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Phosphorus Chlorides
John, Polverone posted about this in the Ongoing Scanning Projects thread.

Google Books does offe ...
22-2-2009 at 15:36
by: Sauron
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
Read the thread title. LOOKING FOR OXALYL CHLORIDE

So don't knock me for telling the guy the sli ...
22-2-2009 at 15:06
by: Sauron
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
The attempt to correct stupid mistakes of the ignorant is neither ranting nor raving. I said nothing ...
22-2-2009 at 13:39
by: Sauron
Phosphorus Chlorides
I did a fast OCR and test search and did not see anything about PBr3 -> PCl3 either with Cl2 or a ...
22-2-2009 at 13:32
by: Sauron
Phosphorus Chlorides
Which edition of Gmelin is that from, please?
22-2-2009 at 11:46
by: Sauron
Another "Two-for" Reaction CCl4 + PSCl3
Three members responded to translation request, two with brief but cogent synopses, the other with a ...
22-2-2009 at 02:27
by: Sauron
Parr Shaker Hydrogenator
Well, if I ever were to sell it I will give you first shot at it. But I have plans for it.
21-2-2009 at 05:01
by: Sauron
Parr Shaker Hydrogenator
I have a complete 1000 ml Parr 4521 and controller and paid $2000 for it.

The money is in the pre ...
21-2-2009 at 04:20
by: Sauron
Parr Shaker Hydrogenator
Slightly off topic, but it's an auction for a Parr temperature controller and allegedly a 4521 react ...
21-2-2009 at 03:49
by: Sauron
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
Also notice that while TCCA contains three carbonyl oxygens, TCT does not. TCT contains no oxygen.
...
21-2-2009 at 01:24
by: Sauron
Another "Two-for" Reaction CCl4 + PSCl3
I fought my way through the German of that article. The gist is:

PCl5 only reacts with CS2 at tem ...
21-2-2009 at 00:33
by: Sauron
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
I am really getting tired of having to repeat myself but let's try one more time:

Trichloro-s-tri ...
21-2-2009 at 00:03
by: Sauron
Parr Shaker Hydrogenator
Try Waters Edge Surplus in Google.

http://watersedgesurplus.com/index.aspx

I am still on their ...
20-2-2009 at 20:17
by: Sauron
PBr3 -> PCl3 "New" Old Method
I just downloaded the classic 63 page Baudrimont paper from Ann.Chim.Phys. (1864) so frequently cite ...
20-2-2009 at 11:52
by: Sauron
Parr Shaker Hydrogenator
Actually the vendor IS still in business, just under another name, This is the 4th name change in th ...
20-2-2009 at 11:45
by: Sauron
PBr3 -> PCl3 "New" Old Method
Gladstone does say that the relative affinity for P of the halogens is Cl>Br>I and yes he does ...
20-2-2009 at 08:31
by: Sauron
Another "Two-for" Reaction CCl4 + PSCl3
A related paper from Annalen describes the parallel reaction

CS2 + 2 SbCl5 -> CCl4 + 2 SbCl3 + ...
20-2-2009 at 05:28
by: Sauron
How to Make a Fume Hood
In a residential environment, by which I mean suburbis, you need not only a hood but a good scrubber ...
20-2-2009 at 03:13
by: Sauron
PBr3 -> PCl3 "New" Old Method
Thanks. There is also a prep in "Synthetic Inorganic Chemistry" in the forum library, employing 25 g ...
20-2-2009 at 02:20
by: Sauron
PBr3 -> PCl3 "New" Old Method
I spent last night and this morning trying the usual sources for information on Gg2Cl2 prep beyong w ...
19-2-2009 at 23:51
by: Sauron
How to Make a Fume Hood
My advice is, if you can't afford a new hood, buy a second hand one. LOTS of those not only on eBay ...
19-2-2009 at 22:18
by: Sauron
The Wang-Hendrickson Synthesis
You're welcome.
19-2-2009 at 16:47
by: Sauron
PBr3 -> PCl3 "New" Old Method
Yes it is IE specific. The webpage with instructions specifically mentioned it would not work for Fi ...
19-2-2009 at 06:10
by: Sauron
PBr3 -> PCl3 "New" Old Method
Won't that screen dump give me everything and not just the page window?

And at screen resolution? ...
19-2-2009 at 05:11
by: Sauron
PBr3 -> PCl3 "New" Old Method
Thanks but I already learned how to get the image files, by a roundabout method.

1. Go to the boo ...
19-2-2009 at 02:35
by: Sauron
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