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Synthesis of L-Phenylacetylcarbinol(L-PAC)
Well, I always find acyl chloride preps interesting, esp. oddball ones. Regarding your question on ... |
28-4-2009 at 20:01
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
And here is the prep of the reagent 1,1-dichloromethyl methyl ether
Assuming that lactyl chloride ... |
28-4-2009 at 18:20
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
That Org.Syn. monohraph is >25 years old, a lot can happen in a quarter century of chemistry.
... |
28-4-2009 at 17:50
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Quite right. I did not say that LPAC can be made from phenylglyovalic acid. Somone else posted that ... |
28-4-2009 at 16:36
by: Sauron |
MCA sulponation
Thr ptoduct depends on the workup.
Cl-SO2-OH reacts at the -OH with the aryl compound end and giv ... |
28-4-2009 at 00:15
by: Sauron |
Fresh Look at Sulfur Halide Rxn w/Acyl Salts
Well done!
You were smart to buy the anhydrous NaOAc as this is the point so many others got stuc ... |
27-4-2009 at 22:42
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
DJK, FC with benzeme and oxalyl chloride will not produce the dione you describe (1-phenyl-1,2-propa ... |
27-4-2009 at 17:15
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
First of all there are many different yeast methods and many different yeasts.
There are continuo ... |
27-4-2009 at 12:21
by: Sauron |
Fuck "Pyrex"
Pyrex is a trademark of Corning
Kimax is a trade name of Kimble
Both are borosilicate
DO NOT ... |
27-4-2009 at 04:41
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Biotech is not simple and not cheap.
Hygiene is critical.
Anyway, S.crevicea is not the ideal ... |
27-4-2009 at 04:16
by: Sauron |
Fresh Look at Sulfur Halide Rxn w/Acyl Salts
Use a batter pump and distill at c.25 mm Hg not 580 mm on a water bath (a rotav is ideal) and you wi ... |
27-4-2009 at 04:03
by: Sauron |
Sodium Hyponitrite
How stable is it?
If it has a long shelf life, just keeping it is an option.
What brand is it? ... |
26-4-2009 at 20:43
by: Sauron |
Fuck "Pyrex"
There's a lot of phony "pyrex" around that is not borosilicate.
This is particularlytrue of house ... |
26-4-2009 at 20:27
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
This is a replay of hector's demeanor in the AA thread.
Naked wholesale demand for spoonfeeding
... |
26-4-2009 at 16:00
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
No comment needed re the "famous" UF. |
26-4-2009 at 05:36
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Read the patent
Benzaldehyde (106 mg, 1 mmol),
petroleum ether (80 ml),
ethanol (0.5 ml),
b ... |
26-4-2009 at 05:16
by: Sauron |
Synthesis of L-Phenylacetylcarbinol(L-PAC)
3333 x c.100 ml is 333 liters and that is the vioreactor size needed to make 100 g L-PAC a day per t ... |
26-4-2009 at 03:02
by: Sauron |
Canadian Intelligence: an Oxymoron
Let them wallow in their mis- or dis-imformation.
[Edited on 25-4-2009 by Sauron] |
24-4-2009 at 19:19
by: Sauron |
Controlled substances/grandfathered?
Yes, nanny. |
24-4-2009 at 13:44
by: Sauron |
Controlled substances/grandfathered?
Well mark me down as hard right then.
Waterboarding is to torture what a wet noodle is to a bullw ... |
24-4-2009 at 03:14
by: Sauron |
Disapearing posts
Recent posts in References have also vanished |
20-4-2009 at 14:00
by: Sauron |
Sarin from Ball-point ink by "CSIS"
That's very glib. What makes you think that the Levinstein process is conducted at anything but STP? ... |
20-4-2009 at 10:59
by: Sauron |
Sarin from Ball-point ink by "CSIS"
chief, between them Iran and Iraq in a brief period in the 1980s bought up the entire production cap ... |
20-4-2009 at 04:44
by: Sauron |
Spammer Report Thread
My advice is, put this thread in a PW protected forum because if not then it plays to the sick ego o ... |
19-4-2009 at 11:15
by: Sauron |
Sarin from Ball-point ink by "CSIS"
Thiodiglycol is not the main way to make mustard, nor is mustard the only vesicant, or even the most ... |
18-4-2009 at 15:52
by: Sauron |
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