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Pseudo-Pentolite via ETN and TNT?
That was the main reason I chose the co-precipitation method of forming the explosive. I am sure ETN ...
4-12-2014 at 11:38
by: Hennig Brand
Pseudo-Pentolite via ETN and TNT?
Good idea Bert, I will see about doing a few tests in the next little while. Anyone else is welcome ...
4-12-2014 at 11:09
by: Hennig Brand
Pseudo-Pentolite via ETN and TNT?
Thanks Microtek, that would make the process easier as well. I now see that it actually does say in ...
4-12-2014 at 09:38
by: Hennig Brand
Pseudo-Pentolite via ETN and TNT?
I will have a look under the microscope, but I am not convinced that it is imperative that mixing be ...
3-12-2014 at 12:06
by: Hennig Brand
Best way for getting high density ?
Sounds like good suggestions. I haven't made any in several years. I made some two or three times, a ...
3-12-2014 at 02:13
by: Hennig Brand
Pseudo-Pentolite via ETN and TNT?
I always try to put the last test hole about the middle of the picture, vertically, and to the far r ...
2-12-2014 at 14:17
by: Hennig Brand
Glass Reaction Vessel Pressure Calculation
I decided to work through this, just for my own interest mostly. Assuming ideal behavior, will use R ...
2-12-2014 at 14:02
by: Hennig Brand
1.0g of Tetrolite Initiated; 7.6mm id Al, 0.30g LA (Unreinforced Configuration & ca. 6000psi Loading Pressure)
PHILOU, I think I prefer your name for this material (Tetrolite).

I am very impressed with this m ...
2-12-2014 at 12:47
by: Hennig Brand
Pseudo-Pentolite via ETN and TNT?
I believe what you are saying about TNT purity is true, but I believe there are other reasons that m ...
2-12-2014 at 10:18
by: Hennig Brand
Best way for getting high density ?
Methanol is quite toxic and its boiling point is less than 65C. I used a long piece of glass tubing ...
2-12-2014 at 05:44
by: Hennig Brand
Entolite Production
I made a small amount of 50/50 Entolite this morning by the co-precipitation method, which is briefl ...
2-12-2014 at 05:19
by: Hennig Brand
TETRYL
I got a present for you Bert. :)
1-12-2014 at 09:31
by: Hennig Brand
Trinitrotoluene preparation
Here is a graph with associated equations for TNT & DNT solubility in methanol. Several of the d ...
30-11-2014 at 07:04
by: Hennig Brand
what do you use to store iodine/bromine
Here is a how I have been storing iodine. Small, 50mL, Erlenmeyer flasks were fitted with homemade T ...
29-11-2014 at 09:15
by: Hennig Brand
Trinitrotoluene preparation
Sounds like a decent solution. The TNT did seem like it just needed a little more kick to get it int ...
28-11-2014 at 11:21
by: Hennig Brand
2.0g of TNT Initiated; 7.6mm id Al, 0.25g DDNP & 0.35g of LA (Unreinforced Configuration & ca. 6000psi Loading Pressure)
I initiated 2g of the purified TNT shown in the last picture of the last post. I used DDNP in spite ...
28-11-2014 at 09:29
by: Hennig Brand
TNT Synthesis Post Reaction Work-Up
In total there were 2 hours of DNT addition and 4 hours of heating at elevated temperature to comple ...
28-11-2014 at 08:36
by: Hennig Brand
Reaction Progression Pictures


[file]35502[/file] [file]35504[/file] [file]35506[/file] [file]35508[/file] [file]35510[/file] ...
28-11-2014 at 07:35
by: Hennig Brand
TNT Production From DNT, Oven Dried NaNO3 and 98% H2SO4
I was using the article Rosco posted earlier, from "The Journal of Industrial and Engineering Chemis ...
28-11-2014 at 07:17
by: Hennig Brand
Trinitrotoluene preparation
I am quite sure that I have successfully produced TNT using sodium nitrate and 98% sulfuric acid. I ...
27-11-2014 at 23:17
by: Hennig Brand
Trinitrotoluene preparation
Thanks for the patent.

I just wanted to add that the DNT produced still had a slight smell of mon ...
27-11-2014 at 13:23
by: Hennig Brand
Trinitrotoluene preparation
Thanks for posting the great article. I have been looking it over off and on for more than a week. : ...
26-11-2014 at 18:36
by: Hennig Brand
Post Reaction Work-up
After the three hour addition time, and two hour heating at 80C, the stirring was continued but the ...
25-11-2014 at 08:50
by: Hennig Brand
Continuation of Nitration and Color Change


[file]35398[/file] [file]35400[/file] [file]35402[/file] [file]35404[/file] [file]35406[/file] ...
25-11-2014 at 08:25
by: Hennig Brand
DNT Synthesis In One Step
I spent the last few days making some TNT and taking a lot of pictures along the way. The nitration ...
25-11-2014 at 08:17
by: Hennig Brand
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