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Purifying of denaturated alcohol. [rquote=415816&tid=63104&author=Bot0nist]You say 3L of [b]pure[/b] ethanol... I assume you m ...	22-8-2015 at 08:49 by: dermolotov
Possible OTC, 'safe' methylating agents [rquote=415457&tid=11580&author=clearly_not_atara]Not terrifically safe, but -- silver tosyl ...	22-8-2015 at 08:43 by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories? [rquote=415838&tid=63305&author=RareEarth]What kind of Pd catalyst are you using?[/rquote] ...	22-8-2015 at 08:29 by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories? [rquote=415820&tid=63305&author=AvBaeyer]A good deal of the Buchwald-Hartwig chemistry is fr ...	13-8-2015 at 22:49 by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories? Tossing out a wild question here in hopes of answers. After two failed attempts with a Pd-catalyse ...	13-8-2015 at 15:37 by: dermolotov
Purifying of denaturated alcohol. [rquote=413568&tid=63104&author=aga]It is far simpler to brew yourself some crude ethanol an ...	13-8-2015 at 13:11 by: dermolotov
Reductive Amination I believe raney nickel is used only because of its price on the industrial level. I have never even ...	13-8-2015 at 13:06 by: dermolotov
Uses for H2WO4??? [rquote=414088&tid=63158&author=diggafromdover]Make the Tungstic Acid into a salt and ship i ...	13-8-2015 at 13:02 by: dermolotov
Bad Habits In The Lab I'm probably going to be shamed to hell and back for this but... I smoke a cigar when I do refluxes/ ...	21-4-2015 at 19:47 by: dermolotov
Bromo-methane Disposal - Quick Question Quick Question, gents. Just routinely demethylating an anisole to produce a phenol. More specifical ...	21-4-2015 at 19:28 by: dermolotov
Platinum Wire for Electrolysis [rquote=397127&tid=61786&author=cyanureeves]i can plate stuff but just cant get it to stick ...	15-3-2015 at 18:53 by: dermolotov
Synthesis of Aluminium Phenoxide [rquote=397125&tid=61808&author=gdflp]I can't answer definitively, but this thread may be of ...	15-3-2015 at 18:31 by: dermolotov
Platinum Wire for Electrolysis [rquote=397123&tid=61786&author=cyanureeves]dermolotov how similiar?have you electroplated w ...	15-3-2015 at 18:11 by: dermolotov
Synthesis of Aluminium Phenoxide Ah! Brilliant. This was the exact pdf that I found a few days ago. For some reason, I couldn't find ...	15-3-2015 at 17:55 by: dermolotov
Platinum Wire for Electrolysis [rquote=397080&tid=61786&author=jock88] Try to purchase a used Pt crucible (scrap) if you c ...	15-3-2015 at 17:45 by: dermolotov
Synthesis of Aluminium Phenoxide Addendum: I should mention that gritted aluminium is one of the biggest wastes of money if I can jus ...	15-3-2015 at 17:42 by: dermolotov
Synthesis of Aluminium Phenoxide I can't find any current methods of this synthesis at the moment. The only one came from an old manu ...	15-3-2015 at 17:34 by: dermolotov
Palladium on Carbon Hydrogenation - Working out the kinks Late time bump. things have been too cold nowadays to work in my shed. I might have discovered a new ...	15-3-2015 at 17:31 by: dermolotov
5 Ltr rbf, hotplate, other bits too! 200 quid or dollars? Overhead stirrer is bloody expensive most of the times. 200 would be great i ...	11-1-2015 at 12:22 by: dermolotov
Naoum's improved glass nitrating funnel Honestly... This just looks way too overcomplicated. I can understand why someone would want if nitr ...	10-1-2015 at 13:27 by: dermolotov
Magic! I do the same with my hotplate/stirrer (Corning PC 420) for overnight oxidation sometimes. Since it ...	10-1-2015 at 13:09 by: dermolotov
OTC Calcium Chloride - Good for Drying Yupp. This is what I recommend in lue of impure Magnesium Sulphate and others. This I have found ...	7-1-2015 at 10:43 by: dermolotov
Any one else feel good after smelling ammonia? [rquote=383875&tid=58153&author=forgottenpassword]Smelling salts are tried and teated over g ...	3-1-2015 at 15:29 by: dermolotov
Ammonia and tap water [rquote=384846&tid=59438&author=gardul]Awesomeness - Since my local store only had ammonia i ...	3-1-2015 at 15:28 by: dermolotov
Iodine from iodised salt? [rquote=383623&tid=58625&author=blogfast25] You'll form also ICl.[/rquote] Didn't know the ...	29-12-2014 at 11:52 by: dermolotov
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