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Can you make p-TSA in situ without too much residual H2SO4?
Ok thats really interesting.
I need some more CBD to try this out, although I thought that the delt ...
6-10-2020 at 12:09
by: karlos³
Can you make p-TSA in situ without too much residual H2SO4?
But its just lousy delta-8.
6-10-2020 at 08:33
by: karlos³
2020 Secret Santa [tell everyone how it went]
I am already very excited too, less so about the receiving though.
Hopefully I get someone who I ca ...
3-10-2020 at 13:08
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
Its the double bond besides the alpha-alkyl group which causes that you end up with an oxime always ...
2-10-2020 at 14:43
by: karlos³
Concise, Step by step Reaction Scheme for Dimethyltryptamine
Wow, then you are the first person that doesn't got (almost) solely cyclised pictet-spengler ß-carb ...
2-10-2020 at 13:10
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
In case of Zn/HCl, they reduce different.
The one goes to the amine, the other to the oxime.
2-10-2020 at 04:59
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
The issue would be that simply Al dissolving won't result in nascent hydrogen which is why the amalg ...
2-10-2020 at 01:48
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
After looking a bit around, I think that sadly your reaction probably hasn't worked as intended.
Ye ...
2-10-2020 at 00:25
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
Well, I have prepared gallium amalgam too years ago, by simply dissolving aluminium foil pieces into ...
1-10-2020 at 21:10
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
Interesting!
Gallium chloride is said to react violent with water, but it still worked as aqueous s ...
1-10-2020 at 20:33
by: karlos³
Acid Chlorides
You should still get it, who knows how long you will be able to access that?
When I got that stuff ...
1-10-2020 at 20:29
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
The nitrostyrene reduction with Al/Ga did work for your? Really?
So far, everything I've seen and r ...
1-10-2020 at 20:03
by: karlos³
Theoretical Reaction Scheme for the Synthesis of Diethyltryptamine
Its not about its "base power" here, otherwise you could use a strong anorganic base.
Why it is bas ...
1-10-2020 at 19:16
by: karlos³
YOUR inventory against Covid - Chemicals & Hardware only
For the most extreme cases?
NaClO2, to prepare a solution of ClO2 from, I guess, would be the most ...
1-10-2020 at 19:10
by: karlos³
Societal Issue around COVID (in my city anyway)
[rquote=645591&tid=156241&author=Herr Haber]change without sitting when I get home so I dont ...
1-10-2020 at 18:24
by: karlos³
Concise, Step by step Reaction Scheme for Dimethyltryptamine
I've seen it in said baking oven cleaner... but not pure, so forget about this source.
Its containe ...
1-10-2020 at 18:21
by: karlos³
Starter reagents for Organic Chemistry
[rquote=634163&tid=154951&author=Syn the Sizer][rquote=634154&tid=154951&author=Corr ...
1-10-2020 at 18:13
by: karlos³
Removing excess anime from enamine condensation?
[rquote=645588&tid=156246&author=paraguay]Was thinking that as well, I imagine the bp would ...
1-10-2020 at 17:56
by: karlos³
Concise, Step by step Reaction Scheme for Dimethyltryptamine
Also you have to keep in mind, that the decarboxylation is not that simple to get to work as a begin ...
1-10-2020 at 15:48
by: karlos³
Removing excess anime from enamine condensation?
Can you not distill the excess amine of from the enamine?
The enamine should be much higher boiling ...
1-10-2020 at 15:26
by: karlos³
Societal Issue around COVID (in my city anyway)
How many people who use their sleeve for such a thing would wipe sweat from their forehand, with the ...
1-10-2020 at 15:21
by: karlos³
Concise, Step by step Reaction Scheme for Dimethyltryptamine
Haven't you already posted this under another handle?
Yes indeed you have: http://www.sciencemadne ...
1-10-2020 at 14:23
by: karlos³
Societal Issue around COVID (in my city anyway)
[rquote=645560&tid=156241&author=macckone]You are unlikely to touch your elbow to your eyes, ...
1-10-2020 at 14:10
by: karlos³
Societal Issue around COVID (in my city anyway)
Oh boy, here we go again...

Many morticians in my country are on the verge to go bankrupt because ...
1-10-2020 at 09:52
by: karlos³
Preparation of Thalidomide
I think I actually managed to ruin the microwave glutarimide formation :o
I ran that at 20mmol subs ...
29-9-2020 at 10:23
by: karlos³
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