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keten lamp
I fear that you will find that acetic acid will eat your copper tube column very very happily.
N ... |
5-4-2007 at 05:38
by: Sauron |
toluene --> benzaldehyde
True enough, that 1900 German patent failed to mention yield.
Not so however the J.Org.Chem. art ... |
5-4-2007 at 05:05
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
Not my meaning at all.
For "recreational drugs" read "abuse drugs" which covers all the formally ... |
4-4-2007 at 22:32
by: Sauron |
keten lamp
Assuming that boilup rate is correct and stable so that the column does not flood, and that the colu ... |
4-4-2007 at 22:15
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
Oh, I can and do involve myself in medicinal chemistry, just not the recreational variety. |
4-4-2007 at 22:05
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
For every altruistic idealistic drug researcher there seem to be 1000 wannabe heads of the Cali Cart ... |
4-4-2007 at 21:37
by: Sauron |
toluene --> benzaldehyde
Your wish is my commend.
The review cites German Patent 127,388 of 1900, which may be same as @S. ... |
4-4-2007 at 21:11
by: Sauron |
P2P from recycled styrene?
You know, we deal with a lot of dual-use (or multiuse) compounds on this forum. Acetic anhydride has ... |
4-4-2007 at 21:08
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
The dilemna is that an amateur lab where the chemist is "researching drugs" is indistinguishable fro ... |
4-4-2007 at 20:52
by: Sauron |
Frustrating Chemical
Why not just make your own acetyl chloride from TCT and acetic acid?
Sounds like you want to do a ... |
4-4-2007 at 20:35
by: Sauron |
toluene --> benzaldehyde
In the Oxidation of ethanol thread, the use of nickel peroxide (aka nickel oxide hydroxide) arose, w ... |
4-4-2007 at 20:29
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
Being a professional criminal drug chemist is NOT amateur chemistry.
Unlike a few of our European ... |
4-4-2007 at 20:22
by: Sauron |
Illicit Drugs & Amateur Chemistry - What to do?
Check out this very same poster in the P2P from Styrene thread.
Just a fucking meth cook. |
4-4-2007 at 19:54
by: Sauron |
P2P from recycled styrene?
I see. So all that blather about what to do about the drug war, and how much amateur science was thr ... |
4-4-2007 at 19:47
by: Sauron |
keten lamp
The patent calls for refluxing the mixture for ten hours, and using the fractionating column during ... |
4-4-2007 at 19:43
by: Sauron |
keten lamp
All right, @hector, so this was VA and acetic acid with H2SO4 (Merck) as catalyst.
It will be som ... |
4-4-2007 at 09:06
by: Sauron |
keten lamp
OK @hector, now what reaction was this?
VA and AcOH?
or VA and AcCl?
And which proportions, ... |
4-4-2007 at 01:49
by: Sauron |
Oxidation of ethanol
@Eclectic, someone else (@JohnWW I believe) brought up the connection to viniculture in SS vats, it ... |
3-4-2007 at 22:26
by: Sauron |
keten lamp
I just searched Org.Syn. for reactions involving vinyl acetate, there are 12.
I studied two of th ... |
3-4-2007 at 22:18
by: Sauron |
Dry Ice Source
The Edmund ad claims 25% conversion efficiency which would be 2.5 Kg from a 10 Kg (net) cylinder.
... |
3-4-2007 at 19:48
by: Sauron |
keten lamp
This is not directed at hector2000
Please do not email me regarding advice about making Ac2O
P ... |
3-4-2007 at 18:55
by: Sauron |
Dear god... I have a LOT of sodium metal.
Got you both trumped.
Qty 12
500 g Na metal in paraffin oil
Panreac, Spain.
Total 6 Kg.
... |
3-4-2007 at 00:58
by: Sauron |
keten lamp
I already gave you my advice.
1. Do distill the VA in an attempt to free it from inhibitor.
2. ... |
2-4-2007 at 16:15
by: Sauron |
keten lamp
N2O4 is very toxic just like phosgene and ketene.
Someone else is experimenting with this no, wa ... |
2-4-2007 at 07:00
by: Sauron |
keten lamp
Ac2O is acetic anhydride
flash over means distill off rapidly
Acetic acid boils 117
If prod ... |
1-4-2007 at 18:24
by: Sauron |
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