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Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
Did you read my last few posts?
Starting from Al + EtX only, no alloy, you get quant. yield of an ... |
5-4-2009 at 03:01
by: Sauron |
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
The closest common alloy is 2024 and even closer is 2019.
Anyway no other report on reaction of ... |
4-4-2009 at 09:08
by: Sauron |
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
The angels of References appear to be pulling a work slowdown, so that paper from Liebig's Annalen h ... |
3-4-2009 at 23:09
by: Sauron |
reactions that emit radiation
Those are nuclear reactions, globey.
chief is wondering about chemical masers
Wrong sort of ra ... |
3-4-2009 at 14:36
by: Sauron |
From Ullmann's
2.3.2. Reaction of Aluminum With Alkyl Halides to Make Alkylaluminum Sesquichlorides
"Methyl, eth ... |
3-4-2009 at 00:37
by: Sauron |
Parr Shaker Hydrogenator
Since this thread is about Parr shakers, rather than making LAH, I have started a new thread about m ... |
2-4-2009 at 19:38
by: Sauron |
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
In another thread zed complained that the prep of LAH many of us have seen on Rhodium is not very sa ... |
2-4-2009 at 13:47
by: Sauron |
Need Help from the Pyrotechnics Side
It is probably time to start a thread on preparation of LAH |
2-4-2009 at 12:49
by: Sauron |
new phenethylamine?
Here it is so everyone can see what this thread is about.
That's the nice thing about having 5 ma ... |
2-4-2009 at 11:28
by: Sauron |
Need Help from the Pyrotechnics Side
Not to worry, a_bab. My aversion is to unnecessary DIY when a little legwork will turn up either th ... |
2-4-2009 at 11:21
by: Sauron |
new phenethylamine?
Just so. As I stated upthread. |
2-4-2009 at 07:51
by: Sauron |
Need Help from the Pyrotechnics Side
Perhaps, a-bab, your callowness and lack of insight (no offense intended) can be fprgiven. Pyrex may ... |
2-4-2009 at 03:41
by: Sauron |
new phenethylamine?
Damn it, you still make it from the ketone via the oxime, REDUCE that to the N-hydroxy, and O-alkyla ... |
2-4-2009 at 03:17
by: Sauron |
Parr Shaker Hydrogenator
Such devices are common for high pressure steel autoclaves but are not used on shaken or stirred gla ... |
2-4-2009 at 03:05
by: Sauron |
Need Help from the Pyrotechnics Side
Thanks. As I surmised. The melt could be done in pyrex with likely sacrifice of the flask. 30/70 is ... |
1-4-2009 at 15:30
by: Sauron |
Buying from microorganism supply companies
The echoes of the cyber door slamming shut on the Claviceps thread are still resounding, and here th ... |
1-4-2009 at 14:52
by: Sauron |
Need Help from the Pyrotechnics Side
Trialkylaluminums form etherates so ethers are undesirable as solvents.
If it were not so one cou ... |
1-4-2009 at 14:16
by: Sauron |
Parr Shaker Hydrogenator
Sorry, here are the pages from Brauer describing prep of diethylaluminum bromide and triethylaluminu ... |
1-4-2009 at 12:44
by: Sauron |
Need Help from the Pyrotechnics Side
g c, this has been an off the shelf product since the 1930s and I do not wish to turn it into a DIY ... |
1-4-2009 at 11:12
by: Sauron |
Need Help from the Pyrotechnics Side
J reckon not. *f I could do so then I could simply use a mix od Mg turnings and Al granules, couldn' ... |
1-4-2009 at 10:15
by: Sauron |
DNA's Designer Amphetamine thread
It would have been clearer just to say N-methoxyamphetamine as compared to N-methylamphetamine? (Met ... |
1-4-2009 at 05:11
by: Sauron |
Need Help from the Pyrotechnics Side
In the course of investigating the preparation of LAH from sodium aluminum hydride it came to my att ... |
1-4-2009 at 03:55
by: Sauron |
Parr Shaker Hydrogenator
De nada, it was interesting to find out.
I have no doubt that Li, Al, and H2 will combine under ... |
31-3-2009 at 21:59
by: Sauron |
Needed: Small Favor from A Member in Australia
Yeah but I dropped a house on her so all is cool now. The munchkins are having a pissup and the fly ... |
31-3-2009 at 20:37
by: Sauron |
Parr Shaker Hydrogenator
Now read the Nelson followup patent.
-- toluene preferred solvent
-- triethylaluminum catalyst ( ... |
31-3-2009 at 20:28
by: Sauron |
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