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chloroacetonitrile
Well I have sodium monochloroacetate and chloroacetic acid so chloroacetamide can be made from them. ... |
4-6-2008 at 13:03
by: panziandi |
chloroacetonitrile
Vogel says that dehydration of primary amides may also be dehydrated with thionyl chloride.
2CH3 ... |
4-6-2008 at 04:34
by: panziandi |
chloroacetonitrile
Thank you for voicing concern over the hazards. I do indeed have a hood  and
the scale will be qui ... |
3-6-2008 at 09:23
by: panziandi |
chloroacetonitrile
I am looking at preparing chloroacetonitrile. Now I have looked on Orgsyn and found the preparation ... |
3-6-2008 at 07:53
by: panziandi |
Synthesis of LiAlH4 Starting from "Scratch"
This pdf is a technical bulletin on NAH it appears that the reaction rates of some reductions are hi ... |
31-5-2008 at 04:49
by: panziandi |
Sodium Metal from NaCl Reduction using Lead
[quote][i]Originally posted by 12AX7[/i]
I suppose the advantage to that over, say, a Downs cell is ... |
20-5-2008 at 05:54
by: panziandi |
Sodium Metal from NaCl Reduction using Lead
Perhaps a more practical version of this Pb/NaCl would be to electrolyse a molten sodium salt with a ... |
19-5-2008 at 23:14
by: panziandi |
Sodium Metal from NaCl Reduction using Lead
potassium carbonyl forms if the potassium vapour condenses in the presence of carbon monoxide. potss ... |
19-5-2008 at 13:14
by: panziandi |
Lithium Al Hydride quick question
My Lithium Aluminium Hydride came in pre-weighed plastic bags designed to dissolve in THF etc the ba ... |
19-5-2008 at 08:01
by: panziandi |
Deep Eutectic Solvents (OTC Ionic Liquid)
Alcoholysis of ethylene carbonate with ethanol will yield diethyl carbonate. Ethylene carbonate is c ... |
18-5-2008 at 14:11
by: panziandi |
Deep Eutectic Solvents (OTC Ionic Liquid)
I remember reading a paper about side reactions of N,N'-dialkylimidazolium based ionic liquids under ... |
18-5-2008 at 10:06
by: panziandi |
Sodium Metal from NaCl Reduction using Lead
Hey,
Sodium is soluble in lead. In fact an alloy of sodium and lead can be used as a drying agent ... |
18-5-2008 at 09:29
by: panziandi |
Sodium Metal from NaCl Reduction using Lead
You can electrolyse molten lead (II) bromide mp 367°C to recover lead (molten) and bromine (vapouri ... |
18-5-2008 at 07:20
by: panziandi |
H2S intoxication
But then wouldn't you have sulphur dioxide to contend with? Which I find quite unpleasant.  |
10-5-2008 at 08:57
by: panziandi |
Niobium pentoxide wanted
Well I had quotes given for non hazardous solids but as they were packaged in glass jars the price o ... |
10-5-2008 at 08:32
by: panziandi |
Niobium pentoxide wanted
Hey Chemsavers will send non hazardous chemicals internationally (to the UK) as I have had quotes fo ... |
9-5-2008 at 12:03
by: panziandi |
Very old Ethyl Ether
I would open the bottle.
I believe that diethyl ether stored in an airtight amber glass bottle i ... |
23-4-2008 at 07:35
by: panziandi |
Storage of pyridine?
I have noticed that there is a general similar "fishy" smell between amines but the exact odours can ... |
11-4-2008 at 12:46
by: panziandi |
UK Diisopropylethylamine?
I might have some kicking around somewhere! How much would you be looking for? |
10-4-2008 at 10:04
by: panziandi |
Rotary Evaporator
you can order from Buchi UK ltd with no hassel. Buchi glassware is hideously expensive but they will ... |
10-4-2008 at 10:01
by: panziandi |
Suppliers
To quote Microcosmicus above:
"In this respect, Fisher is worse than most other educational suppl ... |
24-2-2008 at 14:46
by: panziandi |
Latest chemical order?
dimethyl carbonate 1L
propylene carbonate 250mL
sodium monochloroacetate 250g
hexamethyldisilazan ... |
24-2-2008 at 11:12
by: panziandi |
Chromium Trioxide
I have 250g of CrO3 in a HDPE bottle and another 250g in a glass jar. The former resembles iodine to ... |
9-11-2007 at 14:29
by: panziandi |
P4O10 and P4S10 w/Oxalyl Chloride
I think the gist of it is that the phosphorus sulphide is easily obtained as its an industrial chemi ... |
25-9-2007 at 14:58
by: panziandi |
Carbon Tetrabromide
i have a prep of carbon tetrabromide. it is sourced from Experimental chemistry a laboratory manual, ... |
3-8-2007 at 18:25
by: panziandi |
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