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Sarin from Ball-point ink by "CSIS"
Andi, methanol is not used. you are right about cyclohexanol, the other alcohol sometimes used is pi ...
16-4-2009 at 17:07
by: Sauron
Sarin from Ball-point ink by "CSIS"
It is a ridiculous assertion.

VX is produced from materials that are relatively hard to come by, ...
16-4-2009 at 14:07
by: Sauron
Junk members
You misread his morivation badly.

He is NOT a self promoting wannabe author. He is a troll.

He ...
16-4-2009 at 04:55
by: Sauron
Acetic anhydride preparation
First of all forget Rhodium.

If you work out the mass balance you will quickly see that it takes ...
15-4-2009 at 19:13
by: Sauron
If you had to ...
Take something lethal. At least you won't be wasting your time dreaming up silly exercises such as t ...
15-4-2009 at 13:18
by: Sauron
Junk members
The troll is back under his alias top secret. Another major round of spamming.
15-4-2009 at 07:25
by: Sauron
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
It depends on what fittings the box comes with, I would not count on the gloves being in serviceable ...
13-4-2009 at 21:51
by: Sauron
Junk members
Presently those posts are merely Detritused, they have not been deleted, and they still are showing ...
13-4-2009 at 07:54
by: Sauron
Chlorosulfonic acid
[rquote=150876&tid=12041&author=Sauron]Here is Reference 2, Williamson's paper decribing chl ...
11-4-2009 at 14:14
by: Sauron
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
In addition to the airlock this has a large door to allow karger equipment in and out, I would set o ...
10-4-2009 at 23:54
by: Sauron
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
Yes I have a full size airlock equipped lighted and electrically serviced Labconco glove box equippe ...
10-4-2009 at 21:28
by: Sauron
Chlorosulfonic acid
There's another claim that Cl2 and SO2 gives chlorosulfonic acid when passed through activated charc ...
10-4-2009 at 20:04
by: Sauron
Lab Prep of Diethyl Sulfate
I am not advocating making sodium ethyl sulfate. I am advocating the JACS article procedure which by ...
10-4-2009 at 19:15
by: Sauron
Chlorosulfonic acid
And reference 16 the last of the four references that Jackson says teach that Cl2 directly chlorinat ...
10-4-2009 at 11:50
by: Sauron
Chlorosulfonic acid
Here is reference 227 (from the Jackson review) from Ber 6 (1873) by Max Muller.
10-4-2009 at 11:03
by: Sauron
@woelen:
Well, here is a US patent to McKee and Salls that teaches that sulfuryl chloride and 100% H2SO4 or c ...
10-4-2009 at 10:47
by: Sauron
Chlorosulfonic acid
And Reference 13 from Ber. 11 (1878)
Also no obvious mention of Cl2 as such, although since it is i ...
10-4-2009 at 09:19
by: Sauron
Chlorosulfonic acid
Here's reference 358, the only one in English. I saw nothing about elemental chlorination of H2SO4, ...
10-4-2009 at 08:04
by: Sauron
Chlorosulfonic acid
Here is Reference 3 by Kirby Jackson from Chemical Review, the relevant pages are 81-83.

There's ...
10-4-2009 at 05:30
by: Sauron
Chlorosulfonic acid
Here is Reference 2, Williamson's paper decribing chlorination of H2SO4 with chlorides of P, in two ...
10-4-2009 at 05:02
by: Sauron
Chlorosulfonic acid
Sometimes an annoying trait in Mellor, and Gmelin, and ATBOIC, is that a promising one line will be ...
10-4-2009 at 04:44
by: Sauron
Chlorosulfonic acid
Nicodem, in the very passage you quote, a variety of chlorinating agents are stated to work on H2SO4 ...
10-4-2009 at 03:50
by: Sauron
Chlorosulfonic acid
Further. re hydrolsis of SO2Cl2:

Take ONE mol SO2Cl2 and add ONE mol water at ambient with stirri ...
10-4-2009 at 03:06
by: Sauron
Chlorosulfonic acid
Nicodem I posted an entire subchapter from Mellor with references and these claim that controlled hy ...
10-4-2009 at 02:56
by: Sauron
Lab Prep of Diethyl Sulfate
I think he means the sodium salt of ethyl hydrogen sulfate

Na replaces H in the -OH
10-4-2009 at 02:09
by: Sauron
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