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Methaqualone
[b]Deleted[/b] - I asked about TLC, but I see you already answered that in your reply to Pumukli. So ...
8-1-2021 at 13:24
by: SuperOxide
Polyphosphoric acid
What did you use as the source of phosphoric acid? Did you buy straight phosphoric acid, or did you ...
8-1-2021 at 08:31
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652699&tid=156836&author=zed]Short path vacuum distillation?

https://patents.goog ...
7-1-2021 at 08:22
by: SuperOxide
Polyphosphoric acid
@Benignium - Thank you for sharing this! I was looking for data on the synthesis of polyphosphoric a ...
5-1-2021 at 09:38
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652467&tid=156836&author=Tsjerk]I didn't think you added water, but in sublimations ...
3-1-2021 at 10:34
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652450&tid=156836&author=Tsjerk]The way to go is to just melt the phthalic acid (it ...
3-1-2021 at 09:08
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652401&tid=156836&author=Fyndium][...]

The filter paper should be supported with ...
2-1-2021 at 12:51
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652384&tid=156836&author=Dr.Bob]It is still used occasionally for compounds that wor ...
1-1-2021 at 18:31
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652377&tid=156836&author=valeg96]When the oven was shut off, then, workers entered t ...
1-1-2021 at 16:24
by: SuperOxide
How is medium/large scale sublimation accomplished?
[rquote=652363&tid=156836&author=valeg96]The answer is very simple... On a large scale, you ...
1-1-2021 at 14:25
by: SuperOxide
How is medium/large scale sublimation accomplished?
I just got through making ~53g of phthalic anhydride, and overall it was a pretty simple process, bu ...
1-1-2021 at 11:39
by: SuperOxide
DIY acid washed sand changed color unexpectedly
[rquote=652264&tid=156391&author=macckone]Based on the photo with the clear line, gravity se ...
31-12-2020 at 08:48
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=652267&tid=156798&author=macckone]A couple of notes:
[...]
2) formaldehyde is very ...
30-12-2020 at 17:24
by: SuperOxide
DIY acid washed sand changed color unexpectedly
[rquote=652232&tid=156391&author=VeritasC&E]
Given the many applications of pure SiO2 I ...
30-12-2020 at 09:30
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=652217&tid=156798&author=unionised]Distilling a solution of a gas can be challenging ...
29-12-2020 at 15:07
by: SuperOxide
Campa-chem original as formaldehyde source?
I purchased the 1 quart bottle today (cheaper than I thought, I was expecting like $10, it was less ...
29-12-2020 at 09:26
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=651995&tid=156798&author=UC235]You do know that formalin normally contains 10-15% me ...
25-12-2020 at 12:18
by: SuperOxide
first dean stark.
Damn, that's genius! lol. I was tempted to buy a DS apparatus, but I think your setup may suffice fo ...
25-12-2020 at 11:53
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=651961&tid=156798&author=aromaticfanatic]From a 30 second non in depth google search ...
25-12-2020 at 07:26
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=651940&tid=156798&author=aromaticfanatic]I've used this stuff to make hexamine. The ...
24-12-2020 at 18:15
by: SuperOxide
Campa-chem original as formaldehyde source?
[rquote=651940&tid=156798&author=aromaticfanatic]I've used this stuff to make hexamine. The ...
24-12-2020 at 16:36
by: SuperOxide
Campa-chem original as formaldehyde source?
The other day when I was at Walmart, out of boredom I started looking at random products that I thou ...
24-12-2020 at 09:12
by: SuperOxide
DIY acid washed sand changed color unexpectedly
[rquote=651853&tid=156391&author=MidLifeChemist]Your dedication to this project amazes me![/ ...
23-12-2020 at 11:01
by: SuperOxide
DIY acid washed sand changed color unexpectedly
[rquote=651643&tid=156391&author=macckone]If it was pure hematite it would have dissolved in ...
22-12-2020 at 14:55
by: SuperOxide
Mystery Glassware Identification Thread
Anyone know what this thingy is?
[img]https://64.media.tumblr.com/898583b11592491825e369e9407de7ca/ ...
20-12-2020 at 07:20
by: SuperOxide
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