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Easy Route to Thionyl Chloride SOCl2
Thionyl chloride is not an easy compound to prepare. The classical method is a pressure reaction inv ...
13-4-2007 at 17:17
by: Sauron
Anodizing Aluminum
The process I am talking about certainly uses chillers to keep the temperatures down. That much I re ...
13-4-2007 at 16:14
by: Sauron
Anodizing Aluminum
What you want is Martin Hardcoat.

Most other anodizing just isn't very durable.
13-4-2007 at 15:10
by: Sauron
Posting pictures of purified safrole?
I look around and see none of those present. So I guess you are just venting.
13-4-2007 at 14:23
by: Sauron
Posting pictures of purified safrole?
@dedalus So? Your point is?

@eclectic, that's a slight improvement, but in that case, just who ar ...
13-4-2007 at 14:07
by: Sauron
keten lamp
I have now provided in this thread three simple ways to make acetyl chloride from cyanuric chloride ...
13-4-2007 at 11:33
by: Sauron
Posting pictures of purified safrole?
I never said you did so intentionally, nevertheless you did so, with resulting train wreck of a thre ...
13-4-2007 at 11:16
by: Sauron
Garage Experiments With Trichloromethane.
The haloform reaction is a general one for any compound having a methyl group alpha to a carbonyl.
...
13-4-2007 at 11:11
by: Sauron
Posting pictures of purified safrole?
That remark is in rather poor taste, @eclectic.
13-4-2007 at 11:06
by: Sauron
keten lamp
I've been telling @hector that for eight pages but he is stubborn.
13-4-2007 at 10:57
by: Sauron
Posting pictures of purified safrole?
There are a variety of governmental and non-governmental, international groups who do carcinogenicit ...
13-4-2007 at 10:54
by: Sauron
keten lamp
I think you are asking for trouble.

You can't scale up the lamp. You can't increase flow rate of ...
13-4-2007 at 10:27
by: Sauron
Posting pictures of purified safrole?
That's an important distinction.

But one lost all too often in the night and fog.

As far as I ...
13-4-2007 at 09:40
by: Sauron
keten lamp
@chemicalpower

Here is protocol for acetyl chloride at room temperature from CC and AcOH in aceto ...
13-4-2007 at 09:32
by: Sauron
Posting pictures of purified safrole?
As it appears that safrole is NOT a Schedule One controlled substance or any sort of controlled subs ...
13-4-2007 at 08:54
by: Sauron
Posting pictures of purified safrole?
It was described in this thread as Schedule One. That is not same as List One. Schedule One controll ...
13-4-2007 at 04:23
by: Sauron
Posting pictures of purified safrole?
Major difference. A lot of "energetics" are analytical reagents and as long as they are stored wet a ...
13-4-2007 at 04:07
by: Sauron
Posting pictures of purified safrole?
Theoretical photos?

Come now. Pics of doing it are the essence of practice. No "discussion" New ...
13-4-2007 at 03:48
by: Sauron
Posting pictures of purified safrole?
Told you so, Levi. I don't believe wicca has ANY exemptions under DEA regs and I seriously doubt tha ...
13-4-2007 at 03:36
by: Sauron
Posting pictures of purified safrole?
What pray tell is theoretical about posting PHOTOS of the PROCESS of fractional crystallization of S ...
13-4-2007 at 03:23
by: Sauron
Posting pictures of purified safrole?
If this guy is asking PERMISSION about whether or not it is appropriate then the only person who can ...
13-4-2007 at 02:44
by: Sauron
Posting pictures of purified safrole?
Your friend of a friend wants to make carcinogenic root beer?

Or just MDA?
13-4-2007 at 00:30
by: Sauron
Indium Mediated Redn of Aryl Nitro to Amine
I do understand basic research.

This is just an example of economically egregious basic research. ...
12-4-2007 at 19:54
by: Sauron
Prep of p-Nitrobenzyl Bromide & Relatives
True, but it's about same price as benzyl alcohol. The Vogel procedure from the alcohol, GAA and a l ...
12-4-2007 at 13:00
by: Sauron
keten lamp
First of all, there are more than one method to make acetyl chloride from CC.

1. Old method 1. Re ...
12-4-2007 at 10:13
by: Sauron
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