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Vogel. 5th edition
The 1st edition is arrived today. In a very good condition.

So, it looks like I am returning to t ...
29-7-2021 at 03:05
by: teodor
Reaction of sulfur and TCCA
I don't think the idea of high-temp synthesis of SxCly is a good idea because chlorine in S-Cl bond ...
29-7-2021 at 01:56
by: teodor
pyrosulfuryl chloride
Based on the data of SO2 solubility in SO2Cl2 (solubility data series, vol. 12) - 32% my mass or 187 ...
29-7-2021 at 00:01
by: teodor
Acetic anhydride preparation
"Upon treating sodium acetate with chlorosulfonic acid in a little acetic
anhydride there is formed ...
28-7-2021 at 23:41
by: teodor
pyrosulfuryl chloride
[rquote=663324&tid=157752&author=woelen]
I ampouled 100+% H2SO4 and SO2Cl2 together and kep ...
28-7-2021 at 04:30
by: teodor
pyrosulfuryl chloride
I wouldn't take a safety sheet as a reference for compound properties. Which is still good as a prec ...
27-7-2021 at 11:26
by: teodor
pyrosulfuryl chloride
SO3 and CCl4 is a "classical" route which any man will try to avoid of course (COCl2 is a byproduct) ...
27-7-2021 at 06:41
by: teodor
Reaction of sulfur and TCCA
ZnCl2 and FeCl3 have their melting point below sulfur, if this route would work these salts (especia ...
27-7-2021 at 02:55
by: teodor
pyrosulfuryl chloride
In the article "Über das Pyrosulfurylchlorid S2O5Cl2" Prandtl, Borinski there is an interesting equ ...
27-7-2021 at 00:46
by: teodor
pyrosulfuryl chloride
I think the pyrosulfuryl chloride S2O5Cl2 should be an interesting compound for anhydrous chemistry. ...
26-7-2021 at 04:47
by: teodor
Solubility of Copper Salts
Your memory is precious Bedlasky for anything regarding metal complexes so it should be good for oth ...
22-7-2021 at 11:09
by: teodor
Solubility of Copper Salts
[rquote=663172&tid=157733&author=Bedlasky]
Copper(II) glycinate definitely exist, Teodor ha ...
22-7-2021 at 09:55
by: teodor
Storage of 35% H2O2
Indeed, I have no problems with storing 25% H2O2 at room temperature in normal light conditions but ...
22-7-2021 at 02:04
by: teodor
Vogel. 5th edition
Vogel is so much used by me as a reference that I already prefer him in a printed form.
z-lib is a ...
21-7-2021 at 07:40
by: teodor
Leading reaction fumes out with a tube?
I think the 1 1/2'' PVC hose for above ground pools is the way to go ("pool vacuum hose"). You can b ...
19-7-2021 at 22:56
by: teodor
Leading reaction fumes out with a tube?
[rquote=663071&tid=157732&author=Fyndium]Fluoropolymers would withstand anything, but they w ...
19-7-2021 at 15:14
by: teodor
Leading reaction fumes out with a tube?
I think hoses without suction/air blowing is not a good solution because a lot of compounds (I recal ...
19-7-2021 at 09:47
by: teodor
Leading reaction fumes out with a tube?
This is a nice topic which I did a really lot experiments with.
So, my road was:

Step 1. Use all ...
19-7-2021 at 08:51
by: teodor
Different possible products of reaction of alcohol with SOCl2
OK, I found some answers to my questions here: https://sci-hub.se/https://doi.org/10.1021%2Fcr60226a ...
19-7-2021 at 07:14
by: teodor
Different possible products of reaction of alcohol with SOCl2
[rquote=663058&tid=157729&author=rockyit98]SOCl2 is used to make when you need pure product ...
19-7-2021 at 05:39
by: teodor
Different possible products of reaction of alcohol with SOCl2
I try to understand the reaction of alcohol with SOCl2. I can see that depending on conditions it wo ...
19-7-2021 at 03:19
by: teodor
Cobalt compounds
Thanks for idea of tetrachloronickelate. I've added it to my TODO list, its very interesting.

AcC ...
16-7-2021 at 01:58
by: teodor
Cobalt compounds
Thank you for the reply, Bedlasky.

To check whether it forms stable etherate I can try to boil-of ...
15-7-2021 at 01:05
by: teodor
Rare and hard to obtain chemicals for sale
I have received a new package from chemship1978, it is very fast & reliable comparing with some ...
14-7-2021 at 07:38
by: teodor
Cobalt compounds
It's amazing how fast wet anhydrous CoCl2 turns pink on contact with the air. When I opened the flas ...
14-7-2021 at 02:04
by: teodor
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