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Reducing surface coating of CuO to metal
You might be able to get away with thermal decomposition of copper oxalate directly onto the glass i ...
28-10-2021 at 08:59
by: walruslover69
Synthesis of Pigments For Oil Paints
there are a lot of oxides that make white paint, most notably TiO2, ZnO. Iron oxides can make red or ...
28-10-2021 at 08:52
by: walruslover69
Soluble Caffeine
caffeine citrate is a very water solution caffeine compound commercially available as powder and sol ...
28-10-2021 at 05:04
by: walruslover69
Reducing surface coating of CuO to metal
why do you need to reduce the oxide to the metal instead of just starting with pure metal? does the ...
27-10-2021 at 15:21
by: walruslover69
Some experiments with cyanate ion
Do you have any insights into if the complexes are pure cyanates, or mixed aqua cyanates?

It woul ...
23-10-2021 at 08:29
by: walruslover69
Making Sodium Cyanide
The urea will just thermally decompose. I believe it starts around 100C There is no way it would be ...
22-10-2021 at 14:59
by: walruslover69
Making Sodium Cyanide
I didn't see that It was only a catalytic amount of iron and carbon. Makes sense that the iron would ...
22-10-2021 at 07:59
by: walruslover69
Making Sodium Cyanide
I have carried out a similar procedure by nurdrage with success a long time ago. Carbon does the red ...
21-10-2021 at 17:35
by: walruslover69
CBD solubility in organic solvents
I have come across most of these sources regarding the solubility. I think I will end up conducting ...
11-10-2021 at 11:34
by: walruslover69
Preparation of NaH from sodium metal.
Monoamine - is it possible that the brown/black goop formed during the reaction in THF could be due ...
3-10-2021 at 08:04
by: walruslover69
Non-polar chromaphores
I have used ferrocene and acetylferrocene while TA'ing like Dr.Bob said. We got great separation wit ...
30-9-2021 at 07:11
by: walruslover69
CBD solubility in organic solvents
I have started working on how to make the CBD isolation and purification process more efficient. My ...
29-9-2021 at 08:01
by: walruslover69
Help with solvent extraction and TLC of 5 hydroxymethyl furfural
if you have a good vacuum pump, you could leave it under vacuum for a few hours or overnight, most o ...
26-7-2021 at 11:16
by: walruslover69
How to effect a separation of two nearly identical cholesterols/steroids
Could you provide some of the solubility data regarding the two steroids? Looking at the structure r ...
26-7-2021 at 08:48
by: walruslover69
Pyridine hydrogenation - methods?
Would the reduction of pyridine to piperidine be possible with aluminum?

I have seen some posts ...
14-5-2021 at 08:28
by: walruslover69
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I think the presence of a large proportion of the ketimine is unlikely. I have done the precipitatio ...
9-4-2021 at 05:20
by: walruslover69
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
That's a really interesting short paper. I have tried using aqueous acid extraction with acetic acid ...
3-4-2021 at 08:10
by: walruslover69
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I apologize for the separate topic, I know there are already a lot of tryptophan decarboxylation thr ...
2-4-2021 at 10:37
by: walruslover69
Preparation of Hünig's base (diisopropylethylamine)
Just wanted to give an update on this old procedure.

I used scr0t's 49.3g (488mmol) DIPA and 3 ...
21-9-2020 at 05:16
by: walruslover69
Alternative reducing agent to LAH Lithium aluminum hydride
Red-al definetly sounds like something I will look into and potentially try. especially considering ...
12-8-2020 at 09:44
by: walruslover69
Synthesis, storage of sodium ethoxide
I have only ever synthesized it from sodium metal and ethanol and then pulled a vacuum to remove exc ...
12-8-2020 at 05:01
by: walruslover69
Alternative reducing agent to LAH Lithium aluminum hydride
Not necessarily an amateur/home chemistry but I was wondering if there were any alternative reagents ...
12-8-2020 at 04:40
by: walruslover69
Strange separation of layers
are you saying you did a purely aqueous extraction and ended up with 2 separate layers? No organic s ...
1-1-2020 at 08:01
by: walruslover69
Yellowing of Sodium Methoxide
I didn't have any problems making NaOEt from sodium and ethanol, but I found making Sodium hexanoxid ...
14-12-2019 at 14:04
by: walruslover69
Yellowing of Sodium Methoxide
Here is the absorbance and Fluorescence of Sodium Ethoxide. The PL was taken at 330,360,380,400,420, ...
14-12-2019 at 11:19
by: walruslover69
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