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terephthaloyl chloride synthesis (procedure)
[quote]
As of today I know no easily accessible and safe method for making dicarboxyl dichloride - ... |
9-2-2018 at 03:59
by: subskune |
terephthaloyl chloride synthesis (procedure)
[quote]
then the water can be distilled off as it forms, leaving the acid and ester in the distilla ... |
7-2-2018 at 12:29
by: subskune |
terephthaloyl chloride synthesis (procedure)
Hi,
for upcoming experiments I need to make some terephthaloyl chloride. Because I want some back ... |
6-2-2018 at 12:22
by: subskune |
Magnetic stirrer hotplate free to a good home
Vosoryx, you must be really desperate to own a hotplate stirrer that you even "steal" pg from your e ... |
11-9-2017 at 04:14
by: subskune |
Easy Pyridine Synthesis Pt.2 - Qualitative Analysis
Hi,
I have posted a thread about an easy way to massproduction of pyridine a month ago or so but is ... |
23-8-2017 at 01:30
by: subskune |
Magnetic stirrer hotplate free to a good home
Yeah, I can understand, ammonia sucks. Thats why I used an acid trap. This avoided any ammonia smell ... |
12-8-2017 at 03:02
by: subskune |
Magnetic stirrer hotplate free to a good home
honestly, that is looking way better the density og pg is 1.06 so you are in between which serms to ... |
11-8-2017 at 08:36
by: subskune |
formaldehyde from urea?
maybe its just ammonia maybe an amine from the ton of other ingredients in pee or maybe its really f ... |
6-8-2017 at 00:10
by: subskune |
formaldehyde from urea?
from pee that is really not an efficient way if so use fertilizer that is even cheaper than the wate ... |
5-8-2017 at 00:29
by: subskune |
Preparation of aluminium triethoxide without mercury?
yeah melgars approach definitely seems better ad faster because of the larger surface area. if i do ... |
2-8-2017 at 12:03
by: subskune |
Preparation of aluminium triethoxide without mercury?
at least with isopropanol and commercial aluminum foil + small amount of iodine I was able to make ... |
2-8-2017 at 05:57
by: subskune |
Can I use any silicone grease from the hardware store as vacuum grease?
I use cheap glycerol most times vapour pressure is < 0,1 pa thats less than my 2 stage pump can p ... |
1-8-2017 at 12:24
by: subskune |
Preparation of aluminium triethoxide without mercury?
It works but is extremely slow with aluminium foil pieces. I used 3g of iodine for 30g of aluminium ... |
1-8-2017 at 12:19
by: subskune |
What is a good first project for someone with college-level chemistry knowledge, but no lab equipment?
Some salt preciptation. You can buy some mgso4 fertilizer, naoh drain cleaner, sodium bicarbonate ba ... |
27-7-2017 at 06:26
by: subskune |
Refractories in Germany
The internet. THis might sound stupid but there are tons of sites that are located in ger. and have ... |
27-7-2017 at 01:17
by: subskune |
Magnetic stirrer hotplate free to a good home
In my case the aspirator trap worked very well. It caught all the ammonia and left me with a lot of ... |
22-7-2017 at 03:08
by: subskune |
Is it possible to make this?
It seems that you want to add a thiol to a double bond. If it was an alcohol you would add sulfuric ... |
20-7-2017 at 01:00
by: subskune |
Magnetic stirrer hotplate free to a good home
Vosoryx replied to my short report of making propylene carbonate and made me aware of this thread. M ... |
19-7-2017 at 02:27
by: subskune |
Propylene carbonate Synthesis
It might be ammonium carbonate or ammonium carbamate. However this white stuff smells like ammonia w ... |
19-7-2017 at 01:42
by: subskune |
Easy pyridine synth. found in a paper, does it work?
Reading your suggestion multiplied my interest in this synthesis. Not only because it seems to be pr ... |
12-7-2017 at 00:07
by: subskune |
Ascorbic Acid & KMnO4 As Photoinitiator
ascorbic acid is easy to oxidize. This involves plenty of radicals.
https://de.wikipedia.org/wiki/A ... |
11-7-2017 at 12:47
by: subskune |
Easy pyridine synth. found in a paper, does it work?
Thanks I somhow did oversee the link. The thing is how to get pyridine out of that now? Lets assume ... |
11-7-2017 at 10:58
by: subskune |
Easy pyridine synth. found in a paper, does it work?
@atara:
I think the Claisen condensation is a pretty simple way to acetoacetate since I have propyl ... |
11-7-2017 at 00:51
by: subskune |
Propylene carbonate Synthesis
I leaned the flask against the wall and touched it (ahhh what stupidity to lean a rfb against the wa ... |
9-7-2017 at 11:37
by: subskune |
Propylene carbonate Synthesis
Hi,
some of you may know that I am currently approaching pyridine synthesis. Unfortunately my rea ... |
9-7-2017 at 11:13
by: subskune |
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