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Diphoronepentaperoxide (DPPP)
[quote] [i]Originally posted by Hideki Matsumoto[/i]
Ok you don't beleive me...
[/quote]
... |
18-12-2004 at 18:55
by: Axt |
Diphoronepentaperoxide (DPPP)
[quote][i]Originally posted by Joeychemist[/i]
Ok, let’s just say that this primary has a VoD of ... |
18-12-2004 at 17:07
by: Axt |
Methylenediisonitramine
Solution to your problem ... make more, the copious sludgy precipitate will shrivel up when dried.
... |
18-12-2004 at 00:51
by: Axt |
PLX type explosives
Im attaching a pdf on the mechanism for which amines sensitise nitromethane. |
18-12-2004 at 00:42
by: Axt |
PLX type explosives
NM = 6210m/s in 15/16" glass tube (PATR 2700)
NM = 6350m/s (LLNL handbook)
PLX = 6165m/s in 15/16" ... |
18-12-2004 at 00:28
by: Axt |
Organic Hypochlorites
Water!
12g NaOH, 12g EtOH, 100ml water, bubble chlorine through that. It only takes a few minutes ... |
17-12-2004 at 23:09
by: Axt |
Manganese Heptoxide type reaction.
Before you go playing with your blowtorch, you do realise that Mn2O7 will detonate when heated, dont ... |
16-12-2004 at 21:03
by: Axt |
Methylenediisonitramine
I tried something else yesterday, I tried to form a salt by reacting Cu pipe directly in a mixture ... |
16-12-2004 at 20:07
by: Axt |
Halogenated Amines - the others
I havn't tried slow heating, but I have dropped it onto a hotplate, in which case it puffs off ... |
16-12-2004 at 16:25
by: Axt |
Methylenediisonitramine
Me and Rosco talked of this before, but I've only just got around to trying it, since its synthesis ... |
15-12-2004 at 21:57
by: Axt |
Pseudonitrosites
[quote][i]Originally posted by chemoleo[/i]
So essentially it looks like the reaction of the aci fo ... |
12-12-2004 at 22:24
by: Axt |
Pseudonitrosites
Using the method Mr Wack posted, seemed to go to plan, turning from yellow to red, then back to yell ... |
12-12-2004 at 09:07
by: Axt |
Pseudonitrosites
Hmmm.
Quote from US2401267 "The foregoing reactions are usually carried out by dissolving a ... |
11-12-2004 at 05:03
by: Axt |
Pseudonitrosites
Did you get its structure right Chemoleo! I think its an oxime, where you have a nitroso. Even still ... |
10-12-2004 at 20:53
by: Axt |
sublimation of CuI + I2 to get...
[quote][i]Originally posted by johnnyBbad[/i]
1Filter out the CuI precipitate as per usual
2Then a ... |
10-12-2004 at 09:22
by: Axt |
Diisonitrosoacetone
No, I havnt seen any mention of its toxicity. Its not really a nitroso (<- thats what you mean is ... |
8-12-2004 at 08:17
by: Axt |
Diisonitrosoacetone
I dont have anymore, nor hydroxylamine. But it would be interesting, the trioxime dissolved in ether ... |
7-12-2004 at 20:18
by: Axt |
Pseudonitrosites
Thanks, seems almost too easy.
Regarding the liquid product, it cannot be ignited, so I tried to ... |
7-12-2004 at 20:00
by: Axt |
Diisonitrosoacetone
You could well get a better yield with a different precedure, its only one attempt at it. Theres a ... |
6-12-2004 at 18:28
by: Axt |
Diisonitrosoacetone
I've seen no explosive properties reported for diisonitrosoacetone, but it is a precursor to a new " ... |
6-12-2004 at 07:19
by: Axt |
Pseudonitrosites
The structure is also in PATR and in Rhodium. What are the alternatives? a straight dioxime peroxide ... |
5-12-2004 at 18:09
by: Axt |
Pseudonitrosites
Sorry that pictures confusing people! Its actually NaNO2 injected with 30% H2SO4, I tried that first ... |
5-12-2004 at 06:29
by: Axt |
Pseudonitrosites
Here's a funny one. Made by the interaction of N2O3 with an unsaturated hydrocarbon. Patent US147382 ... |
5-12-2004 at 03:28
by: Axt |
Double salts of Organic Acids
Thanks for the translation 
The precipitate I recieved had no real structure to its crystals ra ... |
5-12-2004 at 02:05
by: Axt |
Double salts of Organic Acids
Ive attached a German reference for diaceto-diplumbo-bromate (lead acetato-bromate in PATR 2700). Th ... |
3-12-2004 at 16:37
by: Axt |
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