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Anhydrous Aluminum Chloride prepration
After some research I came to understanding: if you are an amateur chemist - you don't need the AlCl ...
2-6-2015 at 01:47
by: byko3y
Oh yeah, no reason to be paranoid...
Why should I bother about government spyingfor its citizens. US government is capable of spying all ...
1-6-2015 at 22:57
by: byko3y
Catalysts!
Yes, you are. This is a definition of catalyst.
1-6-2015 at 21:47
by: byko3y
Anhydrous Aluminum Chloride prepration
You can't use a thick one - you need to use thin, because of a possible strong overheating (from 200 ...
1-6-2015 at 04:46
by: byko3y
Anhydrous Aluminum Chloride prepration
Thanks, you have posted it the second time to me. I mentioned it in my last message. This was a setu ...
31-5-2015 at 20:17
by: byko3y
Anhydrous Aluminum Chloride prepration
I'm so funking pissed after reading about how it is easy to perform anhydrous AlCl3, while they have ...
31-5-2015 at 11:15
by: byko3y
Methyl Anthranilate -> Quinazolinone synth with microwaves
There's a lot of examples on rhodium's methaqualone page https://www.erowid.org/archive/rhodium/chem ...
30-5-2015 at 20:37
by: byko3y
P2P from recycled styrene?
Maybe because yield of Favorsii rearrangement of α-chloro-acetophenone is 25% in acetone, 50% in ac ...
30-5-2015 at 03:34
by: byko3y
Sequential Beckmann Rearrangement?
As far as I can see, Schmidt, Hofmann, Beckmann, Lossen and Tiemann rearrangements all go through th ...
30-5-2015 at 01:46
by: byko3y
P2P from recycled styrene?
I just don't want to give you a complete answer, because you need to know more about this reaction b ...
30-5-2015 at 00:39
by: byko3y
Sulphuric acid.... AGAIN
You need a real good equipment to play around with gaseous SO3 in fact. On leakage it creates a clou ...
29-5-2015 at 04:54
by: byko3y
Synthesis of Diethyl Ether
https://web.anl.gov/PCS/acsfuel/preprint%20archive/Files/49_2_Philadelphia_10-04_1181.pdf
Here's th ...
29-5-2015 at 04:32
by: byko3y
Sulphuric acid.... AGAIN
woelen, this is a hundred years old procedure from a russian chemistry book. Probably the sufuric ac ...
29-5-2015 at 03:35
by: byko3y
P2P from recycled styrene?
The answer is simple - do not use 100 years old method without modifications. Actually, Kindler modi ...
28-5-2015 at 22:04
by: byko3y
Sulphuric acid.... AGAIN
PbSO4(s) + 4HCl(conc.) = H2PbCl4(aq) + H2SO4
172 g of CaSO4 + 278 g of PbCl2, add hot 60°C water, ...
28-5-2015 at 21:52
by: byko3y
HCl from SiO2/NaCl/water/heat
My fault, I forgot to mention that my aluminium sulfate was completely dehydrated before the reactio ...
28-5-2015 at 21:12
by: byko3y
Synthesis of Diethyl Ether
xfusion44, Diethyl ether synthesis on alumina is a well studied method. There are reports in the web ...
28-5-2015 at 21:11
by: byko3y
The Strange Fate of a Person Falling into a Black Hole
IrC, you gave very few information about you actually knew and what you derrived. Most likely the au ...
28-5-2015 at 18:31
by: byko3y
Sulphuric acid.... AGAIN
woelen, it's okay, but as you might know, to make Cl2 you actually need an acid.
So it's HOCl + HCL ...
28-5-2015 at 17:11
by: byko3y
P2P from recycled styrene?
Willgerodt-Kindler with ammonia is an old well known reaction, but yes, it requires autoclave, and n ...
28-5-2015 at 17:02
by: byko3y
HCl from SiO2/NaCl/water/heat
For those who encounters this thread and will try to perform the reaction
Al2(SO4)3 + 6NaCl = 3 Na2 ...
28-5-2015 at 06:09
by: byko3y
Synthesis of Diethyl Ether
macckone, thionyl chloride dehydrates and contains acid, but EtOH + SOCl2 does nothing except of EtC ...
28-5-2015 at 05:58
by: byko3y
humanity against hydrides
You need something like of 1 eq. of LAH per 2 moles of reduced compound. In my region 1kg (26 moles) ...
28-5-2015 at 04:33
by: byko3y
Sulphuric acid.... AGAIN
I know no effective way of oxone generation. Sulfur dioxide is a reducing agent, so there's is a lot ...
28-5-2015 at 04:09
by: byko3y
The Strange Fate of a Person Falling into a Black Hole
[rquote=407007&tid=62554&author=IrC]understanding the math yields great insight into the pre ...
27-5-2015 at 23:12
by: byko3y
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