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Novel route to Methylone?
what about ketonization of piperylic acid with propionic acid?
15-1-2007 at 00:32
by: jon
theoretical amphetamine variants
I seem to recall reading about someone's expirience with indanyl amphetamine they said it was'nt ver ...
10-1-2007 at 22:19
by: jon
WTF how to synthesize this?
why that looks like dihydropenisol being mixed with a-hydroxy-vaginol
10-1-2007 at 00:04
by: jon
Amino alcohol via Akabori, trial run
in the workup you did'nt give much detail as to how you worked it up and what you recovered.
if you ...
9-1-2007 at 20:49
by: jon
Reductive amination of L-PAC
here was the reference I was talking about earlier it uses ammonium formate in a CTH with zinc.
Jo ...
9-1-2007 at 18:02
by: jon
Amino alcohol via Akabori, trial run
Rhodium's website will give you a lot of data on PPA.
Tautomerism is going to happen in this reacti ...
3-1-2007 at 14:37
by: jon
Amino alcohol via Akabori, trial run
I dont' think a lewis acid will serve you, in this case the reaction depends on proton abstraction w ...
3-1-2007 at 12:46
by: jon
Several questions regarding Eugenol
refluxing in HBr should accomplish both Bromination, and demethylation, maybee more free radical add ...
2-1-2007 at 12:08
by: jon
Amino alcohol via Akabori, trial run
can you describe the colour changes did it go through the same changes to burgandy? also was there v ...
2-1-2007 at 11:02
by: jon
Dihydrocodeine O-demethylation?
maybe dehydration which is an E-1 or E-2 reaction followed by (markovnikov) addition, i dunno i just ...
2-1-2007 at 10:56
by: jon
Reductive amination of L-PAC
so organikum you think the ZnII(OH) would form a gelatinous mess making extraction next to impossibl ...
2-1-2007 at 10:32
by: jon
Reductive amination of L-PAC
what a find, you know the typical o-chem book would have you believe that slightly acidic conditions ...
31-12-2006 at 23:51
by: jon
Dihydrocodeine O-demethylation?
yes, there was a discussion on this at synthetikal.org just before they went offline it gave a refer ...
31-12-2006 at 23:33
by: jon
pentaerythritol from methanol and ethanol
PARAFORMALDEHYDE AND TRIOXANE will easilly hydrolyse in the prescence of a base there was a discussi ...
23-12-2006 at 11:59
by: jon
NaBH4/NiCl2 reduction
oh I was thinking of the intermediate in the reduction of a nitroolefin.
so what you are talkin abo ...
18-12-2006 at 22:54
by: jon
NaBH4/NiCl2 reduction
oximes of the saturated oxime or the unsaturated oxime?
17-12-2006 at 00:20
by: jon
NaBH4/NiCl2 reduction
why use nickel boride in a reductive amination in the first place?
plain NaBH4 is proven to work i ...
16-12-2006 at 12:01
by: jon
Reductive amination of L-PAC
So I can use sodium pyruvate intstead of acetaldehyde in the fermentation step?

has anyone tried ...
15-12-2006 at 23:21
by: jon
Reductive amination of L-PAC
I was thinking would a luekardt reaction work probably no huh?
what about zinc and ammonium formate ...
13-12-2006 at 23:53
by: jon
10% pallaidium on activated C
I have 20 grams of this, pm me if interested will sell at reasonable price, was going to dump it on ...
13-12-2006 at 21:40
by: jon
Amino alcohol via Akabori, trial run
it appears I stand corrected 2-amino1,2diphenylethanol is soluble as it's hydrochloride just like an ...
12-12-2006 at 05:00
by: jon
Amino alcohol via Akabori, trial run
I'd like to suggest something in the workup of ppa. PPA is a solid at room temperature and the other ...
10-12-2006 at 00:38
by: jon
theoretical amphetamine variants
I know this deviates from the spirit of (novel aromatic) substituted isopropylamines, but nicodem ha ...
5-12-2006 at 14:42
by: jon
theoretical amphetamine variants
I dunno ketones are pretty easy to characterize, without 1h-nmr or gc/ms it might be paydirt. it sur ...
2-12-2006 at 13:33
by: jon
theoretical amphetamine variants
a quick search on google yeilds many supplier's of thiophene-2-carboxaldehyde. available from ll ove ...
1-12-2006 at 22:58
by: jon
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