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propiophenone from calcium propionate and calcium benzoate
I'm not more knowledgeable but accidentally came across this article. It does use an inert solvent a ...
30-11-2015 at 09:49
by: Pumukli
2-octanol
Very good!

Btw. isn't 2-octanone a useful compound? If you made it rather than the 2-octanol at f ...
27-11-2015 at 07:19
by: Pumukli
chlorination of benzene
[rquote=428705&tid=64394&author=JJay]Hmm I have a big bag of FeCl3... I bought it for someth ...
23-11-2015 at 12:04
by: Pumukli
chlorination of benzene
Depends on how do you define "special condition".

It does not require microwaving, sonication, UV ...
19-11-2015 at 11:48
by: Pumukli
chemsketch
They wanted to let you go at first but after they saw your username in SM they changed their minds. ...
8-11-2015 at 12:07
by: Pumukli
Filtration - any issue with using positive pressure instead of vacuum?
Once I tried applying a bit of pressure over a diethyl-ether containing solution/solid particles mix ...
8-11-2015 at 11:50
by: Pumukli
Very high temp (3000+ deg F) reaction vessel - uses in chem?
I don't want to ruin the party but having a high temp capable forge is one thing (which I also wish ...
7-11-2015 at 08:32
by: Pumukli
Putrescine Toxicity
I don't know the classical banana experiment because we extracted DNA from E. coli bacteria. We used ...
3-11-2015 at 00:19
by: Pumukli
Benzotriazole and derivatives
Boffis: "commercially available as a hair dye ingredient" - how should we interpret this?

Did you ...
2-11-2015 at 10:35
by: Pumukli
Putrescine Toxicity
"potentiator of other amines" seems to be a fairly good explanation on what it does.

I would say ...
31-10-2015 at 11:56
by: Pumukli
sebacic acid
What happened to the second batch? Did something go wrong and you sent it down the drain? :-)

I e ...
25-10-2015 at 23:01
by: Pumukli
Quaternary ammonium salt from triethanolamine
My two cents:

I would try something between methyl- to butyl-iodide. I mean the first four primar ...
25-10-2015 at 06:49
by: Pumukli
Bad days in the lab or with glassware?
Unfortunately thiosulphate is not very effective against bromine in the gas phase. :-)

At first I ...
24-10-2015 at 23:42
by: Pumukli
Caffeine citrate synthesis?
The deal is that some compounds have a hard time to crystallize without "seeding". You can help them ...
21-10-2015 at 22:54
by: Pumukli
Nicotine and Lobeline
Geee, I'm a bit late with the warning that nicotine was used as an insecticide too... I know you kno ...
21-10-2015 at 09:52
by: Pumukli
Home made Stands & clamps
Thanks for the tips, Aga!

I bought five 1 meter long threaded steel rods and a couple of fitting ...
21-10-2015 at 09:23
by: Pumukli
Homemade evaporation setup - is this plausible?
Once I tried freeze drying whole (small) mushrooms to preserve their natural shape as much as possib ...
21-10-2015 at 06:19
by: Pumukli
Chemistry of Terephthalic acid
Melting point of terephthalic acid is around 425 Celsius, its monoamide melts above 340 Celsius, dia ...
18-10-2015 at 03:05
by: Pumukli
Caffeine citrate synthesis?
I stand corrected, caffeine is the right spelling. The hydrate means citric acid monohydrate.
17-10-2015 at 12:52
by: Pumukli
Caffeine citrate synthesis?
You need coffeine and citric acid.
Once I mixed equal masses (5g : 5g) coffeine and citric acid hyd ...
17-10-2015 at 00:58
by: Pumukli
extraction - skip defatting
Doing defatting before extraction may have an advantage: one can remove possible emulgeators. In the ...
15-9-2015 at 11:28
by: Pumukli
What to do with tryptamine?
Tryptamine? Wasn't it tryptophane?

(Cloner, your reaction seems to be a decarboxylation attempt. ...
15-9-2015 at 11:14
by: Pumukli
Chemistry of Terephthalic acid
Whoa, sorry for the following (almost) entirely offtopic comment, but I couldn't resist:

After Bo ...
12-9-2015 at 11:05
by: Pumukli
Zinin Reaction (Aniline synthesis) Experimental test Report
I think it would.
See: https://en.wikipedia.org/wiki/Zinin_reaction
11-9-2015 at 21:29
by: Pumukli
Silvering Failures and Waste Disposal
Btw, "Ag crud" i.e. tiny Ag particles might form when the reaction is too quick and the Ag has no ti ...
11-9-2015 at 12:00
by: Pumukli
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