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What are some interesting uses for lithium metal
Ethylenediamine is a good start, but how about lithium acetylide ethylenediamine complex?
You can ...
2-11-2020 at 13:16
by: karlos³
Making Lithium Powder
The preparation of lithium acetylide ethylenediamine complex?
If so, very good choice!
But then ag ...
2-11-2020 at 13:06
by: karlos³
Preparation of Thalidomide
I can just say that the sheer quantity of articles about this substance is really impressively large ...
1-11-2020 at 17:18
by: karlos³
PPA extraction from proin chewable tablets
Believe it or not, simple simple oxalic acid doesn't even fume in the air! :o
1-11-2020 at 04:32
by: karlos³
Preparation of Thalidomide
I've tried a little bit around, also attempted the one-pot synthesis.

What I tried was the amidat ...
1-11-2020 at 04:14
by: karlos³
Make Sodium Hypochlorite from Calcium Hypochlorite?
[rquote=647651&tid=156418&author=teodor]It is strange that you can't use Ca(OCl)2 for the ha ...
29-10-2020 at 03:23
by: karlos³
Make Sodium Hypochlorite from Calcium Hypochlorite?
Read under 2. notes, point 1. here: http://www.orgsyn.org/demo.aspx?prep=CV2P0428
28-10-2020 at 20:27
by: karlos³
Reactions I could do with phthalic annhydride?
I made thalidomide with it, that is something I can recommend.
Its quite simply done, by reacting i ...
28-10-2020 at 17:24
by: karlos³
Oxime?!
Its the oxime.
The density is as far as I know higher than water.

If you treat it right it will ...
28-10-2020 at 12:34
by: karlos³
Preparation of dimethylamine
Don't you have DMF around,because thats so much simpler and apparently, more harmless than what you ...
27-10-2020 at 12:06
by: karlos³
Real sassafras oil from roots!
Ouch! They throw everything together in this article, speak of a rare tree which camphor isn't, of s ...
25-10-2020 at 23:08
by: karlos³
Real sassafras oil from roots!
I repeat, extracting the hydrosol is not worth it, its too bad soluble in water.

chemist1234, you ...
25-10-2020 at 11:41
by: karlos³
Real sassafras oil from roots!
[rquote=647035&tid=156352&author=zed]
I'm thinking that the world's output of Cialis, is gr ...
21-10-2020 at 05:43
by: karlos³
Real sassafras oil from roots!
The hydrosol isn't worth to go after, I know that as one of ours extracted ten kilo of roots(whole r ...
20-10-2020 at 13:59
by: karlos³
How dangerous really is picric acid?
I forgot to add the link, here is everything important mentioned, including the issue with metal con ...
19-10-2020 at 06:22
by: karlos³
How dangerous really is picric acid?
It is, for this purpose, shipped only wet, with a 50% water content or so.
But take a look at our w ...
19-10-2020 at 05:43
by: karlos³
PPA extraction from proin chewable tablets
[rquote=646718&tid=156315&author=zed]Oxalic acid is more of a worry than HCl gas. Very pois ...
18-10-2020 at 13:27
by: karlos³
PPA extraction from proin chewable tablets
Oxalate salts form prefereably well from impure solutions of an amine freebase in an acceptable puri ...
17-10-2020 at 14:28
by: karlos³
PPA extraction from proin chewable tablets
Why haven't you just taken up the freebase in DCM or better ether and precipitated it with acetonic ...
17-10-2020 at 12:52
by: karlos³
PPA extraction from proin chewable tablets
In my experience, I "prescribed" my dog racemic ephedrine made from the aminoketone and that works w ...
17-10-2020 at 11:08
by: karlos³
Powder addition?
They must have different binders in your country, I can't remember I ever was in a "add water to pow ...
10-10-2020 at 20:52
by: karlos³
Powder addition?
I thought it is weird to add water to a powder, isn't it usually almost always preferable to add a p ...
10-10-2020 at 16:38
by: karlos³
Bad days in the lab or with glassware?
[rquote=645778&tid=24908&author=beta4]Yesterday I dropped the stirbar in the sink while wash ...
9-10-2020 at 02:26
by: karlos³
TFDD 2,3,7,8-Tetrafluorodibenzodioxin
Ok, interesting.
But why had it the amine odour after the neutralisation?

Oh and please isolate ...
8-10-2020 at 13:57
by: karlos³
Reduction of helional to its amine
[rquote=645965&tid=156271&author=SaccharinSlayer157]I would be very interested to see you su ...
6-10-2020 at 19:36
by: karlos³
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