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Simple Route to RDX free from HMX
I'm not a swordsmith but if I were I'd put my trust in Japanese steel and learn to be a katanakaji. ...
15-1-2007 at 11:04
by: Sauron
Simple Route to RDX free from HMX
The other thing they hammered into me was not to put too much faith in 19th century chemical lit. Th ...
15-1-2007 at 10:33
by: Sauron
Simple Route to RDX free from HMX
When they taught me synthetic chemistry they gave me three rules

1. Do not trust patent procedure ...
15-1-2007 at 09:59
by: Sauron
Simple Route to RDX free from HMX
References 3 and 4 from the Org.Syn. article I cited above are now available from the Wanted Referen ...
15-1-2007 at 09:36
by: Sauron
H-NMR of benzoyl pyridine
One problem with those Aldrich spectra is that the filename is not meaningful, as such just a code n ...
15-1-2007 at 09:21
by: Sauron
Simple Route to RDX free from HMX
Not my intention to be dismissive of anything; nor to claim any superiority; and certainly not to po ...
15-1-2007 at 09:14
by: Sauron
Fastest Acting Poisons
Ricin is vastly overrated. Three of the five who were poisoned with the infamous ricin umbrella and ...
15-1-2007 at 09:04
by: Sauron
Fastest Acting Poisons
None here will get anywhere near polonium-210 unless you work for the Russian FSS or in their space ...
15-1-2007 at 08:55
by: Sauron
Simple Route to RDX free from HMX
But propionitrile is not what you want, to get to TRAT, it's acetonitrile. Common MeCN solvent. Prop ...
15-1-2007 at 08:20
by: Sauron
H-NMR of benzoyl pyridine
and finally 2-pyridinecarboxaldehyde FT-NMR from same Aldrich site:


Don't mention it. I just re ...
15-1-2007 at 04:33
by: Sauron
H-NMR of benzoyl pyridine
Here's FT-NMR of 2-acetylpyridine from same source

[Edited on 15-1-2007 by Sauron]
15-1-2007 at 04:30
by: Sauron
H-NMR of benzoyl pyridine
Don't any of the usual suspects (Aldrich, Fluka) give that away online, cf. on pages of the compound ...
15-1-2007 at 04:06
by: Sauron
Acetylate amine that has a carboxylic acid group
If you do make Ac2O I'd suggest considering the use of DMAP as acetylating catalyst, prferably DMAP ...
15-1-2007 at 03:58
by: Sauron
Simple Route to RDX free from HMX
NB to above

By readily nitrated I mean as readily nitrated as TAT.

TAT nitration usually gives ...
15-1-2007 at 03:37
by: Sauron
Simple Route to RDX free from HMX
This route eschews the use of hexamine and acetic anhydride completely.

Trioxane + MeCN = TRAT

...
15-1-2007 at 01:27
by: Sauron
cheap vacuum pump that can get down to 17 torr
@S.C.Wack, this is OT but you mentioned Cole Parmer. I have their full catalog as well as their Ency ...
14-1-2007 at 23:56
by: Sauron
cheap vacuum pump that can get down to 17 torr
I am not suggesting that anyone do what I did but rather than you build your own for a small fractio ...
14-1-2007 at 23:38
by: Sauron
cheap vacuum pump that can get down to 17 torr
If anyone is interested I can scan and put up the illustrated manual for my Eyela dual recirculating ...
14-1-2007 at 22:38
by: Sauron
cheap vacuum pump that can get down to 17 torr
And in Thailand where I am the Nalgene agent gets about $40 as they want to make a profit and the im ...
14-1-2007 at 22:29
by: Sauron
cheap vacuum pump that can get down to 17 torr
I got that KNF Neuberger PTFE diaphragm pump for $150

If you go see what the price is for a Nalge ...
14-1-2007 at 19:09
by: Sauron
Paralyzing Substance
A little scop would have had you less aware of your situation.
14-1-2007 at 18:13
by: Sauron
I need a new drug...
Get a physician's desk reference (PDR)

Open to any page.

Pick a therapeutic agent at random.
...
14-1-2007 at 18:08
by: Sauron
fermentation question
You work under clean room conditions? The same media that are used here are beloved of various commo ...
14-1-2007 at 17:59
by: Sauron
Novel route to Methylone?
Calling Dr Grignard!
14-1-2007 at 17:49
by: Sauron
Paralyzing Substance
You might also want to look into tetradotoxin, the toxic principle of the puffer fish (Japanese fugu ...
14-1-2007 at 17:31
by: Sauron
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