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Illicit Drugs & Amateur Chemistry - What to do?
Wake up and smell the coffee. The drug cooks ARE and to a great extent already have ruined things fo ...
6-4-2007 at 21:25
by: Sauron
keten lamp
@chemicalpower:

The two stage reaction scheme is a MECHNISM for the overall reaction, not a PROCE ...
6-4-2007 at 21:17
by: Sauron
Acetic anhydride preparation
That is perfectly resonable.

It is an extremely rapid process, as I recall, and not a slow evolut ...
6-4-2007 at 20:57
by: Sauron
P2P from recycled styrene?
@Nicodem, I have NEVER advocating making weapons of mass destruction on or off this board. To say I ...
6-4-2007 at 20:47
by: Sauron
keten lamp
Try reading them AGAIN.
6-4-2007 at 08:06
by: Sauron
Illicit Drugs & Amateur Chemistry - What to do?
I find I am utterly disinterested in continuing to participate in a forum where so many members are ...
6-4-2007 at 08:02
by: Sauron
Acetic anhydride preparation
No reaction I ever heard of.
6-4-2007 at 07:49
by: Sauron
keten lamp
Try reading the posts and you might understand.

I even drew you a diagram.

The reaction is in ...
6-4-2007 at 02:55
by: Sauron
P2P from recycled styrene?
Bullshit. He's out to turn this into a meth cook's kaffee klatch, swapping recipes for P2P. And all ...
6-4-2007 at 02:42
by: Sauron
P2P from recycled styrene?
All you are doing is wingeing about your criminality being, after all, criminal.

You are not an a ...
6-4-2007 at 01:51
by: Sauron
Acetic anhydride preparation
SO2 is not rich dark red-brown. SO2 is colorless. I am well familiar with the smell of SO2 having ma ...
6-4-2007 at 01:47
by: Sauron
Illicit Drugs & Amateur Chemistry - What to do?
I suggest, @Tup, that you talk to some coke addicts, heroin addicts and amphetamine addicts before y ...
6-4-2007 at 01:32
by: Sauron
keten lamp
I advise that you use conc hydrochloric acid in place of H2SO4

I advise you to distill your VA fi ...
6-4-2007 at 01:13
by: Sauron
Acetic anhydride preparation
When I was a teenager I "discovered" a reaction that I have never bothered as an adult to elucidate. ...
5-4-2007 at 21:58
by: Sauron
Oxidation of ethanol
For oxidation of ethanol, to acetaldehyde it is useless.

To acetic acid, in inert organic solvent ...
5-4-2007 at 20:03
by: Sauron
Oxidation of ethanol
Yes, I noticed that, however it is not an exidation. It is a free radical initiation and dimerizatio ...
5-4-2007 at 17:45
by: Sauron
keten lamp
@hector, take heed. Try conc hydrochloric acid instead of sulfuric acid. @chemicalpower said that th ...
5-4-2007 at 09:59
by: Sauron
Melzer's reagent & chloral
Get or make trichloroacetic acid.

Reduce it to trichloroacetaldehyde. There are reducing agents t ...
5-4-2007 at 09:50
by: Sauron
Acetic anhydride preparation
Try something more inert like petroleum ether or toluene. Look up to double check they won't dissolv ...
5-4-2007 at 09:35
by: Sauron
Acetic anhydride preparation
@Per, wash the solid with a solvent that dissolves Ac2O but not NaNO2 or BaOAc. Filter. Then remove ...
5-4-2007 at 08:47
by: Sauron
Nitrobenzene
The nitro group being a deactivating one, you will have difficulty chlorinating nitrobenzene. If you ...
5-4-2007 at 07:20
by: Sauron
keten lamp
You are right, the patent teaches merely to fractionate off the acetaldehyde formed while refluxing ...
5-4-2007 at 06:56
by: Sauron
Acetic anhydride preparation
Did you dry your NO2 as described in Brauser?

Cold trap for gross moisture then PbO2 then P2O5?
...
5-4-2007 at 06:16
by: Sauron
keten lamp
Yes I wish I wish I could afford a nice PC-controlled, fully instrumented Teflon spinning band still ...
5-4-2007 at 06:04
by: Sauron
Frustrating Chemical
Phloroglucinol if what you mean I think (sym trihydroxybenzene.)

Anyway yes CCl4 can be made from ...
5-4-2007 at 05:47
by: Sauron
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