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Picric acid: different instructions
That sounds good. I think my fourth batch will be OK. I left it in the fridge after leaving it out f ... |
16-12-2022 at 17:59
by: ManyInterests |
Picric acid: different instructions
[quote] Urbanski tome 1 mentions that the French method he describes gives poor yields in Russia  [ ... |
15-12-2022 at 18:44
by: ManyInterests |
Picric acid: different instructions
Yeah, I was making what should have been super obvious mistakes! Right now I ran into another compli ... |
15-12-2022 at 14:03
by: ManyInterests |
Experimental synthesis of Trinitrofructose
Ok I will try that out with the American cold packs I got. |
15-12-2022 at 07:23
by: ManyInterests |
Picric acid: different instructions
OK so I will rewrite my steps again (for me to reference, and for posterity, for future picric acid ... |
15-12-2022 at 03:34
by: ManyInterests |
Picric acid: different instructions
Is it better to crash it in ice cubes (as Rosco wrote) or just ice cold water? It's actually kinda h ... |
15-12-2022 at 03:00
by: ManyInterests |
Picric acid: different instructions
The picture is from my third batch. I will describe everything on what happened.
The synthesis we ... |
14-12-2022 at 20:42
by: ManyInterests |
Picric acid: different instructions
OK this is not good. I think I am doing something REALLY wrong with all my picric acid synthesis. I ... |
14-12-2022 at 19:40
by: ManyInterests |
New chemical restrictions in Canada?
Well I will be running into some problems. While not a legal thing. Westlab apparently stopped selli ... |
13-12-2022 at 20:00
by: ManyInterests |
Sources of Diethylene glycol, Triethylene glycol, and 1,2,4-Butanetriol
I found a common product nearby that is 99-100% DEG (with the possible 1% being EG) Coghlan's Camp H ... |
13-12-2022 at 15:43
by: ManyInterests |
Experimental synthesis of Trinitrofructose
I ordered some of those cold packs. I filtered out the insolubles and dried everything, but it didn ... |
13-12-2022 at 15:13
by: ManyInterests |
Picric acid: different instructions
[rquote=679368&tid=389&author=Herr Haber]Adding water at the end of nitration dilutes the su ... |
12-12-2022 at 11:02
by: ManyInterests |
Picric acid: different instructions
So after filtering I did boil down the remaining liquid by half or so, then I decided to let it cool ... |
12-12-2022 at 09:37
by: ManyInterests |
Experimental synthesis of Trinitrofructose
The ammonium nitrate you use, is it the 34-0-0 stuff or is it the Calcium-Ammonium nitrate you get f ... |
11-12-2022 at 15:49
by: ManyInterests |
Picric acid: different instructions
So my third batch is basically done, just some cooling time and then evaporating the rest still in o ... |
11-12-2022 at 15:13
by: ManyInterests |
Experimental synthesis of Trinitrofructose
I'm going to need to go on a long nitric acid making bender. I have a little azeotropic nitric acid ... |
9-12-2022 at 11:52
by: ManyInterests |
Det Cap Strategies
[rquote=678807&tid=146585&author=Laboratory of Liptakov]Casting is much more laborious and t ... |
9-12-2022 at 09:18
by: ManyInterests |
Experimental synthesis of Trinitrofructose
I ordered some pure granulated fructose to do this experiment.
It's also good that you kept it fo ... |
8-12-2022 at 19:17
by: ManyInterests |
Picric acid: different instructions
So I finally was able to dry the picric of my first two synths. I got a total yield of 103 grams and ... |
8-12-2022 at 14:27
by: ManyInterests |
Z Library seized
What? Man I booked marked that page. I'm going to need to go to the Tor version and download all tha ... |
8-12-2022 at 08:37
by: ManyInterests |
Picric acid: different instructions
Good so I am safe. Thank you for that. |
7-12-2022 at 11:53
by: ManyInterests |
Picric acid: different instructions
[rquote=679150&tid=389&author=Herr Haber]I worry a bit about the Al because even Ca in the f ... |
6-12-2022 at 11:10
by: ManyInterests |
Picric acid: different instructions
Well it's kinda too late when it comes to combining batches since I put them both together (albeit I ... |
5-12-2022 at 17:19
by: ManyInterests |
Picric acid: different instructions
[rquote=679089&tid=389&author=B(a)P]Looks like a different crystal size/shape? That would li ... |
3-12-2022 at 00:34
by: ManyInterests |
Erythritol Tetranitrate
[rquote=679086&tid=1100&author=Laboratory of Liptakov]Experience says that hot methanol is t ... |
3-12-2022 at 00:25
by: ManyInterests |
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