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Phosphorus Chlorides
The PCl5 + P2O5 reaction gives POCl3 not PCl3

and there are easier ways to make POCl3 if that is ...
24-4-2007 at 05:48
by: Sauron
keten lamp
Yes, that's why I specified 125 C. A drying over usually has ventilation option, and temp control. I ...
24-4-2007 at 03:44
by: Sauron
Making Ethanol
The preparation of the wash (mash) is different. The highest yielding starches are cassava, tapioca, ...
24-4-2007 at 03:38
by: Sauron
keten lamp
You heat the trihydrate in a drying oven (with the trihydrate in a large evaporation whish of shallo ...
24-4-2007 at 03:13
by: Sauron
Making Ethanol
Getting ethanol yields that high is subject of research.

12-16% is more typical, 20% possible wit ...
24-4-2007 at 02:05
by: Sauron
keten lamp
Not yet. I have requested quote for VA, and I have purchased a pressure reactor in case the reaction ...
24-4-2007 at 01:50
by: Sauron
Unnecessary enmity
I'll see that yawn and raise you ten z's

ZZZZZZZZZZ
23-4-2007 at 05:14
by: Sauron
toluene --> benzaldehyde
Maybe they added some curry as a PTC.
23-4-2007 at 02:25
by: Sauron
EMNITY not ENMITY chemrox pls edit title!
Polverone is right. This is a chemistry forum first, an amateur science forum second and a politics& ...
23-4-2007 at 02:21
by: Sauron
keten lamp
Just remember to do the fractionation as slowly as you can stand to.

And don't let AcCl get out o ...
23-4-2007 at 01:54
by: Sauron
keten lamp
It would not hurt to refractionate the product.

How are you measuring the temperature? And where? ...
23-4-2007 at 00:10
by: Sauron
Making Ethanol
@Hector, there is nothing to excuse. Your English is okay.

The English think Americans can't spea ...
22-4-2007 at 23:29
by: Sauron
Making Ethanol
I suspect that harly anyone from Morocco to Irian Jaya is slavering for "real" bread, @Roscoe -- you ...
22-4-2007 at 12:25
by: Sauron
Making Ethanol
Mever been to Utah, huh?

And Texas is mostly package liquor only, sale of mixed drinks in restaur ...
22-4-2007 at 11:56
by: Sauron
Making Ethanol
Dry counties or dry countries?

Being from the American South I can assure you that we have more t ...
22-4-2007 at 11:26
by: Sauron
Making Ethanol
So rarely am I EVER accused of being PC that it is amusing when it happens.

How about simple cour ...
22-4-2007 at 10:38
by: Sauron
Making Ethanol
Unleavened bread.

Like religious Jews eat at Passover.

Nice fresh chapatti is really quite ni ...
22-4-2007 at 10:03
by: Sauron
Making Ethanol
@Roscoe, you want to go there, pls do so in Whimsy. If you do so I will happily delete my own remark ...
22-4-2007 at 09:25
by: Sauron
Making Ethanol
The point, @sandmeyer, was that the ethanol recovered from EtOAc is of unknown origin, most likely f ...
22-4-2007 at 01:15
by: Sauron
Making Ethanol
@hector, I could be wrong but I think you may have to dliver the alkili (NaOH) in water, so resultin ...
22-4-2007 at 00:32
by: Sauron
Making Ethanol
Thanks for stating the obvious but @hector as usual can think of a million reasons why not to do it.
21-4-2007 at 18:16
by: Sauron
Making Ethanol
Fer,emtation is finicky, messy, low yielding, and prone to microbial competition. Distillation (whic ...
21-4-2007 at 16:44
by: Sauron
Making Ethanol
Lye is.

Anyway most EtOAc is made from ethanol produced synthetically and by international agreem ...
21-4-2007 at 09:34
by: Sauron
Making Ethanol
Can you get ethyl acetate?

If so it is easy to saponify it w/NaOH to ethanol + sodium acetate.

...
21-4-2007 at 08:59
by: Sauron
Reduction of 2-Piperidone (delta-Valerolactam)
QSAR/QSPR is not so much a matter of theory as it is the assembly of empirical datasets and then the ...
21-4-2007 at 08:53
by: Sauron
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