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Problems with nitroglycerin synthesis
I would use a published procedure, and follow it carefully.
Moreover, it is very important to pur ... |
14-4-2022 at 03:55
by: zed |
Conversion of APAAN(α-phenylacetoacetonitrile) into BMK
This process is well known.
Highly illegal in the jurisdictions where most of us live.
Such Ni ... |
14-4-2022 at 03:08
by: zed |
Determine H2O2 % by density
Hydrometer. |
10-4-2022 at 23:05
by: zed |
Grignard reaction products ?
You could try it. Be aware, there is a possibility of elimination. The product alcohol, could be d ... |
22-3-2022 at 17:07
by: zed |
Benzaldehyde By Reduction Of Benzoic Acid
The reduction of Benzoic Acid to Benzaldehyde is not especially difficult. But, it isn't exactly ea ... |
21-3-2022 at 21:45
by: zed |
How to filter oily sludge/slurry ?
As previously discussed; is your product temperature sensitive? If not, you might simply be able. t ... |
21-3-2022 at 21:34
by: zed |
Grignard reaction products ?
Cycloknight, sludges and emulsions can be maddeningly difficult to break.
Tell us what product yo ... |
21-3-2022 at 20:55
by: zed |
Handling of Aniline
Build some sort of a fume hood. Masks and cartridges, aren't supposed to be a substitute for a good ... |
29-1-2022 at 23:46
by: zed |
Can Platinum be used as a hydrogenation catalyst?
Oh, an easy prep is dissolving the Platinum in Aqua Regia to produce Chloroplatinic Acid.
And the ... |
29-1-2022 at 23:27
by: zed |
Blue Flame
Stabilization would be nice, if possible. Though I would proceed with caution.
Copper complexes, ... |
20-10-2021 at 01:48
by: zed |
Distilled vs Deionized Water
I hail from an area known for the crappy-dirty taste of its tap-water.
Even though it was long a ... |
20-10-2021 at 00:29
by: zed |
Plant killer
CDX Plywood. Older stock is better. Got any surplus plywood? It isn't a metal salt, but it sure ... |
20-10-2021 at 00:06
by: zed |
Types of iron for reduction
Umm. Some of the guys claim "Steel Wool" works pretty well.
These reductions are sometimes descr ... |
6-10-2021 at 00:14
by: zed |
How toxic are Beryllium compounds really ?
Beryllium is bad shit. Fifty years ago, we talked about it plenty. I had a buddy that usta build e ... |
29-9-2021 at 23:59
by: zed |
A Note on the Synthesis of 3-Nitrophthalic Acid
Crystallization is an occult practice. Damned hard to accomplish sometimes.
It is ever so he ... |
20-9-2021 at 00:37
by: zed |
Brewing Homemade Vinegar to Make Acetic Acid
I can't seem to stop it. Apples fall from my Ashmead's Kernal Apple tree, they bruise, and within a ... |
19-9-2021 at 23:50
by: zed |
5-hydroxyvanillin methylation?
Nope! My old-time buddy Dr. Death, methylated 5-hydroxy-vanillin, but he did it the straightforward ... |
8-9-2021 at 01:19
by: zed |
Sodium hydride purification (NaH)
Yup. Ventron used to sell LiAlH4 as a thick paste, mixed with mineral oil.
Eases your mind a lit ... |
5-9-2021 at 21:59
by: zed |
formation of grignard reagents in DIPE
So, you weren't able to start a Grignard in Di-isopropyl Ether. Rats! |
31-8-2021 at 21:16
by: zed |
formation of grignard reagents in DIPE
Ummm. Should work. But, some companies are promoting di-n-butyl ether as a Grignard solvent. They ... |
27-8-2021 at 16:56
by: zed |
Does evaporation release ions into the air?
Awww, I remember making NaOH solutions as a lab tech. You can't see the NaOH getting into the air, ... |
22-8-2021 at 22:57
by: zed |
Too good to be true?
Easy enough to make anhydrous AlCl3. Just capture some Cl2 in a covered flask. Drop a piece of heat ... |
22-8-2021 at 05:51
by: zed |
Too good to be true?
Awww. I read Chinese patent applications all of the time. Mostly, they are ill translated and unint ... |
22-8-2021 at 05:39
by: zed |
Help me identify this compound
You have no idea?
Do a flame test. Try to rule out inorganic.
Organic? Do a melting point de ... |
22-8-2021 at 04:59
by: zed |
Indole-3-Carbinol Oxidation
Do some library research and find a procedure. Indole isn't an Amine, and it doesn't usually react ... |
9-8-2021 at 00:36
by: zed |
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