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Gallium in an Al/Hg reduction Yes, there is a paper on this effect already. I don't have it handy, but it will work for reductions ... |
24-3-2008 at 11:21 by: Fleaker |
Sulfur trioxide from sodium hydrogen sulfate Excellent work!! This is a cheap and effective synthesis for SO3, one I will probably do at home as ... |
24-3-2008 at 10:35 by: Fleaker |
I Have Ethyl Acetate and KI I'd probably buy various things. I'd rather have NaI than KI...more bang for your buck iodine conten ... |
24-3-2008 at 10:12 by: Fleaker |
Synthesis of Sulfur Trioxide and Oleum: The persulfate method No so difficult at all vulture; heat will drive it out, and so will vacuum. |
21-3-2008 at 14:50 by: Fleaker |
Write-up on synthesis of K3CrO8, a very energetic peroxochromate While len has valid concerns, I am with Woelen and Chemoleo: small time exposures really don't add u ... |
19-3-2008 at 11:22 by: Fleaker |
Home Chemistry Society MagicJigPipe,
I don't think we should exclude professional chemists! Don't forget that quite a fe ... |
18-3-2008 at 14:17 by: Fleaker |
Adios What a pity. This is becoming intolerable. |
12-3-2008 at 09:44 by: Fleaker |
WANTED: Barium and Strontium metal I could order a kilogram of each from Alfa, but there would have to be enough interest from others o ... |
12-3-2008 at 09:35 by: Fleaker |
A attempt at Halfapint's dimethylsulfate synthesis.. I tried this reaction again last night on a larger scale using 50 mL of MeOH and excess oleum.
The ... |
11-3-2008 at 04:41 by: Fleaker |
www.totallysynthetic.com Nicodem, your posts are hilarious!
Drunkguy, thanks for the link to totalsynthesis, I hadn't seen ... |
10-3-2008 at 16:07 by: Fleaker |
Are you a real mad scientist? While I think it would be nice to live longer, I would far rather live happily.
As for what bfe ... |
8-3-2008 at 19:15 by: Fleaker |
Testing Ar-flushed apparatus for oxygen Argon is cheap enough, 20 dollars for 148 cubic feet of it at the welding store. The tank is what is ... |
8-3-2008 at 11:32 by: Fleaker |
Testing Ar-flushed apparatus for oxygen Couldn't you just vacuum distill it and save gas? |
7-3-2008 at 18:30 by: Fleaker |
bromine You'll have proof of Br2 being easy to isolate quite soon. There are ample examples already on the f ... |
7-3-2008 at 12:17 by: Fleaker |
Synthesis of 3-(p-Hydroxyphenyl)-2-Butanone "raspberry ketone" Very nice post Klute.
Many catalytic converters contain rhodium along with other amounts. I doubt ... |
6-3-2008 at 15:00 by: Fleaker |
Platinum-Tungsten Separation and Other Mystery Metals Iridium is much rarer than platinum, however, it is much less useful and much more difficult to proc ... |
6-3-2008 at 06:15 by: Fleaker |
Ruthenium metal Well that would be 100g of PtRu on what I think is some sort of trade name for carbon black.
If i ... |
6-3-2008 at 06:06 by: Fleaker |
Platinum-Tungsten Separation and Other Mystery Metals Likewise on the iridium.
I'm seconding the use of peroxide.
Reason other acids (save HF) don ... |
5-3-2008 at 17:09 by: Fleaker |
Ruthenium metal I have acquired some ruthenium metal. It is catalytic grade and is suitable for many experiments, in ... |
5-3-2008 at 10:50 by: Fleaker |
Platinum Anode Mind you it wasn't his 300 dollar a gallon plating bath, and that was back in December, about 600 do ... |
2-3-2008 at 08:38 by: Fleaker |
Platinum Anode What of it? Should we discuss some platinum anodes?
I can post a picture of some commonly seen pl ... |
1-3-2008 at 19:46 by: Fleaker |
Butyl Diglyme solvent extraction process. http://www.goldrefiningforum.com has pictures of the process and first hand experience posted up.
... |
29-2-2008 at 09:57 by: Fleaker |
Compressed Gases on the Cheap What is wrong with renting cylinders? Usually one time deposit that you get back, and then monthly f ... |
28-2-2008 at 18:28 by: Fleaker |
Acetic anhydride preparation :-) By some of us I did not mean me, I have several that I can use. Soon I'll have a very nice one a ... |
27-2-2008 at 14:13 by: Fleaker |
Acetic anhydride preparation Hm, so to make this useful one would need a good source of dry chlorine, a tube furnace, and some si ... |
27-2-2008 at 10:50 by: Fleaker |
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