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DDNP & related compounds: The über thread!
Thanks, I couldnt find the patent you are refering to. Next synth I will try just isolating the prod ... |
18-5-2015 at 14:32
by: nitro-genes |
DDNP & related compounds: The über thread!
I think we might have a winner! 
Thanks to Rosco for looking up the references on isopicramic ... |
18-5-2015 at 12:35
by: nitro-genes |
dinitrobenzofuroxan derivatives
Isopicramic acid from paracetamol seems an interesting possibility, the synthesis of N-methylated is ... |
17-5-2015 at 17:08
by: nitro-genes |
dinitrobenzofuroxan derivatives
Had some dot 4 brakefluid lying around and diammonium phosphate (yeast nutrient salt for wine making ... |
13-5-2015 at 16:32
by: nitro-genes |
dinitrobenzofuroxan derivatives
Hmm, detonation of reactants is never a good thing...
Offtopic These KC300 nitrile gloves can eas ... |
12-5-2015 at 16:29
by: nitro-genes |
dinitrobenzofuroxan derivatives
IMO, from a practical standpoint, regarding isolation of the TNA, the solvent needs to be soluble in ... |
12-5-2015 at 09:15
by: nitro-genes |
dinitrobenzofuroxan derivatives
The brown stuff is partly a condensation product of the cyanuric acid and formed picramide indeed, I ... |
12-5-2015 at 01:34
by: nitro-genes |
dinitrobenzofuroxan derivatives
The synthesis of trinitroaniline from picric acid and urea works perfectly as described. In a beaker ... |
11-5-2015 at 05:49
by: nitro-genes |
DDNP & related compounds: The über thread!
Mysterious it is, amazing to see that the postassium terazeno salt is able to make DDT in <1 mg a ... |
9-5-2015 at 03:26
by: nitro-genes |
dinitrobenzofuroxan derivatives
Thanks for the full text! Definitely going to try this on a small scale. Wanted to know how the reac ... |
9-5-2015 at 02:46
by: nitro-genes |
dinitrobenzofuroxan derivatives
Would this be useful as a very simple OTC route? Making a dough from urea and picric acid and baking ... |
8-5-2015 at 16:42
by: nitro-genes |
DDNP & related compounds: The über thread!
Tested 5 different setups this evening, using 0.1 mm steel tubing, ID 7mm, target, 1.5 mm steel plat ... |
7-5-2015 at 10:48
by: nitro-genes |
dinitrobenzofuroxan derivatives
@ Boffis, interesting compounds these benzoriazoles, what is your plan with them? :-) How are you pl ... |
3-5-2015 at 10:35
by: nitro-genes |
DDNP & related compounds: The über thread!
Great idea Rosco, one of the ideas I had was indeed to test the brisance of the potassium salt at hi ... |
3-5-2015 at 10:28
by: nitro-genes |
DDNP & related compounds: The über thread!
Order of ignition:
1. DDNP (Fluffy type, Yellow)
2. Hydrazine tetrazeno salt (Dark red)
3. Copp ... |
2-5-2015 at 12:01
by: nitro-genes |
DDNP & related compounds: The über thread!
Yes, also expected the gas was nitrogen, which lead me to believe that maybe the azido compund was f ... |
2-5-2015 at 05:09
by: nitro-genes |
dinitrobenzofuroxan derivatives
Haha, the mystery of the waxy substance that doesn't dissolve easily in water or heptane... I think ... |
2-5-2015 at 03:35
by: nitro-genes |
DDNP & related compounds: The über thread!
Was kind of frustrated with the benzofuroxan syntesis, so tried something else instead.
This see ... |
1-5-2015 at 14:14
by: nitro-genes |
dinitrobenzofuroxan derivatives
12.5 grams of NaOH were dissolved in 50 ml water and put on ice, chlorine was produced from TCCA + H ... |
1-5-2015 at 08:07
by: nitro-genes |
dinitrobenzofuroxan derivatives
A small amount of the ehtanol extracted acetaminophen was dissolved in the least amount of ethanol:w ... |
1-5-2015 at 02:25
by: nitro-genes |
dinitrobenzofuroxan derivatives
The chewing gum residues are definitely from the binder within the tablet. Any ideas for purifying a ... |
30-4-2015 at 03:33
by: nitro-genes |
dinitrobenzofuroxan derivatives
Ok, nitration went much smoother than anticipated. I did't use HNO3, I was out, and didn't want to d ... |
30-4-2015 at 01:10
by: nitro-genes |
Short question / quick answer - Thread
2 Ag+ + HCCH --> Ag2C2 + 2H+, so the HNO3 is formed by the reaction anyway, you only need a litt ... |
29-4-2015 at 12:12
by: nitro-genes |
dinitrobenzofuroxan derivatives
Thanks for looking up that reference from org syn! :-) Read the rescorcinol from paracetamol thread ... |
28-4-2015 at 03:35
by: nitro-genes |
dinitrobenzofuroxan derivatives
Many thanks for the replies, Should have been more clear in the first post: nitrites, azides, hydraz ... |
27-4-2015 at 15:26
by: nitro-genes |
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