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P2NP microwave crystallization problem
ohh HgI2 is more soluble in solutions of potasium or sodium iodides. this is because it forms a comp ...
28-11-2006 at 22:41
by: jon
theoretical amphetamine variants
by this compound (1-(thien-2-yl)isopropylamine) you imply thiophene substitution for benzene in say ...
28-11-2006 at 15:48
by: jon
Amino alcohol via Akabori, trial run
wash the aqueous phase with acetone? you can try it but I'll think you'll be dissapointed.
acetone ...
27-11-2006 at 12:13
by: jon
general high-yielding one-pot procedure for the reduction of conjugated aliphatic nitro groups.
potasium formate is a better hydride donor than formic acid i read some patents that the reduction c ...
28-10-2006 at 23:26
by: jon
PPA->4-MAR
more likely rapid decomposition would take place of the cyanic acids at a ph below 2 it will decompo ...
4-10-2006 at 21:14
by: jon
PPA->4-MAR
you suggest bubbling cyanic acid into the hydrochloride if you look at the reaction the lone pair on ...
4-10-2006 at 10:23
by: jon
Amphetamine from Cinnamaldehyde
the phemetazine process orginally was from 2-hydroxylethylnor-ephedrine however that was prepared, p ...
3-10-2006 at 21:10
by: jon
Why does ppa require hcl boil before a reaction?
the deal with the cyantate route is that the isomer has to be erythro and not threo which means +,- ...
3-10-2006 at 20:33
by: jon
Chemoluminescence
those glow sticks use a combination of glucose and a base (NaOH) I think.
when the stick is snapped ...
3-10-2006 at 16:28
by: jon
nitroethane from distilling nitromethane?
nitroethane is also used as a stabilizer for chlorinated hydrocarbons perchloroethylene for example. ...
3-10-2006 at 15:28
by: jon
PPA->4-MAR
cyanic acid isn't very stable it decomposes to ammonia and CO2 in water that's why the salt is added ...
3-10-2006 at 15:21
by: jon
MnO2 -> MnSO4; What is the best route?
from what I undertstand MnSO4 is used as a fertilizer just buy some and save yourself the trouble.
3-10-2006 at 15:13
by: jon
Amino alcohol via Akabori, trial run
man in that mechanism there is the tautomerizm you were talking about and the main product of the re ...
2-10-2006 at 14:55
by: jon
chloroform formation without distillation
I tried adding salt to the reaction I would do it in an ice chest with plastic bags packed with ice ...
31-1-2006 at 19:47
by: jon
THF in general synthesis.
In grignard reactions thf is it.
the reason is that oxygen in the ether forms complexes with the gr ...
21-1-2006 at 18:51
by: jon
THF in general synthesis.
THF is more prone to peroxide formation than aliphatic ethers because the lone pairs on the oxygen a ...
20-1-2006 at 20:21
by: jon
Mr. Anonymous: HgCl2 prep
aqau regia does that in one fell swoop how about HCl and conc. H2O2 does that work? I once heard of ...
20-1-2006 at 19:13
by: jon
Experimental Preparation of Chlorobutanol
has anyone messed around with clomethiazole I hear it's a superb hypnotic it's made from vitamin b-1 ...
19-1-2006 at 20:49
by: jon
possibility for THC extraction
Hexane is even better than butane it gets a pure cut of the cannabonoids you go down to office max I ...
19-1-2006 at 20:39
by: jon

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