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DDNP & related compounds: The über thread!
Quite possibly the product consists mostly of pDDNP instead of the DDNR, although I wonder why in th ... |
23-7-2015 at 05:18
by: nitro-genes |
Perchloric acid and bismuth
It may be that only a certain strenght of perchloric acid is needed to act as an oxidizer instead of ... |
23-7-2015 at 01:33
by: nitro-genes |
Perchloric acid and bismuth
Chlorate and acid to generare chloric acid is a good idea.  Its extremely
unstable at higher conce ... |
22-7-2015 at 18:33
by: nitro-genes |
DDNP & related compounds: The über thread!
Regarding the synthesis of DDNR:
In a recent experiment I heated 3 grams of isopicramic acid with ... |
22-7-2015 at 17:51
by: nitro-genes |
DDNP & related compounds: The über thread!
First of all, thanks to Boffis and Philou for the requested hydroxylamine synthesis from nitrite. I ... |
18-7-2015 at 13:47
by: nitro-genes |
High speed cameras
In case of a nuclear event, at least you don't need external lighting. 
Speaking of light...so ... |
17-7-2015 at 15:56
by: nitro-genes |
Perchloric acid and bismuth
The superoxide crust forms very slowly under mineral oil, in which case only very small amounts of o ... |
17-7-2015 at 02:20
by: nitro-genes |
Unconventional Shaped Charges
Like this (forgive my terrible drawing skills):
So the red colour representing some 3 mm piece o ... |
16-7-2015 at 08:56
by: nitro-genes |
Perchloric acid and bismuth
Interesting, maybe bismuth is unique in being able to reduce perchloric acid to lower oxychlorites s ... |
16-7-2015 at 08:10
by: nitro-genes |
Unconventional Shaped Charges
With these charge sizes, it might also help to give the detonator a thick bottom of foam or plastic ... |
16-7-2015 at 07:48
by: nitro-genes |
DDNP & related compounds: The über thread!
Something completely different:
Would something along these lines possibly work? |
10-7-2015 at 13:59
by: nitro-genes |
Possible route to resorcinol from Tylenol / Paracetamol?
@ Boffis and Rosco:
The paper regarding nitrite mediated nitration of acetaminophen to the suppos ... |
9-7-2015 at 01:31
by: nitro-genes |
Unconventional Shaped Charges
A very interesting way of possibly making spherical ETN (PERFORM REMOTE though!!!) that I thought of ... |
7-7-2015 at 12:02
by: nitro-genes |
DDNP & related compounds: The über thread!
Great finds Rosco! Initiating power equal to lead azide for the potassium salt of DDNR sounds great, ... |
26-6-2015 at 14:23
by: nitro-genes |
DDNP & related compounds: The über thread!
1 gram of the purified isopicramic acid (IPA) was diazotized using three different methods, stirring ... |
25-6-2015 at 03:42
by: nitro-genes |
easy way to synthesis nitroglycrine
Should work, but finely powder the KNO£ before dissolving it in the sulfuric acid and make sure all ... |
24-6-2015 at 09:56
by: nitro-genes |
DDNP & related compounds: The über thread!
One curious thing I want to look into is whether an insoluble carbonate salt/adduct can be formed fr ... |
22-6-2015 at 16:52
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks, also would be interesting to see what the product will be after diazotization. Hopefully, th ... |
22-6-2015 at 13:51
by: nitro-genes |
DDNP & related compounds: The über thread!
I was thinking, maybe it doesn't need complete neutralization at all. Maybe
adding ice and a very ... |
22-6-2015 at 07:57
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks for your ideas about performing the reactions. The more I think about it, using AN for the ni ... |
20-6-2015 at 15:10
by: nitro-genes |
DDNP & related compounds: The über thread!
Yeah, sorry...you were talking about crystallizing ammonium DNAc directly from the neutralized nitra ... |
19-6-2015 at 17:16
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks for the info, the 250 ml and 2 grams isopicramic was based on this, but it certainly didn't d ... |
19-6-2015 at 12:37
by: nitro-genes |
DDNP & related compounds: The über thread!
Sounds familiar
For the solubilty test in diluted SA, it seemed a good idea to start with very ... |
19-6-2015 at 12:16
by: nitro-genes |
DDNP & related compounds: The über thread!
Yeah your right, was the colour recrystallized this way a sort of bright yellow, orange/brown or dar ... |
19-6-2015 at 06:10
by: nitro-genes |
DDNP & related compounds: The über thread!
Here a picture of 5 grams of DNAc reacting O/N at room temperature in 20 ml 68% nitric acid (left) a ... |
19-6-2015 at 04:01
by: nitro-genes |
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