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Synthesis of m-nitro ethylbenzoate
[align=center][size=2]Synthesis of m-nitro ethylbenzoate[/size][/align]
[b]Literature:[/b] Orgsyn ... |
28-3-2018 at 10:02
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
Seems to be a good idea.
Also, the note about not being pure product but a mixture of MeNH2 and oth ... |
28-3-2018 at 08:41
by: Pumukli |
Synthesis of m-nitro-ethylbenzoate
The ethylbenzoate saga continues.
I'm over two batches, same procedure. The second one went more ... |
20-3-2018 at 11:16
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
ChemiPharma:
I use this complicated setup because I learned (of course the hard way) that the t ... |
17-3-2018 at 23:47
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
[align=center][size=2]Making methylamine from glycine[/size]
testing a hypothetical pathway[/align] ... |
17-3-2018 at 14:05
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
Since then I tried carbylamine test on NH4Cl. I could only smell sharp ammonia stench, nothing rotti ... |
17-3-2018 at 04:16
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
Preliminary result:
We all know that preliminaries could have big mistakes, but here it goes anyw ... |
17-3-2018 at 00:33
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
That's it, the carbylamine reaction!
I'll go that way. It is quick and can be done theoretically ... |
16-3-2018 at 16:36
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
I would give it a go.
My plan is roughly: put a few NaOH beads into a mortar, put some glycine po ... |
16-3-2018 at 11:41
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
All right :-) Now I know that NH3 and MeNH2 smell the same. And I also know they are quite different ... |
16-3-2018 at 09:14
by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
"@Diball sniffed only ammonia smell instead methylamine"
Can anyone tell the difference by smell ... |
16-3-2018 at 07:43
by: Pumukli |
Borohydride
Offer closed. |
13-3-2018 at 11:50
by: Pumukli |
Carbamazepine Synthesis
You are probably over this but yes, try the original reaction at reflux temperature too! And don't f ... |
13-3-2018 at 09:28
by: Pumukli |
Ethyl benzoate synthesis
[size=2][align=center][b]Synthesis of ethyl benzoate[/b][/align][/size]
[align=center][size=2]-two ... |
12-3-2018 at 10:22
by: Pumukli |
Pretty Pictures (2)
Have you ever tried sublimating benzoic acid in a pickle's jar?
After two days 8 g benzoic acid fil ... |
10-3-2018 at 12:58
by: Pumukli |
Carbamazepine Synthesis
I understand your problem. Unexpectedly unreactive acid chloride.
I would expect at least partial h ... |
10-3-2018 at 12:16
by: Pumukli |
Experiments with Vanillin and Ethyl Vanillin Ideas
Forget DMS or any other alkylating agents under your circumstances! Do more basic stuff with less vo ... |
8-3-2018 at 13:17
by: Pumukli |
Experiments with Vanillin and Ethyl Vanillin Ideas
Condensation reactions with ketones. With simple acetone it is good, but even better with acetylacet ... |
8-3-2018 at 12:22
by: Pumukli |
Synthesis of ethylbenzoate
I finished my epic synthesis yesterday and now I'm compiling/translating the results into a Prepubli ... |
8-3-2018 at 12:01
by: Pumukli |
Borohydride
No offence taken, at all! What if you U2Ud me the address of your source? I'd rather pay less if I c ... |
5-3-2018 at 02:28
by: Pumukli |
Borohydride update
Hello Guys,
As I said I kept open the borohydride offer for a few days.
It seems that in the E ... |
3-3-2018 at 08:45
by: Pumukli |
Bumping on salt. Why?
It always intrigued me why on Earth does a distilling solvent bump when there is a fair ammount of s ... |
28-2-2018 at 13:19
by: Pumukli |
Borohydride
I came across a source of sodium-borohydride.
Downside is I have to buy at least a whole kg if I w ... |
25-2-2018 at 11:01
by: Pumukli |
Titration of HCl with sodium carbonate
Potassium hydrogen carbonate is a good primary standard so you can titrate strong acids with this co ... |
21-2-2018 at 13:26
by: Pumukli |
Removing alcohols from nonpolar solvents
Corrosive Joeseph: once I was told that unsaturated hydrocarbons are a problem source in fuels beca ... |
10-2-2018 at 11:44
by: Pumukli |
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