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Preparation of 2-aminophenol from Salicylic Acid
Interesting synthesis, thanks for posting!
I have a couple of questions, you write:
4- 50ml wa ... |
27-8-2015 at 08:18
by: nitro-genes |
DDNP & related compounds: The über thread!
The main thing I had in mind for the 3-amininopicric acid was KNDB, a mil spec approved replacement ... |
27-8-2015 at 04:55
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks, and no, I thought of it myself, reasoning that most metals are able to reduce nitric acid (w ... |
25-8-2015 at 07:10
by: nitro-genes |
DDNP & related compounds: The über thread!
The copper came from 2 mm thick solid eleectricity wire, cut with siccors to about 3 mm long "beads" ... |
25-8-2015 at 05:57
by: nitro-genes |
DDNP & related compounds: The über thread!
Who would have thought 
It seems isopicramic acid can be conveniently and completely OTC diazot ... |
25-8-2015 at 05:37
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
Hi Careysub,
Thanks for you suggestions. Good point, it's good to know more about the stuff that ... |
24-8-2015 at 11:24
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
Thanks for the reference, I'll include it together with the other references. 
Since pDDNP was ini ... |
24-8-2015 at 09:59
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
I thought it might be nice to put all of the p-DDNP stuff in a document, still needs some work and a ... |
24-8-2015 at 07:44
by: nitro-genes |
DDNP & related compounds: The über thread!
My bad, by refluxing in ethanol I meant keeping the solution at 40 deg C. (Boiling point of DCM), wh ... |
16-8-2015 at 17:12
by: nitro-genes |
DDNP & related compounds: The über thread!
It's not due to a colour shift from changes in pH, dinitro N-nitroso acetaminophenol is an existing ... |
16-8-2015 at 14:07
by: nitro-genes |
Moonshiners' 'Thumpers': Myth or Reality?
Apart from making 95% nitric acid, distillation is also a nice way to get rid of undrinkable wines ( ... |
16-8-2015 at 13:35
by: nitro-genes |
Unconventional Shaped Charges
One pack of straw might be enough to get most of the kinetic energy absorbed for these charge sizes ... |
14-8-2015 at 03:32
by: nitro-genes |
Unconventional Shaped Charges
Really cool to see people are trying to catch the EFP projectile. The idea of holding something in y ... |
14-8-2015 at 02:00
by: nitro-genes |
Nitrogen trichloride NCl3 production
TCCA and ammonia salt, try extremely small amounts only
[Edited on 13-8-2015 by nitro-genes] |
12-8-2015 at 17:39
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks, after having performed the nitration of acetaminophen again to update the synthesis protocol ... |
11-8-2015 at 07:31
by: nitro-genes |
Short question / quick answer - Thread
Never seen a pinkish colour for lead azide, what was the source of the potassium azide and lead nitr ... |
11-8-2015 at 05:47
by: nitro-genes |
Hydrogen Peroxide Explosives
They are indeed nice looking, reminds me of the breaking bad episode with the mercury fulminate, thi ... |
9-8-2015 at 11:01
by: nitro-genes |
DDNP & related compounds: The über thread!
Version 2.0:
[b][size=2]Synthesis of 4-amino-2,6-dinitrophenol (iso-picramic acid) from acetam ... |
8-8-2015 at 13:00
by: nitro-genes |
DDNP & related compounds: The über thread!
Seems old Rosco was right as usual regarding the solubility of the isopicramic acid sulfate after de ... |
8-8-2015 at 12:57
by: nitro-genes |
Getting rid of Nitration mix stains on my hands
Use a nail file, usually the staining is very superficial, fine sanding paper also works wonders |
8-8-2015 at 11:58
by: nitro-genes |
Short question / quick answer - Thread
Sounds like erythritol although it could be that it is a mix with other low calory sweeteners, what ... |
28-7-2015 at 21:27
by: nitro-genes |
DDNP & related compounds: The über thread!
Interesting read from "organic chemistry of explosives", it seems diazophenols are presumably formed ... |
27-7-2015 at 03:31
by: nitro-genes |
DDNP & related compounds: The über thread!
Well, after is has dried, yield was only 1.2 grams pDDNP/DDNR from 3 grams of isopicramic (made by A ... |
25-7-2015 at 03:58
by: nitro-genes |
DDNP & related compounds: The über thread!
Holy shit!!! It may turn out the nitration of isopicramic with 65% nitric acid
at elevated te ... |
24-7-2015 at 02:32
by: nitro-genes |
DDNP & related compounds: The über thread!
Most likely you are right as usual, I was hoping that somehow water content would be a contributing ... |
23-7-2015 at 15:56
by: nitro-genes |
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