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FTP Downtime
And I can provide a fast FTP for you to upload the public files if you wish to distribute them to a ...
27-2-2011 at 16:35
by: Eclectic
Charring of Lignocellulosic composites
You can make furfural from ground corncob and dilute sulfuric acid at no overpressure....it steam di ...
27-2-2011 at 15:15
by: Eclectic
Synthesis of longer chain tertiary alcohols
I found a few routes to terpineol googleing terpineol with terpin hydrate.
At least one recommended ...
27-2-2011 at 13:20
by: Eclectic
Synthesis of longer chain tertiary alcohols
Skip step 1? Just neutralize acid, remove alcohol or acetone solvent that was used to make turpen ...
27-2-2011 at 05:47
by: Eclectic
Storage of pressurized liquid SO2 in plastic containers
I'm pretty sure the "Schrader" valve is spring loaded pressure relief, but there are adapters availa ...
26-2-2011 at 19:44
by: Eclectic
Storage of pressurized liquid SO2 in plastic containers
Why the need for plastic container? What about used empty propane cylinders for low pressure gasses ...
26-2-2011 at 18:45
by: Eclectic
Vanillin Extraction from OTC Vanilla extract.
You may be able to get to vanillin from a permanginate oxidation of Euginol (oil of clove, oil of ci ...
25-2-2011 at 17:47
by: Eclectic
Make Potassium (from versuchschemie.de)
That's just if you start with limonene....Start with turpentine:

http://en.wikipedia.org/wiki/Alp ...
25-2-2011 at 07:58
by: Eclectic
Experimental Preparation of Chlorobutanol
Seems it might be advantageous to neutralize the alkali with HCl before workup.
24-2-2011 at 15:14
by: Eclectic
Make Potassium (from versuchschemie.de)
Well as a dehydrating agent maybe powdered magnalium 50:50 as it's very easy to break up? Also I ra ...
24-2-2011 at 15:07
by: Eclectic
Make Potassium (from versuchschemie.de)
I you have time, try distilling off the low boilers from the kerosene? I'd suspect at least 2/3 of ...
23-2-2011 at 16:14
by: Eclectic
Methanol from Windshield Washer Fluid
Also, unless you are using a fractionating column, the vapors are going to be coming out of the liqu ...
23-2-2011 at 02:50
by: Eclectic
garbage can chloroform
The prep is a bit easier with Clorox Ultra, especially if you can freeze it in a chest freezer to sl ...
21-2-2011 at 16:07
by: Eclectic
Dissolving germanium metal
@Blogfast: You can get germanium from Ebay as IR lenses
20-2-2011 at 13:21
by: Eclectic
Tin (II) Chloride
@Blogfast:

Could be, but I had slight excess of the Sb mud which should keep the valence at III. ...
20-2-2011 at 06:18
by: Eclectic
Tin (II) Chloride
The grey or black mud left after dissolving lead free solder in boiling muriatic acid is most likely ...
17-2-2011 at 01:34
by: Eclectic
Garage Experiments With Trichloromethane.
Experiment was retried with 2X184oz bottles 6.15% Sodium Hypochlorite.
Poured in 5 gallon plastic b ...
21-1-2011 at 08:43
by: Eclectic
What acid will dissolve copper/brass but not chromoly steel?
Ammonium nitrate and/or acetate and peroxide might attack the lead as well as the copper and brass.. ...
19-1-2011 at 23:23
by: Eclectic
Garage Experiments With Trichloromethane.
Yes, pure sodium hypochlorite solution is better. The emulsion is
chloroform and water, but it's ...
16-1-2011 at 19:34
by: Eclectic
Garage Experiments With Trichloromethane.
Freezing the bleach to a slush to avoid needing ice was the main point of
the experiment. It seem ...
16-1-2011 at 06:38
by: Eclectic
Garage Experiments With Trichloromethane.
(BUMP)

Did anyone ever figure out what the White precipitate is? I tried this with 3 gallons Clo ...
15-1-2011 at 19:18
by: Eclectic
Electrolysis of sodium chloride in acetone
Electrolizing 25% acetone/water saturated with sodium chloride might be worth trying as a means to m ...
13-1-2011 at 23:37
by: Eclectic
Ceramic chemistry ware.
No, but her is a google search that turns up more interesting links for formulating bodies using tal ...
13-1-2011 at 18:12
by: Eclectic
Ceramic chemistry ware.
yup....Cordierite is almost totally impervious to thermal stress....it's just a matter of adding eno ...
13-1-2011 at 16:50
by: Eclectic
Ceramic chemistry ware.
I think adding talc to the body to get 30-50% cordierite would help with sintering and consolidation ...
13-1-2011 at 16:18
by: Eclectic
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