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PETN synth
Thanks for that, Microtek.
So slow below-boiling distillation does work.
I imagine it's very slow ... |
27-4-2008 at 10:59
by: Pulverulescent |
Acetic anhydride preparation
It'll be Autumn before I can attempt the ketene, or any other route (blasted major home-improvement ... |
27-4-2008 at 08:49
by: Pulverulescent |
Vacuum Nitric Distillation
With gas-tight connections and a good vacuum, loss of vapour sounds like the receiver isn't cold eno ... |
27-4-2008 at 06:35
by: Pulverulescent |
PETN synth
[quote][i]Originally posted by Microtek[/i]
I tested it with nitric acid that titrated as 99.5 % c ... |
27-4-2008 at 05:19
by: Pulverulescent |
Acetic anhydride preparation
And you don't actually need GAA!
Ketene and water will work if you don't mind waiting a bit longer ... |
26-4-2008 at 10:20
by: Pulverulescent |
PETN synth
Hexamine was the first compound I nitrated, and I did it in the kitchen-sink.
The reaction-vessel w ... |
26-4-2008 at 10:12
by: Pulverulescent |
PETN synth
[url=http://]http://www.svenskakemi.nu/lagerkemikalier.html[/url]
This Swedish pyro-supplier list ... |
26-4-2008 at 05:27
by: Pulverulescent |
PETN synth
PETN is fairly difficult, all things considered, VTchem!
Have you thought about cyclonite (RDX)!
... |
26-4-2008 at 03:56
by: Pulverulescent |
PETN synth
Actually, I should have described myself as someone with a strong interest in energetic materials!
... |
25-4-2008 at 13:17
by: Pulverulescent |
PETN synth
Have a look in Davis' COPAE in the site-library.
It's the best place to start.
PETN is a very powe ... |
25-4-2008 at 12:47
by: Pulverulescent |
Acetic anhydride preparation
Duh. . .I noticed the method above was discussed earlier. . . it is a long thread!
I think it was t ... |
24-4-2008 at 12:45
by: Pulverulescent |
Acetic anhydride preparation
'Sorry, I'll try another link!
][url=http://]http://v3.espacenet.com/origdoc?DB=EPODOC&IDX= ... |
24-4-2008 at 08:53
by: Pulverulescent |
Acetic anhydride preparation
[url=http://]http://v3.espacenet.com/origdoc?CY=gb&LG=en&DB=EPODOC&IDX=GB424573&DOC= ... |
24-4-2008 at 07:58
by: Pulverulescent |
nitroglycerin
[quote][i]Originally posted by gregxy[/i]
One way to purify your acids would be to add the nitrate ... |
23-4-2008 at 11:11
by: Pulverulescent |
nitroglycerin
IMO, using AN in nitro-synth could be hazardous since FGAN is often impure.
Some FGAN is made fro ... |
23-4-2008 at 06:03
by: Pulverulescent |
nitroglycerin
Pdb, I should just say I'm not insinuating any bad practise on your part.
Some accidents are inex ... |
21-4-2008 at 12:10
by: Pulverulescent |
Did you ever hear of Einstein's Refrigerator?
Yes, Shingoshi, we'd (most all) be on the list, if he were still around!
P |
21-4-2008 at 11:55
by: Pulverulescent |
Did you ever hear of Einstein's Refrigerator?
[quote][i]Originally posted by Sauron[/i]
[b]
Groves regarded him as a crackpot [/quote]
IIRC ... |
21-4-2008 at 09:32
by: Pulverulescent |
Home Chemistry Society
[quote][i]Originally posted by woelen[/i]
guests cannot even read it.
[/quote]
Will that not ma ... |
21-4-2008 at 09:17
by: Pulverulescent |
nitroglycerin
Oh, and drain-cleaner + nitrate salts will have no part in it.
The H2S04 will, hopefully, be the st ... |
21-4-2008 at 09:00
by: Pulverulescent |
nitroglycerin
I used a thermometer to mix the reactants when I made nitro and I remember the slight worry that too ... |
21-4-2008 at 08:34
by: Pulverulescent |
Liquid bomb plot demo video
The really worrying thing is---the next bomb-threat may be somewhat more sophisticated than the last ... |
20-4-2008 at 14:24
by: Pulverulescent |
Ireland
Apologies. . .
P |
19-4-2008 at 10:52
by: Pulverulescent |
Ireland
[quote][i]Originally posted by MagicJigPipe[/i]
-if they didn't harm uninvolved civilians. [/quote ... |
19-4-2008 at 06:15
by: Pulverulescent |
Ireland
[quote][i]Originally posted by MagicJigPipe[/i]
I bet Ireland is almost as bad or worse than the US ... |
19-4-2008 at 04:16
by: Pulverulescent |
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