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Catechol preparation
I think I have found 2 better syntheses for catechol:

One starts with guaiacol and uses 48% HBr. ...
9-1-2018 at 19:55
by: Magpie
Catechol preparation
Thanks so much yobbo II. I have a 400w source of h√ so will give this a try.
9-1-2018 at 14:57
by: Magpie
Phosphorous pentoxide from phosphate?
I have bought P2O5 from a supplier in Poland. Recently I ordered a lb from Firefox Enterprises in P ...
8-1-2018 at 22:08
by: Magpie
Catechol preparation
yes, I believe it was! It might have been in a referenced paper.
8-1-2018 at 22:05
by: Magpie
catechol
I remember reading on this forum about making catechol using calcium bromide. This was 1-2 months a ...
8-1-2018 at 19:24
by: Magpie
Phosphorous pentoxide from phosphate?
[rquote=502918&tid=66317&author=ave369]Does anyone have an experience of losing glassware to ...
7-1-2018 at 18:05
by: Magpie
Concentrating phosphoric acid
See "Phosphoric acid from calcium phosphate" in Prepublication.
6-1-2018 at 17:20
by: Magpie
Adventures in acetalization
Here's the mechanisms for the esterifications of vanillin:

in base:

[file]63905[/file]

in ...
6-1-2018 at 15:04
by: Magpie
Adventures in acetalization
The experiment is from "Introduction to Organic Laboratory Techniques, a Small Scale Approach," by P ...
6-1-2018 at 12:02
by: Magpie
Adventures in acetalization
This is very nice work, Crowfjord. Thanks for the well done write-up.

In organic chemistry clas ...
5-1-2018 at 20:56
by: Magpie
New information For UK chemists
I use oxalic acid (Bartender's Friend) almost daily to clean my sink and glass top stove. It's non- ...
4-1-2018 at 20:07
by: Magpie
Sodium Cyanate into Sodium Cyanide
Yes, you should get about 30-35% sodium cyanide. Let us know what you get.

Dissolve in warm wate ...
4-1-2018 at 09:11
by: Magpie
Thermometers
My problem with thermometers is that often times I cannot read them because the area of interest is ...
2-1-2018 at 14:46
by: Magpie
Sodium Cyanate into Sodium Cyanide
[rquote=502097&tid=79311&author=chemplayer...]Ok sorry must have missed that bit, but that r ...
1-1-2018 at 08:25
by: Magpie
Slow high torque electric motors for stirrer?
[rquote=502006&tid=41539&author=GrayGhost-]
For more torque im thinking in use washing mach ...
31-12-2017 at 10:53
by: Magpie
Reduce cinnamaldehyde to hydrocinnamaldehyde
Could sodium metabisulfite be use to protect the aldehyde?
31-12-2017 at 10:35
by: Magpie
Slow high torque electric motors for stirrer?
[rquote=501998&tid=41539&author=GrayGhost-]Im use a chip chinese type Dremmel, with stainles ...
30-12-2017 at 14:55
by: Magpie
Separating phthalic acid isomers
xylene is available at the hardware store. Can m-xylene be converted to resorcinol with facility? ...
30-12-2017 at 09:49
by: Magpie
Sodium Cyanate into Sodium Cyanide
Use carbon in a covered crucible. Check the cyanide thread for the temperature regimen.
30-12-2017 at 09:47
by: Magpie
Proper tubing for vacuum - what works best?
Buy red rubber hose for vacuum at Carolina Biological.
30-12-2017 at 09:44
by: Magpie
SOCL2
How much do you need and how much are you willing to pay?
30-12-2017 at 09:27
by: Magpie
Calcium Acetate dry distillation
If you have material crystallizing in your condenser you don't need a condenser. But if you use one ...
29-12-2017 at 22:10
by: Magpie
keten lamp
[rquote=501741&tid=8148&author=sykronizer]NZniceguy.....you've got far too much wire coiled ...
28-12-2017 at 20:48
by: Magpie
Synthesis of malonic acid
You can easily get a dangerous runaway reaction if the nitric is too strong or added too fast.
27-12-2017 at 20:13
by: Magpie
Where is Blogfast25 ?
I think Blogfast is a chemical engineer, like me. But he knew much more about advanced math and phy ...
26-12-2017 at 14:54
by: Magpie
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