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Phenylacetonitrile from Phenylalanine
DBDMH is soluble in acetone and ethanol, so what about an aqueous solvent system with one of those? ...
12-4-2018 at 19:29
by: Loptr
Mystery compound burning at ~400 degrees?
I hope they used PPE

[quote]
On burning SO2 and P2O5 are produced
[/quote]
12-4-2018 at 17:48
by: Loptr
Phenylacetonitrile from Phenylalanine
[rquote=513870&tid=76161&author=AvBaeyer]As an addendum, I have recently tried using 1,3-dib ...
12-4-2018 at 09:46
by: Loptr
Lab Labels
Thank you, Xeon! I appreciate you getting this started. I have had the intention of switching over t ...
10-4-2018 at 06:19
by: Loptr
Latest chemical order?
[rquote=508375&tid=9890&author=Geocachmaster]This just arrived today. I’m super excited be ...
9-4-2018 at 16:49
by: Loptr
Someone is wrong (about organic chemistry) on the Internet!
Why are we referencing that forum here?

What is it that you hope to gain?
7-4-2018 at 18:47
by: Loptr
Silver Nitrate for Sale
I keep mine slightly acidic and it stays bright white. I bought a few silver bars a while back and m ...
24-2-2018 at 07:55
by: Loptr
Catechol preparation
Hydroxylation and decarboxylation of hydroxybenzoic acids by
Fe[sup]2+[/sup]-chelates

Halvor Aar ...
19-2-2018 at 19:47
by: Loptr
Selling Silver Nitrate Profitable
You can sell silver nitrate on eBay. I have been in violation of their hazardous materials policy la ...
18-2-2018 at 16:30
by: Loptr
Synthesis of phenyl-2-ethanol
I seem to recall there being several factors around this, but in general if the reaction takes the S ...
30-1-2018 at 19:42
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
That's a good idea, but my interest wasn't in obtaining hydrocinnamaldehyde. It was more about the r ...
2-1-2018 at 19:42
by: Loptr
Diethyl Ether Storage
My wife would kill me! lol
22-12-2017 at 16:44
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
[rquote=499182&tid=78639&author=clearly_not_atara]I continue to recommend dithionite/PTC. Th ...
1-12-2017 at 16:46
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
According to this, there might be some issues with reducing double bonds in a,b-unsaturated carbonyl ...
1-12-2017 at 14:38
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
Well, this is certainly interesting. Hydroxylamine hydrochloride and ethyl acetate used for the prep ...
1-12-2017 at 14:29
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
[rquote=499139&tid=78639&author=CuReUS][rquote=499069&tid=78639&author=Loptr]I know ...
1-12-2017 at 07:10
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
http://orgsyn.org/demo.aspx?prep=cv7p0451

[file]62949[/file]

The discussion topic seems to im ...
30-11-2017 at 10:19
by: Loptr
Boron- Skylighter
The magnesium needs to be reasonably pure, but as Chem Player demonstrated in their ghetto Grignard ...
30-11-2017 at 08:43
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
I know that sodium in alcohol can reduce that double bond when it’s conjugated, not sure about whe ...
30-11-2017 at 06:34
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
Does an acetal still have the same character as a carbonyl? Would that double bond not then be consi ...
30-11-2017 at 06:26
by: Loptr
Reduce cinnamaldehyde to hydrocinnamaldehyde
Hey guys,

I am trying to reduce cinnamaldehyde to hydrocinnamaldehyde, and have several reducing ...
30-11-2017 at 05:42
by: Loptr
Boron- Skylighter
They still have magnesium up for sale on their website. I went ahead and bought 5lbs of it, add that ...
30-11-2017 at 05:22
by: Loptr
Schmidt reaction - advice on solvents
According to this paper solvents that have been used are choroform, benzene, and ether.

[file]61 ...
27-9-2017 at 18:16
by: Loptr
Piperine extraction question
[rquote=492664&tid=75566&author=LearnedAmateur]This is the first time I've heard of it, I ca ...
21-9-2017 at 11:08
by: Loptr
Piperine extraction question
[rquote=492540&tid=75566&author=LearnedAmateur][rquote=489611&tid=75566&author=XV750 ...
19-9-2017 at 13:01
by: Loptr
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