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Amination of tertiary alkyl halide
[rquote=279008&tid=23757&author=ctrade]Id like to synthesize neophylamine from neophyl chlor ... |
25-3-2013 at 12:15
by: Nicodem |
Diazotization safety
[rquote=278604&tid=23775&author=maxpayne]If temperature is higher than 5°C, this compund is ... |
21-3-2013 at 10:26
by: Nicodem |
Amination of tertiary alkyl halide
[rquote=278528&tid=23757&author=ctrade]I am actually starting from 2-napthyl-2-propanol. Sin ... |
21-3-2013 at 10:13
by: Nicodem |
Why is methyl benzoate more reactive to EAS bromination than m-xylene?
[rquote=278383&tid=23756&author=killswitch]A significantly greater color change was observed ... |
20-3-2013 at 08:37
by: Nicodem |
Amination of tertiary alkyl halide
[rquote=278405&tid=23757&author=ctrade]I am trying to synthesize napthyl isopropylamine from ... |
20-3-2013 at 07:59
by: Nicodem |
Boric Acid Catalysis of Amide
[rquote=278390&tid=23743&author=NuovoChem]Currently, thermal condensation to promote amide b ... |
20-3-2013 at 07:45
by: Nicodem |
1-Iodo-3,4-Methylenedioxybenzene from sesamol?
[rquote=278417&tid=23758&author=ChemistryGhost]Can 1-Iodo-3,4-Methylenedioxybenzene be obtai ... |
20-3-2013 at 07:18
by: Nicodem |
Dimethylation of tryptamine via formaldehyde/STAB
Though there are several examples in the literature of STAB being used for the dimethylation of prim ... |
14-3-2013 at 11:39
by: Nicodem |
structure of galangol (alpinol)
I made a mistake. I confused galangol with galangin which is a flavone isolated from [i]Alpinia gala ... |
13-3-2013 at 07:22
by: Nicodem |
Metal/acid reduction of benzoin
That is an interesting result. It makes me wander, if it would be possible to obtain mainly one prod ... |
12-3-2013 at 00:17
by: Nicodem |
structure of galangol (alpinol)
That is not galangol. Galangol is a flavone, check its structure! |
12-3-2013 at 00:05
by: Nicodem |
Sulfur and oil reaction
Reducing sulfur by heating it with hydrocarbons (like paraffin oil, for example) gives hydrogen sulf ... |
11-3-2013 at 23:56
by: Nicodem |
Nitroalkane syntheses ?
[rquote=277059&tid=2995&author=AndersHoveland]The reaction is very versatile.[/rquote]
Only ... |
6-3-2013 at 07:24
by: Nicodem |
Nitroalkane syntheses ?
And where do you have the reference? |
5-3-2013 at 08:50
by: Nicodem |
How can I prevent excess solvent loss?
Try to use a bleed valve to increase the distillation pressure and thus reduce losses. |
5-3-2013 at 08:47
by: Nicodem |
Aldehyde and Amide condensation?
See [url=http://pubs.acs.org/doi/abs/10.1021/ja01335a085]DOI: 10.1021/ja01335a085[/url] |
1-3-2013 at 13:50
by: Nicodem |
serine methyl ester HCl to freebase
[rquote=276497&tid=23546&author=peyotepacman]I have tried washing with Na2CO3 and then extra ... |
1-3-2013 at 12:06
by: Nicodem |
Blog Syn
It would be stupid to waste experimental time on Indian and Iranian articles like these, when their ... |
1-3-2013 at 11:37
by: Nicodem |
do you need to use a magnetic stirrer in reflux
For homogeneous reaction mixtures stirring during reflux is obsolete. For heterogeneous mixtures, st ... |
27-2-2013 at 07:35
by: Nicodem |
Hydrogenation
Confined mixtures of butane and air can explode when ignited. (seems like some posters are unaware o ... |
27-2-2013 at 07:26
by: Nicodem |
Reaction of potassium metal with ketones
https://www.sciencemadness.org/whisper/viewthread.php?tid=16568
[rquote=211563&tid=16568&au ... |
27-2-2013 at 07:21
by: Nicodem |
Acetamide Synthesis
[rquote=276014&tid=23491&author=Myeou]It was liquid so it is not acetamide. [/rquote]
It sh ... |
26-2-2013 at 09:04
by: Nicodem |
Synthesis of Vanillyl Acetamide, a capsaicin derivative
Acetic acid [i]is[/i] glacial acetic acid. "Glacial" only means that it is anhydrous enough for it t ... |
24-2-2013 at 03:43
by: Nicodem |
Voltaic cell question
[rquote=275857&tid=23474&author=Rich_Insane]What I've done in the past is that I've integrat ... |
24-2-2013 at 03:12
by: Nicodem |
Aliphatic alcohol activation orthogonal to primary amide
Transprotonations like this are equilibrium reactions - there are no [i]paths[/i] for these equilibr ... |
24-2-2013 at 02:34
by: Nicodem |
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