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Formaldehyde bisulfite adduct preparation
Yea maybe rotovap half of the solution not crystallizing or add NaCl to make a brine to reduce the s ... |
20-12-2020 at 06:59
by: ChemichaelRXN |
AlCl3 is an alternative to SOCl2
Thanks for talking about it for me to get one. Not too familiar with titanium hydride, maybe sodium ... |
15-12-2020 at 15:49
by: ChemichaelRXN |
AlCl3 is an alternative to SOCl2
Mine are 0.6Mpa or 87psi. I guess a hot water bath would be safe enough.
I just bought one too; H ... |
14-12-2020 at 16:35
by: ChemichaelRXN |
AlCl3 is an alternative to SOCl2
Here is some more info. on TCCA reactions; https://www.organic-chemistry.org/chemicals/oxidations/tr ... |
14-12-2020 at 14:49
by: ChemichaelRXN |
2,2,7,7-tetramethyloxepane
Yea, it might just work. I recall hearing anything less than the 1,4-dibromobutane would just break ... |
13-12-2020 at 09:43
by: ChemichaelRXN |
2,2,7,7-tetramethyloxepane
Hello,
Has anyone ever performed a Grignard reaction where you are reacting two halogen groups wi ... |
13-12-2020 at 06:59
by: ChemichaelRXN |
Benzoyl chloride from benzoic acid
Ok, great, thank you for the info., I appreciate it! |
9-12-2020 at 13:04
by: ChemichaelRXN |
I need help finding the very bane of roaches existence...
You will have to experiment. You’d probably need like ten of these around the house in cabinets an ... |
9-12-2020 at 10:58
by: ChemichaelRXN |
Benzoyl chloride from benzoic acid
Here is knitting for you. Those who dare to think outside of the box always seem to get ridiculed.
... |
9-12-2020 at 09:21
by: ChemichaelRXN |
Benzoyl chloride from benzoic acid
You can distill benzoyl chloride.
I was talking about SnO2. I must have been misinformed about th ... |
9-12-2020 at 09:06
by: ChemichaelRXN |
Benzoyl chloride from benzoic acid
I am a laid back person, so you can just see how you sound...
Germanium, tin and lead oxides
For ... |
9-12-2020 at 08:03
by: ChemichaelRXN |
Benzoyl chloride from benzoic acid
What is your experience on this reaction?
With good ventilation, I was wondering what would occur ... |
8-12-2020 at 15:56
by: ChemichaelRXN |
Preparation of dimethylamine
What if you use methyl iodide in the right amount to ammonia and keep the product under 7C to have i ... |
30-10-2020 at 04:19
by: ChemichaelRXN |
Real sassafras oil from roots!
Thanks, I appreciate it. I strive to do more, but I am usually in a state of feeling miserable from ... |
29-10-2020 at 09:16
by: ChemichaelRXN |
Real sassafras oil from roots!
I dont do anything with anything scheduled, but if you were to get every last drop, Id extract the s ... |
28-10-2020 at 22:09
by: ChemichaelRXN |
Preparation of Red Selenium Gone Wrong
Thanks for the info. I notice just a slight sublimated amount in the air makes me nauseous. I must h ... |
22-10-2020 at 07:31
by: ChemichaelRXN |
Preparation of Red Selenium Gone Wrong
A little off topic, but have you noticed that selenous acid in ppm in the air makes you nauseous? I ... |
22-10-2020 at 00:55
by: ChemichaelRXN |
Real sassafras oil from roots!
MDMA is great, but it isnt worth risking your life over. There are many other compounds out there. U ... |
21-10-2020 at 08:12
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
I’ll think about it and may try it out. I was thinking of gassing the sulfurol with HCl too, but t ... |
20-10-2020 at 07:21
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
How about using Conc. HCl with addition of H2SO4? Reminds me of a nitration, but may help with repla ... |
19-10-2020 at 11:25
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
Ok excellent info, thanks! Yes I do own a chemical company, but some compounds are difficult to obta ... |
19-10-2020 at 11:20
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
Yea, I got ahead of myself and from all the little tests I did along with its odour, I didnt think t ... |
19-10-2020 at 10:45
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
Yes, I didnt update the thread to not bring back an old topic. The product was separated with brine, ... |
19-10-2020 at 10:17
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
Yea the sulfurol is quite stubborn. I though I chlorinated it to form clomethiazole before. It smell ... |
19-10-2020 at 09:09
by: ChemichaelRXN |
Ferric chloride and HCl halogenation of hydroxyl groups
Ah nevermind...the reaction didnt work. I need something stronger. It did smell like clomethiazole, ... |
19-10-2020 at 08:34
by: ChemichaelRXN |
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