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Oxidation of THF with nitric acid
Succinic acid seems more likely. It sounds as though the nitric acid chewed up THF pretty well.

...
10-2-2007 at 14:50
by: Sauron
propionyl chloride
@chemrox, the reference you are still lacking (after downloading above attachment) is Tett.Lett. 40 ...
10-2-2007 at 01:56
by: Sauron
Interesting cancer drugs?
I guess anyone who has looked into oncological therapeutics knows about 5FU (5-fluorouracil.)

Wel ...
10-2-2007 at 01:41
by: Sauron
propionyl chloride
We've posted quite a number of different articles on the forum in different threads, use Search and ...
10-2-2007 at 00:03
by: Sauron
odd vacuum pump parameters
Not particularly. Lab supply houses now are very inquisitive as they are all obliged by law to be un ...
9-2-2007 at 22:09
by: Sauron
Thermate
You need to PM MadHatter (the member here) and request access to the FTP site. You will need a good ...
9-2-2007 at 21:59
by: Sauron
Cl2 + CS2 -> four very useful compounds
If making CCl4 is your goal and you don't want to, or can't, deal with CS2 and various stinking sulf ...
9-2-2007 at 21:48
by: Sauron
Novichoks and Related 3rd/4th Gen. OP Agents
I obtained the full (25 page) DTIC document reporting on Fluorochem's preparation of FDNE via CFNM.
...
9-2-2007 at 21:05
by: Sauron
Thermate
Here's something that will enlighten.

I am removing this attachment as it is rather large and so ...
9-2-2007 at 13:52
by: Sauron
Ground glass joints - US to EU ISO adaptors?
DIN is certainly the German standard.

ISO again is not a Euro entity, it is a global NGO with ro ...
9-2-2007 at 11:52
by: Sauron
Toxic or Poisoning Substances
Phosgene oxime is inferior to some other vesicants precisely because its effects are immediate rathe ...
9-2-2007 at 11:00
by: Sauron
New Energetic Materials - Current Research
The REALLY amazing thing about that article is that some gullible reporter bought the notion that an ...
9-2-2007 at 10:10
by: Sauron
Methyliodid and funstuff do do with it
That's a very expensive reagent you are talking about. Absolutely do not throw it away, not only on ...
9-2-2007 at 09:53
by: Sauron
propionyl chloride
TCT is about $2 a Kg cheaper, but has 3 active chlorines to benzoyl chloride's 1, and does not have ...
9-2-2007 at 09:32
by: Sauron
propionyl chloride
[87-90-1]

C3Cl3N3O3

[Edited on 9-2-2007 by Sauron]
9-2-2007 at 08:42
by: Sauron
propionyl chloride
[108-77-0]

C3Cl3N3

[Edited on 9-2-2007 by Sauron]
9-2-2007 at 08:29
by: Sauron
propionyl chloride
Two different but related compounds with very different properties.

Cyanuric chloride is trichlor ...
9-2-2007 at 08:09
by: Sauron
odd vacuum pump parameters
Is this the seller of the used Gast?
9-2-2007 at 04:36
by: Sauron
propionyl chloride
Acros sells benzoyl chloride and benzoic acid for roughly same price. And it's rather cheap.

I'll ...
9-2-2007 at 03:41
by: Sauron
Cl2 + CS2 -> four very useful compounds
That might be useful for process development but if folks need CS2 as a solvent or reagent then I'd ...
9-2-2007 at 02:49
by: Sauron
propionyl chloride
You can also chlorinate benzoic acid or sodium benzoate to the benzoyl chloride with TCT alone or TC ...
9-2-2007 at 02:45
by: Sauron
Cl2 + CS2 -> four very useful compounds
Another useful and productive chlorination is that of methyl thiocyanate.

The yields from 100 g o ...
8-2-2007 at 23:23
by: Sauron
propionyl chloride
Thanks @solo. Another tool in the arsenal.

Time for a cost analysis and comparative study of the ...
8-2-2007 at 22:20
by: Sauron
Thermate
I wouldn't say "explode" but the sulfur scatters it a bit.

I don't think you need the Ba nitrate, ...
8-2-2007 at 22:07
by: Sauron
propionyl chloride
What environmental concerns might there be with CC? The byproduct is solid cyanuric acid, and that i ...
8-2-2007 at 21:19
by: Sauron
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