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Dehydration of 3-Phenyl-1-propanol
[rquote=492196&tid=13508&author=Melgar]Somehow I got confused and thought the discussion was ...
13-9-2017 at 07:28
by: Loptr
What did I make from bromoethane that smells fruity/flourescent?
Maybe floralescent?
9-9-2017 at 09:04
by: Loptr
What's your job?
Principal Software Engineer

[Edited on 17-8-2017 by Loptr]
17-8-2017 at 07:42
by: Loptr
Phenylacetonitrile from Phenylalanine
Very nice, AvBaeyer!

I am so glad to see that this was picked back up!
15-8-2017 at 06:43
by: Loptr
Gallium Hydroxide to Gallium Hydrochloride (EDIT: GaCl3:NH3 complex)
[rquote=490421&tid=76139&author=Melgar]You probably have a mix of gallium oxides, hydroxides ...
14-8-2017 at 12:01
by: Loptr
Gallium Hydroxide to Gallium Hydrochloride (EDIT: GaCl3:NH3 complex)
I am planning to redisolve this complex in conc. HCl, and then attempt to precipitate it with NaOH. ...
14-8-2017 at 05:31
by: Loptr
Gallium Hydroxide to Gallium Hydrochloride (EDIT: GaCl3:NH3 complex)
I should have just gone this route to begin by making the nitrate, and then thermally decomposing to ...
13-8-2017 at 18:16
by: Loptr
Gallium Hydroxide to Gallium Hydrochloride (EDIT: GaCl3:NH3 complex)
Alright, so I dissolved about 20 grams of gallium into a HCl(aq) solution, but ended up having to us ...
12-8-2017 at 19:12
by: Loptr
On the usefulness of amateur chemistry to society
My question is why does everyone seem to think that Sigma-Aldrich is a good idea to buy from, especi ...
8-8-2017 at 07:33
by: Loptr
Encrypted Lab Notebook
Yeah, no need to go to all that trouble to hide your lab notebook. What is in there that isn't alrea ...
6-8-2017 at 20:24
by: Loptr
Reduction with alkali metal and alcohol
Another interesting reagent is magnesium and methanol.

http://www.sciencemadness.org/talk/files.p ...
5-8-2017 at 17:21
by: Loptr
Sulforaphane synthesis for the amateur
It's an essential amino acid. I see it for sale on eBay.

EDIT:

Sorry, I see that it has one mo ...
1-8-2017 at 11:59
by: Loptr
POCl3,Acyls,Anhydrides,AlkalyMetals and Halogens
I would try posting coherent directed questions as posts, and not throw in the entire kitchen sink.
...
31-7-2017 at 05:34
by: Loptr
Pretty Pictures (2)
[rquote=489000&tid=26378&author=zts16]An intermediate product in the synthesis I'm doing at ...
28-7-2017 at 08:56
by: Loptr
Selling chemicals questions
[rquote=488858&tid=75754&author=LD5050][rquote=488849&tid=75754&author=PirateDocBrow ...
27-7-2017 at 09:31
by: Loptr
Sodium Acetate-'Hot Ice'-What Could I Have Made?
That sounds like a reasonable approach. It would help to keep the water at the minimum level needed ...
27-7-2017 at 09:29
by: Loptr
Things I Will Never Make
[rquote=488834&tid=72825&author=JJay]I'd probably use phenyllithium and copper (I) chloride. ...
27-7-2017 at 07:55
by: Loptr
Sodium Acetate-'Hot Ice'-What Could I Have Made?
Try adding [b]some[/b] (small test amount) of this powder to water in a test tube and letting it dis ...
27-7-2017 at 07:48
by: Loptr
Schmidt reaction - advice on solvents
[rquote=440106&tid=65413&author=AvBaeyer]The paper posted above by DFJ90 (thanks!) tells wha ...
27-7-2017 at 06:51
by: Loptr
Things I Will Never Make
[rquote=488769&tid=72825&author=JJay]I've actually been considering bromoacetaldehyde. I thi ...
26-7-2017 at 10:51
by: Loptr
Piperine extraction question
There you go--now onto separation and crystallization!

I am planning on doing this shortly with a ...
21-7-2017 at 07:10
by: Loptr
Use of K2CO3 instead of pyridine etc. as sacrificial base acid halide Ar-OH
Potassium carbonate is commonly used for this purpose. I have used it to neutralize the HBr released ...
20-7-2017 at 10:02
by: Loptr
Benzoic acid to benzaldehyde or benzyl alcohol
[rquote=488382&tid=14431&author=Booze]

Can I ask why references are so vastly necessary?
...
20-7-2017 at 09:49
by: Loptr
Acid Attacks in UK: Here We Go Again
Eventually even the rocks on the street will be the target of legislation.
14-7-2017 at 09:59
by: Loptr
Benzoic acid to benzaldehyde or benzyl alcohol
[rquote=487699&tid=14431&author=wayne_m]This paper shows ZnO or ZrO to be good catalysts for ...
12-7-2017 at 19:39
by: Loptr
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