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Advice on buying a GC/MS
after reading all the comments i think im going to get a GC/MS. What about LC/MS is that similar in ...
19-5-2020 at 03:56
by: nleslie321
Advice on buying a GC/MS
So im hoping to get a GC/MS off ebay for around $2,500 to $4,000 seen some in working condition with ...
18-5-2020 at 00:53
by: nleslie321
advice on buying a IR spec or raman
or thers this one with software and pc
https://www.ebay.com/itm/PerkinElmer-Spectrum-RX-I-FT-IR-Spe ...
1-5-2020 at 20:56
by: nleslie321
advice on buying a IR spec or raman
so i have been looking at getting an IR spectrometer second hand for under $3000 US or $6000 austral ...
1-5-2020 at 20:54
by: nleslie321
Chemicals wanted or for trade in nz
i have both the anhydrides but im in oz
28-4-2020 at 01:25
by: nleslie321
sodium borohydride
Does anyone in Australia or in a country that can send airmail still with this covid19 thing going o ...
4-4-2020 at 02:23
by: nleslie321
Deprotection of N-benzyl piperidine compound
So I finally got the debenzylation to work using 10% Pd/C in an acetic environment. Thanks for every ...
13-3-2020 at 21:21
by: nleslie321
Deprotection of N-benzyl piperidine compound
Im going to try give it a go this weekend.
26-2-2020 at 04:10
by: nleslie321
Deprotection of N-benzyl piperidine compound
Hmmm ok so if i use 5% Pd/C i should run it twice as long. I got the ammonium formate off ebay from ...
25-2-2020 at 03:58
by: nleslie321
Deprotection of N-benzyl piperidine compound
So ive got 2g of 10% Pd/C and 20g of 5% Pd/C im pretty sure the 10% Pd/C is good but i haven't teste ...
25-2-2020 at 02:16
by: nleslie321
Deprotection of N-benzyl piperidine compound
Yes i did that exact reaction you linked. The N-benzyl-4-piperidone is from sigma and other chemical ...
24-2-2020 at 21:15
by: nleslie321
Deprotection of N-benzyl piperidine compound
No i want to make some unregulated analogues not normal fentanyl.
24-2-2020 at 05:15
by: nleslie321
Deprotection of N-benzyl piperidine compound
Because im starting with N-benzyl-4-piperidone and i dont want fentanyl as the end product. I specif ...
24-2-2020 at 05:11
by: nleslie321
Deprotection of N-benzyl piperidine compound
Yes i do have access to just about anything the only restriction is money lol a lot of good stuff is ...
24-2-2020 at 01:43
by: nleslie321
Deprotection of N-benzyl piperidine compound
Sorry ive been flat out at work. Its benzyl fentanyl and im trying to make some unregulated analogue ...
24-2-2020 at 01:41
by: nleslie321
Deprotection of N-benzyl piperidine compound
I only have TLC to monitor reaction i dont have access to any equipment to test it as of yet. Im sav ...
19-2-2020 at 18:58
by: nleslie321
Boron tribromide
Did anyone get anywhere with the bromine and boron carbide at 800 C ?
I was going to try it in a 12 ...
19-2-2020 at 04:50
by: nleslie321
Deprotection of N-benzyl piperidine compound
So im having trouble with deprotection of a N-benzyl group on a piperidine based compound. Im using ...
18-2-2020 at 03:42
by: nleslie321
BBr3 synthesis
Has anyone tried the BBr3 synthesis from BF3 and AlBr3? Im wanting to try it and just wanted to know ...
2-2-2020 at 20:59
by: nleslie321
De-protection of N-Benzyl groups
I managed to complete the previous experiment. I am now trying a deprotection of a n-benzyl group at ...
2-2-2020 at 20:54
by: nleslie321
De-protection of N-Benzyl groups
Im trying to remove benzyl group attached to a piperidine based compound. I was trying to do a catal ...
15-11-2019 at 02:40
by: nleslie321
Aluminum amalgam -- is there any good reason to use it?
NaBH4 is so easy to get and cheap i pay like $18 for 100g i dont bother with the huge toxic mess of ...
31-10-2019 at 05:58
by: nleslie321
best option for analysing chemicals in home lab
So im looking to spend no more than $5000 on a system to analyse compounds both liquid and solid. Im ...
31-10-2019 at 05:38
by: nleslie321
De-protection of N-Benzyl groups
So im trying to de-protect a N-Benzyl group using 5% Pd/C and having no luck. Since reading up im se ...
30-10-2019 at 23:52
by: nleslie321
keten lamp
From memory i think it was a little more propionic anhydride than acetic anhydride via mek pyrolisis ...
27-8-2019 at 00:13
by: nleslie321
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