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Making KNO3 from ashes n earth
Interesting thing would be to have a pure culture of the bacteria producing the nitrate from nitroge ... |
17-9-2015 at 05:20
by: nitro-genes |
Making KNO3 from ashes n earth
Not exactly piss-easy, but doable 
https://www.youtube.com/watch?v=8wW5KR1pDxs
[Edited on 17-9 ... |
17-9-2015 at 02:34
by: nitro-genes |
DDNP & related compounds: The über thread!
my guess would be that the yield from mixtures containing sulfuric acid will be higher, since the pD ... |
17-9-2015 at 01:31
by: nitro-genes |
DDNP & related compounds: The über thread!
Wouldn't use the 65% nitric acid alone synthesis, it give fairly low yields, presumably since much o ... |
16-9-2015 at 09:06
by: nitro-genes |
DDNP & related compounds: The über thread!
Nice! looks like a good yield too. When it dries, you'll see it will take on a more orange colour. F ... |
16-9-2015 at 08:27
by: nitro-genes |
DDNP & related compounds: The über thread!
thanks for explaining all that philou, it's a lot to think about, I need to let it all sink in befor ... |
14-9-2015 at 12:09
by: nitro-genes |
DDNP & related compounds: The über thread!
@ Greenlight, how did the deactylation work out?  Can you take a look at your
bottle of 70% HNO3 b ... |
13-9-2015 at 15:34
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
[b]EDIT:[/b] Old file removed, and replaced with new file, containing:
- Different diazotization ... |
13-9-2015 at 07:37
by: nitro-genes |
DDNP & related compounds: The über thread!
Dissolving the precipitate again may be very difficult, you could try dissolving at 10 deg C. again, ... |
11-9-2015 at 07:21
by: nitro-genes |
DDNP & related compounds: The über thread!
Hi Greenlight,
The nitration is exceedingly fast, I think most of the dinitroacetaminophenol pres ... |
11-9-2015 at 06:23
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
Page numbers added, 1 ref changed, abstract added, hyperlinks to experimental procedures.
[file ... |
11-9-2015 at 04:06
by: nitro-genes |
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen
Thanks to Rosco, Solo, Philou and Nicodem for the references and remarks, Henning brand for providin ... |
10-9-2015 at 10:06
by: nitro-genes |
DDNP & related compounds: The über thread!
70% nitric acid means 70 grams of HNO3 per 100 grams, the molecular weight of HNO3 is 63, that means ... |
8-9-2015 at 05:47
by: nitro-genes |
DDNP & related compounds: The über thread!
Viable route to a possible iso-DDNR? What do you guys think?
Up to the reduction of 5-nitro b ... |
7-9-2015 at 03:17
by: nitro-genes |
Preparation of 2-aminophenol from Salicylic Acid
Yes, really surprised to find that the reaction described in the patent seems to work exactly as des ... |
1-9-2015 at 15:03
by: nitro-genes |
DDNP & related compounds: The über thread!
Hi Philou, thanks for this synthesis scheme, some interesting compounds, some of them never describe ... |
1-9-2015 at 14:07
by: nitro-genes |
Pretty Pictures (2)
All three would die or already have died, because mixing implies you either take out the lung, or ha ... |
31-8-2015 at 13:25
by: nitro-genes |
Pretty Pictures (2)
I AM possessed, you grammar nazi  |
31-8-2015 at 12:53
by: nitro-genes |
Pretty Pictures (2)
Some pretty cool photo's in this thread, and thanks, it was a precursor to 4-diazo 2,6 dinitrophenol ... |
31-8-2015 at 12:10
by: nitro-genes |
Preparation of 2-aminophenol from Salicylic Acid
Great find for this synthesis route, it works in high yield, even with household bleach. The plan ... |
31-8-2015 at 00:10
by: nitro-genes |
Unconventional Shaped Charges
Nice picures greenlight, was the lower one from a tulip shaped liner by chance? The mushroom shape a ... |
29-8-2015 at 07:10
by: nitro-genes |
Preparation of 2-aminophenol from Salicylic Acid
Yeah, your right, any possible phosgene would immediately hydrolyse when the solution is kept well b ... |
28-8-2015 at 17:07
by: nitro-genes |
Pretty Pictures (2)
Thin, plate like crystals of 4-amino 2,6-dinitrophenol, resembling a pure gold pigment powder when d ... |
28-8-2015 at 16:43
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks, was surprised it worked so well actually, since supposedly o-DDNP is destroyed by hot concen ... |
28-8-2015 at 16:17
by: nitro-genes |
Preparation of 2-aminophenol from Salicylic Acid
contemplating to perform this reaction, bit worried about toxicity of by-products during the synthes ... |
28-8-2015 at 05:49
by: nitro-genes |
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