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general high-yielding one-pot procedure for the reduction of conjugated aliphatic nitro groups.
You should have included the original reference, would be way easier to look at where you got this f ... |
28-9-2020 at 16:04
by: karlos³ |
This is mandatory stuff for (amateur) chemists (Safety)
[rquote=645413&tid=156221&author=Cou]I like organic chemistry, but I don't think I'm a very ... |
28-9-2020 at 14:17
by: karlos³ |
2020 Secret Santa [tell everyone how it went]
[rquote=645375&tid=156198&author=woelen]Matching me with someone in the EU also would be nic ... |
28-9-2020 at 11:03
by: karlos³ |
2020 Secret Santa [tell everyone how it went]
[rquote=645198&tid=156198&author=nzlostpass][rquote=645066&tid=156198&author=karlos ... |
26-9-2020 at 03:11
by: karlos³ |
Preparation of n-butylamine(consult)
Although I've seen an example of the preparation of ethylamine with the delepine once, back on versu ... |
23-9-2020 at 13:24
by: karlos³ |
Is there a way to avoid carcinogen exposure at home?
I am actually quite satisfied with the yields I've gotten without catalytic DMF or DBU.
It might ma ... |
23-9-2020 at 13:10
by: karlos³ |
Preparation of n-butylamine(consult)
You have to ask one of the moderators for access to the reference section, just like you have to for ... |
23-9-2020 at 11:21
by: karlos³ |
Is there a way to avoid carcinogen exposure at home?
Then its all fine if you use only the (COCl)2 as it is without a catalyst.
The reaction is driven f ... |
23-9-2020 at 11:10
by: karlos³ |
Is there a way to avoid carcinogen exposure at home?
Not a real answer on your question, though what I'm saying might make your issue obsolete.
I assume ... |
23-9-2020 at 11:07
by: karlos³ |
Preparation of n-butylamine(consult)
You want to stick to the gabriel synthesis?
Then it is best if you forget about stupid phthalimide ... |
23-9-2020 at 08:29
by: karlos³ |
2020 Secret Santa [tell everyone how it went]
Count me in!
I hope I get someone I can make happy with what I can give away 
By the way, is t ... |
23-9-2020 at 08:21
by: karlos³ |
Theoretical Reaction Scheme for the Synthesis of Diethyltryptamine
I would highly suggest that you use a different base for the ethylation.
Use some organic base, tri ... |
23-9-2020 at 07:58
by: karlos³ |
How would you continue a chemistry hobby, if you had to move into an unsuitable living space?
Dude, it might be helpful if I tell you that, although I am always working at small scales, that I m ... |
22-9-2020 at 10:33
by: karlos³ |
Sodium borohydride lump
Its definitely still active, no worries.
Borohydride likes to clump together but that doesn't dimin ... |
18-9-2020 at 17:15
by: karlos³ |
Most toxic compound OTC?
[rquote=644748&tid=155450&author=garphield]in terms of what has the lowest ld50 definitely a ... |
17-9-2020 at 17:52
by: karlos³ |
any recommendations for a gas chromatograph machine?
I tell that one ami friend tomorrow if he wants to earn a buck with your analytical work.
He just s ... |
14-9-2020 at 14:08
by: karlos³ |
The Short Questions Thread (4)
[rquote=644515&tid=25055&author=paulll]Has anybody ever heard of such a thing as a spring-lo ... |
12-9-2020 at 22:42
by: karlos³ |
Collection of bromine preps
A good choice that I used for in-situ chlorine preparation for N-chlorosaccharin that works also wel ... |
10-9-2020 at 08:03
by: karlos³ |
Blanc chloromethylation employing iodine
[rquote=644358&tid=156134&author=ArbuzToWoda]there's TheVespiary (very lovely, engaged moder ... |
8-9-2020 at 15:22
by: karlos³ |
Blanc chloromethylation employing iodine
Next time just write "omg" so I don't have to activate the translator engine 
[Edited on 7-9-2020 ... |
7-9-2020 at 12:54
by: karlos³ |
Can you only dry 3A Molecular Sieves in the Microwave? (OTC)
You can always put a beaker(or plain drinking glass) filled with water in one of the edges, not on t ... |
5-9-2020 at 15:20
by: karlos³ |
Blanc chloromethylation employing iodine
Can you get trimethyl phosphate? This works very good and is cheap and nonsuspicious.
Although I ne ... |
5-9-2020 at 13:13
by: karlos³ |
Blanc chloromethylation employing iodine
The kornblum STINKS, I wouldn't want to use any DMSO based method ever again after my own and only e ... |
5-9-2020 at 12:10
by: karlos³ |
Blanc chloromethylation employing iodine
From wikipedia: "The corresponding fluoromethylation, bromomethylation and iodomethylation reactions ... |
5-9-2020 at 11:29
by: karlos³ |
Anyone else having horrible shipping delays, or is my package lost?
Eh, don't worry, Krumpholz is twice to 3x as expensive as china and usually takes 3-4x as long to de ... |
4-9-2020 at 11:10
by: karlos³ |
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