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Storage of Fuming Nitric acid
Fan? If those bottles were a woman... (zero maintenance) :P


Please though, I really want to see ...
19-6-2009 at 12:39
by: Fleaker
Iodomethane prep.
Arrhenius, good work! You will notice that your yield will go up when you scale it up. Also, that da ...
19-6-2009 at 12:37
by: Fleaker
Storage of Fuming Nitric acid
Good grief! What is wrong with storing it in a FEP bottle? They're practically made for nitric acid! ...
17-6-2009 at 12:51
by: Fleaker
Storage of Fuming Nitric acid
Saber, get one of those FEP bottles if you want to store it. You should store RFNA rather than WFNA, ...
12-6-2009 at 18:19
by: Fleaker
Time to get rid of some chlorate and perchlorate
Prices are fine.

I've got stuff off of Tim before and it was good. He also shipped responsibly ( ...
3-6-2009 at 16:04
by: Fleaker
Purifying toluene and drying ethyl iodide/iodoethane
Toluene is easy enough to dry with azeotropic distillation. After that, sodium treatment and careful ...
29-5-2009 at 07:59
by: Fleaker
Recent forum unreliability
Tried reaching the forum earlier and it was unavailable. Anyone notice any downtime around 10 AM EST ...
26-5-2009 at 06:58
by: Fleaker
what material use to lacquer beryllium?
I think iamthewaffler knows what's beryllium and what isn't. Also, if the cube were small enough to ...
26-5-2009 at 06:52
by: Fleaker
Ideas on the formation of Al2O3
Perhaps adding some big blocks or turnings to a dilute mercuric nitrate solution and leaving it outs ...
21-5-2009 at 10:25
by: Fleaker
converting 85-90% KOH to anhydrous KOH?
So then does gold have to be molten to dissolve in mercury? Sugar molten to dissolve in water?

Ob ...
19-5-2009 at 19:05
by: Fleaker
keten lamp
Copper can be used.

See this thread with pictures where I did it.
https://www.sciencemadness.o ...
19-5-2009 at 18:55
by: Fleaker
bottle for CCl4
I REALLY recommend you check out what this seller has to offer and order as many as you think you'll ...
18-5-2009 at 08:53
by: Fleaker
Here are some articles
I have already attempted the black phosphorus synthesis on numerous occasions. I had a tougher time ...
10-5-2009 at 18:55
by: Fleaker
Recent forum unreliability
Polverone,

Do you have any idea what the costs would be to upgrade the forum hosting?

7-5-2009 at 17:39
by: Fleaker
Black Phosphorus
Yep, better get it while you can! It's not that easy to make and rather bothersome to recover the ex ...
7-5-2009 at 12:57
by: Fleaker
Diamminedinitritoplatinum (Platinum P-salt)
I never said the yield was great. I suggest you check Brauer's for information on that, as I don't r ...
7-5-2009 at 12:55
by: Fleaker
Diamminedinitritoplatinum (Platinum P-salt)
I've made this one on many different occasions.

It's not all that energetic of an explosive. It d ...
27-4-2009 at 11:01
by: Fleaker
Chlorosulfonic acid
I'm curious about how the SO2 and Cl2 over finely divided platinum black at red heat works? I have a ...
10-4-2009 at 16:16
by: Fleaker
Lab Prep of Diethyl Sulfate
[rquote=150834&tid=12034&author=garage chemist]Fleaker, it's very interesting that you state ...
10-4-2009 at 15:54
by: Fleaker
Chlorosulfonic acid
Someone should put it to the test.

It would be very convenient if SO2Cl2 can be made into ClSO2OH ...
8-4-2009 at 17:05
by: Fleaker
Lab Prep of Diethyl Sulfate
@User
I didn't know that it was watched, but I would not be surprised. If it's drug related, it's ...
7-4-2009 at 12:39
by: Fleaker
Lab Prep of Diethyl Sulfate
Seeing as perhaps I'm the only one in this thread who has actually made these alkylating agents on m ...
7-4-2009 at 09:34
by: Fleaker
Need Help from the Pyrotechnics Side
Goodness gracious! This can all be done easily. Sauron can simply melt the aluminum and magnesium in ...
1-4-2009 at 13:52
by: Fleaker
Osmium tetroxide
Osmium can be had much cheaper than 100/g. Osmeth is popular for storing OsO4 for stains, although I ...
31-3-2009 at 10:11
by: Fleaker
Osmium tetroxide
Are you seriously using OsO4 for this? General rule is that if you can smell it, it's not good. It h ...
30-3-2009 at 12:37
by: Fleaker
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