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MEK peroxide or not?
Hi.

I opened yesterday jar with MEK and saw some white crust on the lid. Lid was was covered befo ...
1-7-2021 at 20:33
by: Bedlasky
Cerium trichloride from Cerium dioxide
[url]http://www.sciencemadness.org/talk/viewthread.php?tid=65869[/url]

[url]https://www.sciencema ...
27-6-2021 at 21:36
by: Bedlasky
XeF2 for making Perbromate
Tdep: I'll try to add 20% of diperiodatonickelate(IV) needed for full conversion of bromate to perbr ...
27-6-2021 at 08:11
by: Bedlasky
XeF2 for making Perbromate
What about Au2F10?

[url]https://en.wikipedia.org/wiki/Gold(V)_fluoride[/url]


[quote]
Krypto ...
26-6-2021 at 22:01
by: Bedlasky
Silver electrode amalgamated in mercury
Hi.

I often work with silver electrode amalgamated in mercury. It is used in chelatometry instead ...
26-6-2021 at 20:32
by: Bedlasky
Reaction between Potassium Bromate and sulfuric acid?
Yes. You can separate them by fractional crystallization. KBr is far more soluble than KBrO3. KBrO3 ...
26-6-2021 at 08:00
by: Bedlasky
Sodium bisulfate questions & reactions
Making sulfate salts from NaHSO4 isn't good idea. It will be hard to separate your metal sulfate fro ...
26-6-2021 at 07:22
by: Bedlasky
GC analysis
Hi.

I have access to GC, so I can offer sample analysis. If someone is interested, please messege ...
25-6-2021 at 07:43
by: Bedlasky
Preparation of NaH from sodium metal.
[rquote=662128&tid=157640&author=Monoamine][rquote=662125&tid=157640&author=rockyit9 ...
25-6-2021 at 05:34
by: Bedlasky
Preparation of NaH from sodium metal.
H+? What H+?

2Na + H2 --> 2NaH

And why do you talk about H+ as it is a gas? H+ practically ...
24-6-2021 at 11:37
by: Bedlasky
Reaction between Potassium Bromate and sulfuric acid?
[rquote=661978&tid=157622&author=MidLifeChemist]Adding concentrated H2SO4 to solid KBrO3 sou ...
24-6-2021 at 10:23
by: Bedlasky
silver permanganate AgMnO4 - is there any usage for it?
You can use it for preparation of other permanganates by double displacement with metal chloride. In ...
24-6-2021 at 10:16
by: Bedlasky
Reaction between Potassium Bromate and sulfuric acid?
If you add conc. sulfuric acid directly on to solid KBrO3, HBrO3 is formed which than decompose in t ...
20-6-2021 at 18:01
by: Bedlasky
Use of Mohr's Salt in Ferroin Preparation
Surely you can use it. Small amount of Fe(III) doesn't matter in ferroin indicator.
15-6-2021 at 12:52
by: Bedlasky
Sodium nitrite from iron oxalate and sodium nitrate
Antiswat: Carbon monoxide doesn't react with NaOH.
13-6-2021 at 08:23
by: Bedlasky
Precipitation of TACN (tetraamine copper nitrate)
[Cu(NH3)4]SO4 is often precipitated out using EtOH or MeOH. I think that this will work for nitrate ...
10-6-2021 at 07:33
by: Bedlasky
Potentiometric titrations issues
maldi-tof: Thanks for idea. My titrations were just one-time experiment, I want some data for articl ...
9-6-2021 at 02:46
by: Bedlasky
Sodium nitrite from iron oxalate and sodium nitrate
Antiswat: This procedure looks really good! I never thought about making pyrophoric iron in situ.
5-6-2021 at 11:19
by: Bedlasky
Potentiometric titrations issues
Here in CZ is slightly less humid environment than in UK, but practically similar. Good point, titra ...
5-6-2021 at 11:09
by: Bedlasky
Potentiometric titrations issues
Hi.

I did few potentiometric titrations and have some issues with potential stabilization.

Fir ...
4-6-2021 at 22:18
by: Bedlasky
worst stench
From what I read, thioacetone and carbon diselenide are quite nasty.

[url]https://en.wikipedia.or ...
28-5-2021 at 17:52
by: Bedlasky
The Royal Society’s Wholehearted Endorsement of Hobby Chemistry
[rquote=660822&tid=157518&author=Panache]Fyndium,
Everyone with a chemistry degree has demo ...
27-5-2021 at 03:38
by: Bedlasky
Orthosilicate esters from silica gel
[rquote=660650&tid=157461&author=Triflic Acid][quote]
The material is formed by heating sil ...
25-5-2021 at 05:49
by: Bedlasky
Orthosilicate esters from silica gel
[url]https://en.wikipedia.org/wiki/Silicon_disulfide[/url]
24-5-2021 at 03:30
by: Bedlasky
Cu Dendrite Salvation
Yeah, names are quite similar. However Witch-king is also one of my favorite villains :D.

[rquot ...
13-5-2021 at 23:01
by: Bedlasky
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