates are, at the link a ...
29-11-2004 at 03:14
by: Axt
HCl + H2O2 = ?
Are you by any chance talking about "diggers" HCl?
26-11-2004 at 04:32
by: Axt
h202 concentration?
Ive shaken H2O2 with ether, I think you would have a hard time hurting yourself with the mix, unless ...
25-11-2004 at 21:34
by: Axt
HCl + H2O2 = ?
Its not the HCl, more likely a metal salt dissolved in it. Oxidation of ferrous to ferric chloride i ...
25-11-2004 at 04:14
by: Axt
Organic Hypochlorites
I cant give any more info, only did it once. I chucked a match at it. It takes fire <i>very< ...
29-10-2004 at 18:58
by: Axt
Organic Hypochlorites
I made EtOCl a while ago, by the method Blaster has just mentioned. Using HCl/MnO2 to generate the c ...
28-10-2004 at 14:13
by: Axt
Nitroisobutylglycerol Trinitrate
I'd be trying baking soda (NaHCO3) if K2CO3 isnt available.
28-10-2004 at 13:59
by: Axt
Ammonium permanganate preparation
What did the crystals look like, If you went as far to freeze it I think it less then pure. While it ...
28-10-2004 at 13:54
by: Axt
Ammonium permanganate preparation
It says 7.9 @ 15°C in CRC. One of them has it wrong.

0.8's a typo I reckon! If that were th ...
25-10-2004 at 17:31
by: Axt
Ammonium permanganate preparation
[quote][i]Originally posted by neutrino[/i]
NH<sub>4</sub>MnO<sub>4</sub> = ...
24-10-2004 at 12:05
by: Axt
Organic peroxides
Conveniently, its fairly soluble in Acetone (I think more-so in DCM), why you ask?
19-10-2004 at 09:17
by: Axt
Exotic Primaries - Complex Salts
[quote][i]Originally posted by Axt[/i]
12.5N2[/quote]

7.5N2 :(

Mellor 9 (1939), 795 for K2O6V ...
18-10-2004 at 09:12
by: Axt
Ammonium permanganate preparation
As per pm request,

The ammonium permanganate vid I have <a href="http://geocities.com/rog ...
18-10-2004 at 08:44
by: Axt
Nitrated sugars
[quote][i]Originally posted by Rosco Bodine[/i]
Axt , did you ever experiment with different ratios ...
18-10-2004 at 08:30
by: Axt
Exotic Primaries - Complex Salts
Talking of complex persulphates, what of the other peroxy complexes! its a whole branch that hasnt b ...
18-10-2004 at 08:12
by: Axt
Nitrated sugars
HN = hydrogen nitrate, nitric acid. Seemed like the most logical acronym at the time, but I can now ...
18-10-2004 at 03:29
by: Axt
Exotic Primaries - Complex Salts
Nice :cool:

As I said before, I tried with urea, but no colour change nor precip, though I was us ...
11-10-2004 at 06:28
by: Axt
glycine nitrate
The extract I uploaded was the reference given in Fedoroff, which supposedly gives its syth from its ...
8-10-2004 at 22:12
by: Axt
glycine nitrate
[quote][i]Originally posted by Rosco Bodine[/i]
Since there is no method described...[/quote]
Migh ...
7-10-2004 at 02:25
by: Axt
Methyl Acetylides
Igniting a larger amount of the copper product up today resulted in a self sustaining combustion, sm ...
2-10-2004 at 19:10
by: Axt
Methyl Acetylides
Seems that the patent reference provided shows that straight AgNO3 should create the double salt, si ...
2-10-2004 at 01:50
by: Axt
Methyl Acetylides
Rosco, No I havn't, and I wont get a chance to try now, won't make it home again for a cou ...
1-10-2004 at 19:54
by: Axt
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