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Picric acid sensitivity
[rquote=168431&tid=11304&author=entropy51][rquote=168429&tid=11304&author=ChrisWhewe ... |
29-12-2009 at 19:25
by: Fleaker |
Adulteration of gold with tungsten - continued
If tungsten were interspersed with gold, the detection would be quite simple. Anyone who has ever he ... |
28-12-2009 at 07:20
by: Fleaker |
Reactions in a 'Sealed Tube'
[quote]
You must be doing something seriously wrong. Either your tubing is too thin, of miserable ... |
28-12-2009 at 07:12
by: Fleaker |
Hanovia Bright Platinum coated anodes!
I've mentioned this numerous times before. Titanium can be platinum plated, but it must go wet (and ... |
26-12-2009 at 17:00
by: Fleaker |
Laboratory Tips and Tricks
[rquote=168170&tid=13156&author=DJF90]Use the amalgamated scrap in a vacuum dessicator and t ... |
26-12-2009 at 16:59
by: Fleaker |
Reactions in a 'Sealed Tube'
Quartz is hell to work with unless you've got the tools.
I've had an incident before with a seal ... |
26-12-2009 at 16:49
by: Fleaker |
Bismuth Nitrate
I don't remember the reaction of bismuth metal and nitric acid being all that vigorous. I think I to ... |
26-12-2009 at 16:47
by: Fleaker |
Reaction in Thunder in a Testube?
I wonder if it is presumptuous to think it only oxidizes the organics to their respective carboxylic ... |
9-11-2009 at 07:13
by: Fleaker |
Pd/C
Coal based charcoal is essentially coke. |
10-9-2009 at 03:11
by: Fleaker |
Pd/C
There are numerous ways to make an active Pd/C. PdCl2 can be dissolved in a suitable organic solvent ... |
9-9-2009 at 13:25
by: Fleaker |
starting a organic home lab
I can give a damn about his safety shower or white phosphorus, I want to see his version of the Cont ... |
28-8-2009 at 13:25
by: Fleaker |
Daigger?
Afraid of your getting put on a list? Your parents are afraid of that? Odd indeed that parents to a ... |
28-7-2009 at 16:25
by: Fleaker |
Spectrophotometers
U2U sent. |
12-7-2009 at 12:45
by: Fleaker |
Atomization process in ICP-MS apparatus
I have an excellent book on practical ICP-MS the name of which escapes me, but it discusses this in ... |
12-7-2009 at 12:43
by: Fleaker |
Spectrophotometers
As an aside, I'll only wait 5 days on these before they go to ebay. |
11-7-2009 at 10:34
by: Fleaker |
Spectrophotometers
I have some old but still functional (quite functional) spectrophotometers available.
Comes as ... |
11-7-2009 at 10:32
by: Fleaker |
Black Phosphorus
Well if he doesn't have oxy hydrogen, then he won't have success. Similarly, if he doesn't have ultr ... |
11-7-2009 at 10:12
by: Fleaker |
Ethyl/Isopropyl Bromide preparation
I've done it too. Just make sure that your bromine isn't horribly wet, and that it and your sulfuric ... |
11-7-2009 at 10:09
by: Fleaker |
microwave assisted chemical reaction
Eh, doing this in a domestic microwave isn't exactly the safest thing to do because it lacks the fee ... |
11-7-2009 at 09:58
by: Fleaker |
Adios
I will miss Sauron. I think he has been a valuable member here and has given much. I do not all the ... |
11-7-2009 at 09:35
by: Fleaker |
On the subject of ORMUS
Sounds like a waste of gold to me.
Send me all the pure gold you want though, I'll return pure no ... |
6-7-2009 at 10:57
by: Fleaker |
Adios
I hope he'll reconsider or perhaps take a short vacation. At the very least he should check his U2U ... |
6-7-2009 at 09:01
by: Fleaker |
Iodomethane prep.
P4O10 + 6 MeOH -> 2 MeOP(O)(OH)2 + 2 (MeO)2P(O)OH
is a very efficient reaction... thanks for t ... |
21-6-2009 at 09:20
by: Fleaker |
Storage of Fuming Nitric acid
I did the vanadium (V) oxide-catalyzed oxidation of SO2 and obtained interesting and encouraging res ... |
21-6-2009 at 08:56
by: Fleaker |
The Synthesis of Sulfur Trioxide and Oleum: the vanadium (V) oxide-catalyzed method
I like the ''yet'' part of your statement watson.fawkes! I had very encouraging results with this ex ... |
21-6-2009 at 08:52
by: Fleaker |
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